FR2529472A1 - Nouveau type de micro-unite de test catalytique avec systeme de prelevement par vannes d'echantillonnage - Google Patents
Nouveau type de micro-unite de test catalytique avec systeme de prelevement par vannes d'echantillonnage Download PDFInfo
- Publication number
- FR2529472A1 FR2529472A1 FR8211891A FR8211891A FR2529472A1 FR 2529472 A1 FR2529472 A1 FR 2529472A1 FR 8211891 A FR8211891 A FR 8211891A FR 8211891 A FR8211891 A FR 8211891A FR 2529472 A1 FR2529472 A1 FR 2529472A1
- Authority
- FR
- France
- Prior art keywords
- analysis
- valves
- valve
- microunitis
- sampling system
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000005070 sampling Methods 0.000 title claims description 14
- 238000012360 testing method Methods 0.000 title claims description 13
- 230000003197 catalytic effect Effects 0.000 title description 4
- 239000003054 catalyst Substances 0.000 claims abstract description 9
- 238000007670 refining Methods 0.000 claims abstract description 3
- 238000004458 analytical method Methods 0.000 claims description 13
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000003786 synthesis reaction Methods 0.000 claims description 3
- 238000005259 measurement Methods 0.000 claims description 2
- 238000011282 treatment Methods 0.000 claims description 2
- 239000012847 fine chemical Substances 0.000 claims 1
- 239000003348 petrochemical agent Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 4
- 238000002347 injection Methods 0.000 abstract description 2
- 239000007924 injection Substances 0.000 abstract description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000007789 gas Substances 0.000 description 7
- 238000004587 chromatography analysis Methods 0.000 description 6
- HGCIXCUEYOPUTN-UHFFFAOYSA-N cyclohexene Chemical compound C1CCC=CC1 HGCIXCUEYOPUTN-UHFFFAOYSA-N 0.000 description 6
- 238000005336 cracking Methods 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000012159 carrier gas Substances 0.000 description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
- 238000004523 catalytic cracking Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000003708 ampul Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000004517 catalytic hydrocracking Methods 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 229960004279 formaldehyde Drugs 0.000 description 1
- 235000019256 formaldehyde Nutrition 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
- 238000011176 pooling Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000002407 reforming Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/0053—Controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8211891A FR2529472A1 (fr) | 1982-07-05 | 1982-07-05 | Nouveau type de micro-unite de test catalytique avec systeme de prelevement par vannes d'echantillonnage |
| DE19833324044 DE3324044A1 (de) | 1982-07-05 | 1983-07-04 | Katalytische mikrotesteinheit |
| GB08318196A GB2124369B (en) | 1982-07-05 | 1983-07-05 | Catalytic test apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8211891A FR2529472A1 (fr) | 1982-07-05 | 1982-07-05 | Nouveau type de micro-unite de test catalytique avec systeme de prelevement par vannes d'echantillonnage |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2529472A1 true FR2529472A1 (fr) | 1984-01-06 |
| FR2529472B1 FR2529472B1 (enrdf_load_stackoverflow) | 1985-01-18 |
Family
ID=9275755
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR8211891A Granted FR2529472A1 (fr) | 1982-07-05 | 1982-07-05 | Nouveau type de micro-unite de test catalytique avec systeme de prelevement par vannes d'echantillonnage |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE3324044A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2529472A1 (enrdf_load_stackoverflow) |
| GB (1) | GB2124369B (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2583519A1 (fr) * | 1985-06-17 | 1986-12-19 | Inst Francais Du Petrole | Procede et appareillage de test et d'analyse en ligne permettant d'etablir un bilan matiere d'une reaction chimique |
| FR2777805A1 (fr) * | 1998-04-24 | 1999-10-29 | Inst Francais Du Petrole | Appareillage de type micropilote et procede de test catalytique |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD257206A1 (de) * | 1987-02-02 | 1988-06-08 | Buna Chem Werke Veb | Integralreaktorschuss zur untersuchung heterogen-katalytischer prozesse |
| ES2120842B1 (es) * | 1995-02-23 | 1999-05-16 | Univ Pais Vasco | Equipo de reaccion para ensayos cineticos para prueba de catalizadores o reacciones a escala de laboratorio. |
| FI106409B (fi) * | 1998-05-15 | 2001-01-31 | Fortum Oil & Gas Oy | Järjestely ja menetelmä lyhyen kosketusajan reaktioita varten tarkoitettujen heterogeenisten katalyyttien testaamiseksi |
| US7256052B2 (en) * | 2002-10-18 | 2007-08-14 | Exxonmobil Chemical Patents Inc. | Chemical reaction and analysis system |
| CN103069273A (zh) * | 2010-06-16 | 2013-04-24 | 道达尔研究技术弗吕公司 | 实现反应器流出物的详细分析的采样和分析方法 |
| CN111491725B (zh) * | 2017-11-03 | 2023-04-18 | Hte高通量实验公司 | 用于表征催化过程的设备和方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1553090A (enrdf_load_stackoverflow) * | 1967-11-30 | 1969-01-10 |
-
1982
- 1982-07-05 FR FR8211891A patent/FR2529472A1/fr active Granted
-
1983
- 1983-07-04 DE DE19833324044 patent/DE3324044A1/de not_active Withdrawn
- 1983-07-05 GB GB08318196A patent/GB2124369B/en not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1553090A (enrdf_load_stackoverflow) * | 1967-11-30 | 1969-01-10 |
Non-Patent Citations (1)
| Title |
|---|
| IND. ENG. CHEM. FUNDAM., vol. 18, no. 4, 1979, WASHINGTON D.C. (US), W.A. SMIGIEL et al.: "Development of a microreactor system to measure catalytic activity on Ion-implanted, monocrystalline supports", pages 419-422. * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2583519A1 (fr) * | 1985-06-17 | 1986-12-19 | Inst Francais Du Petrole | Procede et appareillage de test et d'analyse en ligne permettant d'etablir un bilan matiere d'une reaction chimique |
| EP0206905A3 (en) * | 1985-06-17 | 1990-10-10 | Institut Francais Du Petrole | On line test and analysis method and apparatus to obtain a material balance of a chemical reaction |
| FR2777805A1 (fr) * | 1998-04-24 | 1999-10-29 | Inst Francais Du Petrole | Appareillage de type micropilote et procede de test catalytique |
| NL1011869C2 (nl) * | 1998-04-24 | 2000-01-07 | Inst Francais Du Petrole | Inrichting van het micro-proeffabriektype en katalytische testwerkwijze. |
| US6497844B1 (en) | 1998-04-24 | 2002-12-24 | Institut Francais Du Petrole | Micropilot-type equipment for catalytic testing process |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2529472B1 (enrdf_load_stackoverflow) | 1985-01-18 |
| GB8318196D0 (en) | 1983-08-03 |
| GB2124369B (en) | 1986-07-16 |
| GB2124369A (en) | 1984-02-15 |
| DE3324044A1 (de) | 1984-01-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |