FR2528417B1 - Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse - Google Patents

Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse

Info

Publication number
FR2528417B1
FR2528417B1 FR8309765A FR8309765A FR2528417B1 FR 2528417 B1 FR2528417 B1 FR 2528417B1 FR 8309765 A FR8309765 A FR 8309765A FR 8309765 A FR8309765 A FR 8309765A FR 2528417 B1 FR2528417 B1 FR 2528417B1
Authority
FR
France
Prior art keywords
ethylene
hydrolysis
glycol
extraction
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
FR8309765A
Other languages
English (en)
French (fr)
Other versions
FR2528417A1 (fr
Inventor
Vijay Sharatchandra Bhise
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Halcon SD Group Inc
Original Assignee
Halcon SD Group Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Halcon SD Group Inc filed Critical Halcon SD Group Inc
Publication of FR2528417A1 publication Critical patent/FR2528417A1/fr
Application granted granted Critical
Publication of FR2528417B1 publication Critical patent/FR2528417B1/fr
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/12—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of mineral acids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)
  • Treatment Of Fiber Materials (AREA)
FR8309765A 1982-06-14 1983-06-13 Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse Expired FR2528417B1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/388,395 US4400559A (en) 1982-06-14 1982-06-14 Process for preparing ethylene glycol

Publications (2)

Publication Number Publication Date
FR2528417A1 FR2528417A1 (fr) 1983-12-16
FR2528417B1 true FR2528417B1 (fr) 1986-01-17

Family

ID=23533945

Family Applications (1)

Application Number Title Priority Date Filing Date
FR8309765A Expired FR2528417B1 (fr) 1982-06-14 1983-06-13 Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse

Country Status (25)

Country Link
US (1) US4400559A (enExample)
JP (1) JPS5921634A (enExample)
KR (1) KR870000542B1 (enExample)
AR (1) AR241527A1 (enExample)
AU (1) AU556132B2 (enExample)
BE (1) BE897039A (enExample)
BR (1) BR8303125A (enExample)
CA (1) CA1219602A (enExample)
CH (1) CH656871A5 (enExample)
DD (1) DD210026A5 (enExample)
DE (1) DE3321448A1 (enExample)
EG (1) EG16051A (enExample)
ES (1) ES8501357A1 (enExample)
FR (1) FR2528417B1 (enExample)
GB (1) GB2122614B (enExample)
IN (1) IN159399B (enExample)
IT (1) IT1169063B (enExample)
MX (1) MX157512A (enExample)
NL (1) NL8302020A (enExample)
NO (1) NO159164C (enExample)
RO (1) RO88641A (enExample)
SE (1) SE459089B (enExample)
SU (1) SU1572414A3 (enExample)
YU (1) YU44436B (enExample)
ZA (1) ZA834364B (enExample)

Families Citing this family (45)

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US4508927A (en) * 1983-08-02 1985-04-02 The Halcon Sd Group, Inc. Preparation of glycols from ethylene oxide
US4519875A (en) * 1984-05-09 1985-05-28 The Halcon Sd Group, Inc. Purification of ethylene glycol derived from ethylene carbonate
EP0385631A1 (en) * 1989-02-21 1990-09-05 ARCO Chemical Technology, L.P. Oxidation process
US5322626A (en) * 1990-03-02 1994-06-21 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5240603A (en) * 1990-03-02 1993-08-31 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5094741A (en) * 1990-03-02 1992-03-10 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5133859A (en) * 1990-03-02 1992-07-28 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
GB9005814D0 (en) * 1990-03-15 1990-05-09 Shell Int Research A two-step monoethylene glycol preparation process
JPH04301463A (ja) * 1991-03-29 1992-10-26 Sharp Corp 印字装置
JPH0539952U (ja) * 1991-10-29 1993-05-28 三洋電機株式会社 プリンター装置
US5932101A (en) * 1996-08-29 1999-08-03 Eastman Chemical Company Process for fluid/dense gas extraction under enhanced solubility conditions
AU749910B2 (en) * 1998-03-19 2002-07-04 Mitsubishi Chemical Corporation Method for producing monoethylene glycol
RU2137748C1 (ru) * 1998-11-16 1999-09-20 Открытое акционерное общество "Нижнекамскнефтехим" Способ получения концентрированного водного раствора моноэтиленгликоля
US6372925B1 (en) * 2000-06-09 2002-04-16 Shell Oil Company Process for operating the epoxidation of ethylene
KR100980123B1 (ko) * 2002-06-28 2010-09-03 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 촉매 선택성을 향상시키는 방법 및 올레핀 에폭시화 방법
JP4333153B2 (ja) * 2003-02-07 2009-09-16 三菱化学株式会社 アルキレングリコールの製造方法
WO2004069777A1 (ja) * 2003-02-07 2004-08-19 Mitsubishi Chemical Corporation アルキレン誘導体の製造方法及びアルキレン誘導体製造用触媒の再生方法
US20040220433A1 (en) * 2003-03-28 2004-11-04 Evert Van Der Heide Process for the preparation of propylene glycol
US7348444B2 (en) * 2003-04-07 2008-03-25 Shell Oil Company Process for the production of an olefin oxide
JP2006522774A (ja) * 2003-04-09 2006-10-05 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー アルカンジオールの調製方法
US8148555B2 (en) * 2003-06-26 2012-04-03 Shell Oil Company Method for improving the selectivity of a catalyst and a process for the epoxidation of an olefin
JP4657206B2 (ja) * 2003-06-30 2011-03-23 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー プロピレンカーボネートの製造方法
US7378540B2 (en) * 2005-10-21 2008-05-27 Catalytic Distillation Technologies Process for producing organic carbonates
TW200738332A (en) * 2006-02-03 2007-10-16 Shell Int Research A process for treating a catalyst, the catalyst, and use of the catalyst
TWI387584B (zh) * 2006-03-13 2013-03-01 Shell Int Research 碳酸伸烷酯之生產方法及由此生產之碳酸伸烷酯於烷二醇及碳酸二烷酯之製造中之用途
ES2339819T3 (es) * 2006-06-13 2010-05-25 Shell Internationale Research Maatschappij B.V. Separacion y purificacion de glicoles.
CN100586913C (zh) * 2006-08-10 2010-02-03 中国石化扬子石油化工有限公司 催化水合法制备乙二醇的方法
TWI446964B (zh) 2007-05-09 2014-08-01 Shell Int Research 環氧化催化劑，製備該催化劑之方法及製備烯烴氧化物、１，２-二醇、１，２-二醇醚、１，２-碳酸酯或烷醇胺之方法
WO2009021830A1 (en) * 2007-08-14 2009-02-19 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycol
WO2009124987A1 (en) * 2008-04-09 2009-10-15 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene glycol
CN102036940B (zh) * 2008-04-10 2013-11-13 国际壳牌研究有限公司 制备亚烷基二醇的方法
PL2297125T3 (pl) * 2008-05-07 2013-12-31 Shell Int Research Sposób wytwarzania tlenku olefiny, 1,2-diolu, eteru 1,2-diolu, 1,2-węglanu albo alkanoloaminy
CA2723517C (en) * 2008-05-07 2017-03-07 Shell Internationale Research Maatschappij B.V. A process for the start-up of an epoxidation process, a process for the production of ethylene oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine
JP2011524857A (ja) * 2008-05-15 2011-09-08 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー アルキレンカーボネートおよびアルキレングリコールの調製のための方法
JP2011520895A (ja) 2008-05-15 2011-07-21 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー アルキレンカーボネートおよび／またはアルキレングリコールの調製のための方法
JP5511979B2 (ja) * 2010-06-07 2014-06-04 中国科学院過程工程研究所 イオン液体触媒によるエチレングリコールの製造方法
US8802900B2 (en) * 2010-11-29 2014-08-12 Shell Oil Company Process for the preparation of ethylene glycol
KR102027597B1 (ko) * 2011-04-29 2019-10-01 쉘 인터내셔날 리써취 마트샤피지 비.브이. Ｅｏ 촉매의 선택성 개선 방법
WO2013028039A2 (ko) * 2011-08-24 2013-02-28 롯데케미칼 주식회사 알킬렌 카보네이트 및/또는 알킬렌 글리콜 합성용 촉매의 재생 방법 및 알킬렌 카보네이트 및/또는 알킬렌 글리콜의 제조 방법
CN107915577B (zh) * 2016-10-08 2020-12-29 中国石油化工股份有限公司 碳酸乙烯酯水解合成乙二醇的方法
JP7107934B2 (ja) 2016-12-02 2022-07-27 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー エチレンエポキシ化触媒のコンディショニング方法およびエチレンオキシドの生成の関連方法
WO2018211013A1 (en) * 2017-05-19 2018-11-22 Shell Internationale Research Maatschappij B. V. Heat integratyion in a process for the preparation of ethylene carbonate and ethylene glycol
KR102796531B1 (ko) 2018-12-10 2025-04-18 쉘 인터내셔날 리써취 마트샤피지 비.브이. 에틸렌 글리콜의 제조 방법
WO2021140063A1 (en) * 2020-01-09 2021-07-15 Shell Internationale Research Maatschappij B.V. Process for the preparation of ethylene glycol
WO2024137896A1 (en) * 2022-12-21 2024-06-27 Renewco2 Inc. Liquid electrolyzer for single-conversion-step electrocatalytic reduction of co2 to ethylene glycol

Family Cites Families (6)

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US4117250A (en) * 1977-12-22 1978-09-26 Union Carbide Corporation Continuous process for producing alkylene glycols from alkylene carbonates
US4237324A (en) * 1979-01-22 1980-12-02 The Dow Chemical Company Production of monoglycols from alkylene carbonates
CA1121389A (en) * 1979-05-24 1982-04-06 Hiroshi Odanaka Process for the production of alkylene glycols
US4233221A (en) * 1979-10-24 1980-11-11 The Dow Chemical Company Ethylene carbonate process
US4437939A (en) * 1981-07-17 1984-03-20 The Halcon Sd Group, Inc. Process for separating ethylene oxide from aqueous solutions
AU558415B2 (en) * 1981-12-02 1987-01-29 Scientific Design Company, Inc. Preparation of alkylene carbonates

Also Published As

Publication number Publication date
SE459089B (sv) 1989-06-05
RO88641A (ro) 1986-02-28
ES523213A0 (es) 1984-11-16
IT8348494A1 (it) 1984-12-13
DE3321448A1 (de) 1983-12-15
NO832140L (no) 1983-12-15
YU129483A (en) 1986-02-28
IN159399B (enExample) 1987-05-16
MX157512A (es) 1988-11-28
DE3321448C2 (enExample) 1988-04-21
JPS5921634A (ja) 1984-02-03
CA1219602A (en) 1987-03-24
NL8302020A (nl) 1984-01-02
NO159164C (no) 1988-12-07
FR2528417A1 (fr) 1983-12-16
KR840005062A (ko) 1984-11-03
JPS6327333B2 (enExample) 1988-06-02
GB2122614B (en) 1986-03-19
DD210026A5 (de) 1984-05-30
US4400559A (en) 1983-08-23
YU44436B (en) 1990-08-31
IT1169063B (it) 1987-05-27
CH656871A5 (fr) 1986-07-31
EG16051A (en) 1990-10-30
BR8303125A (pt) 1984-01-31
ZA834364B (en) 1985-02-27
GB2122614A (en) 1984-01-18
AU556132B2 (en) 1986-10-23
SE8303324D0 (sv) 1983-06-13
KR870000542B1 (ko) 1987-03-18
GB8316153D0 (en) 1983-07-20
IT8348494A0 (it) 1983-06-13
SE8303324L (sv) 1983-12-15
SU1572414A3 (ru) 1990-06-15
ES8501357A1 (es) 1984-11-16
AR241527A1 (es) 1992-08-31
NO159164B (no) 1988-08-29
BE897039A (fr) 1983-12-13
AU1564083A (en) 1983-12-22

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