FR2528417B1 - Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse - Google Patents

Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse

Info

Publication number
FR2528417B1
FR2528417B1 FR8309765A FR8309765A FR2528417B1 FR 2528417 B1 FR2528417 B1 FR 2528417B1 FR 8309765 A FR8309765 A FR 8309765A FR 8309765 A FR8309765 A FR 8309765A FR 2528417 B1 FR2528417 B1 FR 2528417B1
Authority
FR
France
Prior art keywords
ethylene
hydrolysis
glycol
extraction
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
FR8309765A
Other languages
English (en)
French (fr)
Other versions
FR2528417A1 (fr
Inventor
Vijay Sharatchandra Bhise
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Halcon SD Group Inc
Original Assignee
Halcon SD Group Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Halcon SD Group Inc filed Critical Halcon SD Group Inc
Publication of FR2528417A1 publication Critical patent/FR2528417A1/fr
Application granted granted Critical
Publication of FR2528417B1 publication Critical patent/FR2528417B1/fr
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/12—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of mineral acids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)
FR8309765A 1982-06-14 1983-06-13 Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse Expired FR2528417B1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/388,395 US4400559A (en) 1982-06-14 1982-06-14 Process for preparing ethylene glycol

Publications (2)

Publication Number Publication Date
FR2528417A1 FR2528417A1 (fr) 1983-12-16
FR2528417B1 true FR2528417B1 (fr) 1986-01-17

Family

ID=23533945

Family Applications (1)

Application Number Title Priority Date Filing Date
FR8309765A Expired FR2528417B1 (fr) 1982-06-14 1983-06-13 Procede de preparation de l'ethylene-glycol a partir d'une solution aqueuse d'oxyde d'ethylene, par extraction par du dioxyde de carbone et hydrolyse

Country Status (25)

Country Link
US (1) US4400559A (enExample)
JP (1) JPS5921634A (enExample)
KR (1) KR870000542B1 (enExample)
AR (1) AR241527A1 (enExample)
AU (1) AU556132B2 (enExample)
BE (1) BE897039A (enExample)
BR (1) BR8303125A (enExample)
CA (1) CA1219602A (enExample)
CH (1) CH656871A5 (enExample)
DD (1) DD210026A5 (enExample)
DE (1) DE3321448A1 (enExample)
EG (1) EG16051A (enExample)
ES (1) ES8501357A1 (enExample)
FR (1) FR2528417B1 (enExample)
GB (1) GB2122614B (enExample)
IN (1) IN159399B (enExample)
IT (1) IT1169063B (enExample)
MX (1) MX157512A (enExample)
NL (1) NL8302020A (enExample)
NO (1) NO159164C (enExample)
RO (1) RO88641A (enExample)
SE (1) SE459089B (enExample)
SU (1) SU1572414A3 (enExample)
YU (1) YU44436B (enExample)
ZA (1) ZA834364B (enExample)

Families Citing this family (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4508927A (en) * 1983-08-02 1985-04-02 The Halcon Sd Group, Inc. Preparation of glycols from ethylene oxide
US4519875A (en) * 1984-05-09 1985-05-28 The Halcon Sd Group, Inc. Purification of ethylene glycol derived from ethylene carbonate
EP0385631A1 (en) * 1989-02-21 1990-09-05 ARCO Chemical Technology, L.P. Oxidation process
US5133859A (en) * 1990-03-02 1992-07-28 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5094741A (en) * 1990-03-02 1992-03-10 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5240603A (en) * 1990-03-02 1993-08-31 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
US5322626A (en) * 1990-03-02 1994-06-21 Hewlett-Packard Company Decoupled flow and pressure setpoints in an extraction instrument using compressible fluids
GB9005814D0 (en) * 1990-03-15 1990-05-09 Shell Int Research A two-step monoethylene glycol preparation process
JPH04301463A (ja) * 1991-03-29 1992-10-26 Sharp Corp 印字装置
JPH0539952U (ja) * 1991-10-29 1993-05-28 三洋電機株式会社 プリンター装置
US5932101A (en) * 1996-08-29 1999-08-03 Eastman Chemical Company Process for fluid/dense gas extraction under enhanced solubility conditions
AU749910B2 (en) * 1998-03-19 2002-07-04 Mitsubishi Chemical Corporation Method for producing monoethylene glycol
RU2137748C1 (ru) * 1998-11-16 1999-09-20 Открытое акционерное общество "Нижнекамскнефтехим" Способ получения концентрированного водного раствора моноэтиленгликоля
US6372925B1 (en) 2000-06-09 2002-04-16 Shell Oil Company Process for operating the epoxidation of ethylene
DE60332457D1 (de) * 2002-06-28 2010-06-17 Shell Int Research Verfahren zur verbesserung der selektivität eines katalysators und verfahren zum epoxidieren eines olefins
JP4333153B2 (ja) * 2003-02-07 2009-09-16 三菱化学株式会社 アルキレングリコールの製造方法
WO2004069777A1 (ja) * 2003-02-07 2004-08-19 Mitsubishi Chemical Corporation アルキレン誘導体の製造方法及びアルキレン誘導体製造用触媒の再生方法
US20040220433A1 (en) * 2003-03-28 2004-11-04 Evert Van Der Heide Process for the preparation of propylene glycol
US7348444B2 (en) * 2003-04-07 2008-03-25 Shell Oil Company Process for the production of an olefin oxide
EP1622857B1 (en) * 2003-04-09 2011-10-05 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkanediol
US8148555B2 (en) * 2003-06-26 2012-04-03 Shell Oil Company Method for improving the selectivity of a catalyst and a process for the epoxidation of an olefin
EP1658279B1 (en) * 2003-06-30 2007-11-14 Shell Internationale Researchmaatschappij B.V. Process for the preparation of propylene carbonate
US7378540B2 (en) * 2005-10-21 2008-05-27 Catalytic Distillation Technologies Process for producing organic carbonates
EP1979092A2 (en) * 2006-02-03 2008-10-15 Shell Internationale Research Maatschappij B.V. A process for treating a catalyst, the catalyst, and use of the catalyst
TWI387584B (zh) * 2006-03-13 2013-03-01 Shell Int Research 碳酸伸烷酯之生產方法及由此生產之碳酸伸烷酯於烷二醇及碳酸二烷酯之製造中之用途
DE602007004985D1 (de) * 2006-06-13 2010-04-08 Shell Int Research Glycoltrennung und- aufreinigung
CN100586913C (zh) * 2006-08-10 2010-02-03 中国石化扬子石油化工有限公司 催化水合法制备乙二醇的方法
TWI446964B (zh) 2007-05-09 2014-08-01 Shell Int Research 環氧化催化劑，製備該催化劑之方法及製備烯烴氧化物、１，２-二醇、１，２-二醇醚、１，２-碳酸酯或烷醇胺之方法
BRPI0815487B1 (pt) * 2007-08-14 2017-09-12 Shell Internationale Research Maatschappij B.V. Method for preparing an alkylene glycol from an alken.
US8378154B2 (en) * 2008-04-09 2013-02-19 Shell Oil Company Process for the preparation of alkylene glycol
US8110712B2 (en) * 2008-04-10 2012-02-07 Shell Oil Company Process for the preparation of alkylene glycol
JP6099307B2 (ja) * 2008-05-07 2017-03-22 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー エポキシ化工程の始動方法、エチレンオキシド、１，２−ジオール、１，２−ジオールエーテル、１，２−カーボネートまたはアルカノールアミンの製造方法
CA2723592C (en) * 2008-05-07 2016-08-16 Shell Internationale Research Maatschappij B.V. A process for the production of an olefin oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine
WO2009140318A1 (en) * 2008-05-15 2009-11-19 Shell Oil Company Process for the preparation of an alkylene carbonate and an alkylene glycol
EP2285795B1 (en) 2008-05-15 2017-03-22 Shell Internationale Research Maatschappij B.V. Process for the preparation of alkylene carbonate and/or alkylene glycol
JP5511979B2 (ja) * 2010-06-07 2014-06-04 中国科学院過程工程研究所 イオン液体触媒によるエチレングリコールの製造方法
US8802900B2 (en) * 2010-11-29 2014-08-12 Shell Oil Company Process for the preparation of ethylene glycol
BR112013027585B1 (pt) * 2011-04-29 2020-09-29 Shell Internationale Research Maatschappij B.V Método para melhorar a seletividade de um catalisador de alta seletividade suportado usado na epoxidação de etileno e método para preparar um 1,2-diol, um 1,2-diol éter, um 1,2-carbonato ou uma alcanolamina
WO2013028039A2 (ko) * 2011-08-24 2013-02-28 롯데케미칼 주식회사 알킬렌 카보네이트 및/또는 알킬렌 글리콜 합성용 촉매의 재생 방법 및 알킬렌 카보네이트 및/또는 알킬렌 글리콜의 제조 방법
CN107915577B (zh) * 2016-10-08 2020-12-29 中国石油化工股份有限公司 碳酸乙烯酯水解合成乙二醇的方法
WO2018102377A1 (en) 2016-12-02 2018-06-07 Shell Oil Company Methods for conditioning an ethylene epoxidation catalyst and associated methods for the production of ethylene oxide
KR102613266B1 (ko) * 2017-05-19 2023-12-14 쉘 인터내셔날 리써취 마트샤피지 비.브이. 에틸렌 카르보네이트 및 에틸렌 글리콜의 제조 방법에서의 열 통합
BR112021009797B1 (pt) 2018-12-10 2024-03-12 Shell Internationale Research Maatschappij B.V Processo para a preparação de etilenoglicol a partir de etileno
KR20220123230A (ko) * 2020-01-09 2022-09-06 쉘 인터내셔날 리써취 마트샤피지 비.브이. 에틸렌 글리콜의 제조 방법
WO2024137896A1 (en) * 2022-12-21 2024-06-27 Renewco2 Inc. Liquid electrolyzer for single-conversion-step electrocatalytic reduction of co2 to ethylene glycol

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4117250A (en) * 1977-12-22 1978-09-26 Union Carbide Corporation Continuous process for producing alkylene glycols from alkylene carbonates
US4237324A (en) * 1979-01-22 1980-12-02 The Dow Chemical Company Production of monoglycols from alkylene carbonates
CA1121389A (en) * 1979-05-24 1982-04-06 Hiroshi Odanaka Process for the production of alkylene glycols
US4233221A (en) * 1979-10-24 1980-11-11 The Dow Chemical Company Ethylene carbonate process
US4437939A (en) * 1981-07-17 1984-03-20 The Halcon Sd Group, Inc. Process for separating ethylene oxide from aqueous solutions
IN159117B (enExample) * 1981-12-02 1987-03-28 Halcon Sd Group Inc

Also Published As

Publication number Publication date
YU44436B (en) 1990-08-31
SE8303324L (sv) 1983-12-15
DE3321448C2 (enExample) 1988-04-21
FR2528417A1 (fr) 1983-12-16
YU129483A (en) 1986-02-28
DD210026A5 (de) 1984-05-30
ES523213A0 (es) 1984-11-16
BE897039A (fr) 1983-12-13
NO159164B (no) 1988-08-29
GB2122614A (en) 1984-01-18
NO159164C (no) 1988-12-07
IN159399B (enExample) 1987-05-16
IT8348494A0 (it) 1983-06-13
RO88641A (ro) 1986-02-28
CH656871A5 (fr) 1986-07-31
EG16051A (en) 1990-10-30
AU556132B2 (en) 1986-10-23
GB8316153D0 (en) 1983-07-20
JPS5921634A (ja) 1984-02-03
SU1572414A3 (ru) 1990-06-15
ES8501357A1 (es) 1984-11-16
AR241527A1 (es) 1992-08-31
KR870000542B1 (ko) 1987-03-18
JPS6327333B2 (enExample) 1988-06-02
IT1169063B (it) 1987-05-27
MX157512A (es) 1988-11-28
BR8303125A (pt) 1984-01-31
GB2122614B (en) 1986-03-19
DE3321448A1 (de) 1983-12-15
SE8303324D0 (sv) 1983-06-13
NL8302020A (nl) 1984-01-02
ZA834364B (en) 1985-02-27
US4400559A (en) 1983-08-23
SE459089B (sv) 1989-06-05
IT8348494A1 (it) 1984-12-13
KR840005062A (ko) 1984-11-03
NO832140L (no) 1983-12-15
CA1219602A (en) 1987-03-24
AU1564083A (en) 1983-12-22

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