FR2464745A1 - Regeneration des catalyseurs de reconversion chimique utilises dans un procede cyclique de fabrication du peroxyde d'hydrogene - Google Patents
Regeneration des catalyseurs de reconversion chimique utilises dans un procede cyclique de fabrication du peroxyde d'hydrogene Download PDFInfo
- Publication number
- FR2464745A1 FR2464745A1 FR7922266A FR7922266A FR2464745A1 FR 2464745 A1 FR2464745 A1 FR 2464745A1 FR 7922266 A FR7922266 A FR 7922266A FR 7922266 A FR7922266 A FR 7922266A FR 2464745 A1 FR2464745 A1 FR 2464745A1
- Authority
- FR
- France
- Prior art keywords
- catalyst
- regeneration
- reconversion
- catalysts
- regenerated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003054 catalyst Substances 0.000 title claims abstract description 81
- 230000008929 regeneration Effects 0.000 title claims abstract description 28
- 238000011069 regeneration method Methods 0.000 title claims abstract description 28
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 239000000126 substance Substances 0.000 title claims description 5
- 238000004519 manufacturing process Methods 0.000 title abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 34
- 230000008569 process Effects 0.000 claims abstract description 28
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 230000000750 progressive effect Effects 0.000 claims abstract description 4
- 230000001590 oxidative effect Effects 0.000 claims abstract description 3
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000003517 fume Substances 0.000 claims description 5
- 229910000503 Na-aluminosilicate Inorganic materials 0.000 claims description 3
- 125000004122 cyclic group Chemical group 0.000 claims description 3
- 235000012217 sodium aluminium silicate Nutrition 0.000 claims description 3
- 239000000429 sodium aluminium silicate Substances 0.000 claims description 3
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims 1
- 238000007669 thermal treatment Methods 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 abstract description 20
- 239000002699 waste material Substances 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 22
- 230000000694 effects Effects 0.000 description 10
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 150000004053 quinones Chemical class 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 230000004580 weight loss Effects 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 238000011144 upstream manufacturing Methods 0.000 description 4
- 150000004056 anthraquinones Chemical class 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 239000005416 organic matter Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 150000004763 sulfides Chemical class 0.000 description 3
- 239000012224 working solution Substances 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000000443 aerosol Substances 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- -1 hydrogen peroxide cation Chemical class 0.000 description 2
- 238000005984 hydrogenation reaction Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 150000001721 carbon Chemical class 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000005465 channeling Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 238000001784 detoxification Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000002440 industrial waste Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 238000003969 polarography Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000007420 reactivation Effects 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000011949 solid catalyst Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/20—Regeneration or reactivation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7922266A FR2464745A1 (fr) | 1979-09-06 | 1979-09-06 | Regeneration des catalyseurs de reconversion chimique utilises dans un procede cyclique de fabrication du peroxyde d'hydrogene |
| US06/176,643 US4351820A (en) | 1979-09-06 | 1980-08-11 | Regeneration of chemical reconversion catalysts used in a cyclic process for the production of hydrogen peroxide and apparatus therefor |
| IN583/DEL/80A IN154551B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1979-09-06 | 1980-08-11 | |
| JP11602580A JPS5670834A (en) | 1979-09-06 | 1980-08-25 | Method and device for regenerating catalyst |
| BR8005475A BR8005475A (pt) | 1979-09-06 | 1980-08-28 | Processo de regeneracao dos catalisadores de reconversao quimica utilizados em um processo ciclico de fabricacao de peroxido de hidrogenio e aparelho para a pratica do processo |
| DE8080401260T DE3065891D1 (en) | 1979-09-06 | 1980-09-04 | Reactivation of chemical reconversion catalysts used in a cyclic production process of hydrogen peroxide, and use of an apparatus for putting it into practice |
| EP80401260A EP0025746B1 (fr) | 1979-09-06 | 1980-09-04 | Régénération des catalyseurs de reconversion chimique utilisés dans un procédé cyclique de fabrication du peroxyde d'hydrogène et utilisation d'un appareil pour la mise en oeuvre |
| FI802798A FI66541C (fi) | 1979-09-06 | 1980-09-05 | Foerfarande och anordning foer regenerering av kemiska konversionskatalysatorer anvaenda vid framstaellning av vaeteperoxid |
| ES494795A ES494795A0 (es) | 1979-09-06 | 1980-09-05 | Procedimiento y aparato de regeneracion de catalizadores de reconversion quimica. |
| YU2263/80A YU40781B (en) | 1979-09-06 | 1980-09-05 | Process for the regeneration of catalyst for chemical reconversion, used the cyclic process for hydrogen peroxide production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7922266A FR2464745A1 (fr) | 1979-09-06 | 1979-09-06 | Regeneration des catalyseurs de reconversion chimique utilises dans un procede cyclique de fabrication du peroxyde d'hydrogene |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2464745A1 true FR2464745A1 (fr) | 1981-03-20 |
| FR2464745B1 FR2464745B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1982-09-03 |
Family
ID=9229398
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7922266A Granted FR2464745A1 (fr) | 1979-09-06 | 1979-09-06 | Regeneration des catalyseurs de reconversion chimique utilises dans un procede cyclique de fabrication du peroxyde d'hydrogene |
Country Status (10)
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5336432A (en) * | 1992-01-24 | 1994-08-09 | John Petchul | Composition for microemulsion gel having bleaching and antiseptic properties |
| FI94515B (fi) * | 1994-03-04 | 1995-06-15 | Finnish Chemicals Oy | Menetelmä hydrauskatalyytin reaktivoimiseksi |
| FI98509C (fi) * | 1994-05-20 | 1997-07-10 | Kemira Chemicals Oy | Menetelmä epäpuhtaan alumiinioksidin puhdistamiseksi lämpökäsittelemällä |
| DE19507219C1 (de) * | 1995-03-02 | 1996-05-15 | Daimler Benz Ag | Verfahren und Vorrichtung zum Nachbeschichten einer deaktivierten Katalysatorbeschichtung bei einem Katalysator |
| WO1997047706A1 (de) * | 1996-06-13 | 1997-12-18 | Siemens Aktiengesellschaft | Anlage zur thermischen entsorgung von abfall |
| JP4516091B2 (ja) * | 2007-04-23 | 2010-08-04 | 株式会社東芝 | ナノカーボン生成装置 |
| CN101376099B (zh) * | 2007-08-29 | 2010-12-15 | 上海华明高技术（集团）有限公司 | 过氧化氢工作液再生过程用的活性氧化铝再生处理方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1340901A (fr) * | 1962-09-10 | 1963-10-25 | Oxysynthese | Réactivation des catalyseurs de reconversion utilisés dans un procédé de fabrication cyclique de l'eau oxygénée |
| US3424696A (en) * | 1964-12-30 | 1969-01-28 | Oxysynthese | Method for regenerating catalysts used for reconverting worn solutions in the cyclic method of manufacture of hydrogen peroxide |
| FR2195590A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1972-08-09 | 1974-03-08 | Fmc Corp |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1047259A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | ||||
| LU69405A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1974-02-18 | 1975-12-09 | ||
| DK21475A (da) * | 1975-01-23 | 1976-07-24 | Dansk Leca As | Roterovn til fremstilling af et opbleret lerprodukt samt fremgangsmade til fremstilling af roterovnen |
-
1979
- 1979-09-06 FR FR7922266A patent/FR2464745A1/fr active Granted
-
1980
- 1980-08-11 IN IN583/DEL/80A patent/IN154551B/en unknown
- 1980-08-11 US US06/176,643 patent/US4351820A/en not_active Expired - Lifetime
- 1980-08-25 JP JP11602580A patent/JPS5670834A/ja active Granted
- 1980-08-28 BR BR8005475A patent/BR8005475A/pt unknown
- 1980-09-04 DE DE8080401260T patent/DE3065891D1/de not_active Expired
- 1980-09-04 EP EP80401260A patent/EP0025746B1/fr not_active Expired
- 1980-09-05 ES ES494795A patent/ES494795A0/es active Granted
- 1980-09-05 FI FI802798A patent/FI66541C/fi not_active IP Right Cessation
- 1980-09-05 YU YU2263/80A patent/YU40781B/xx unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1340901A (fr) * | 1962-09-10 | 1963-10-25 | Oxysynthese | Réactivation des catalyseurs de reconversion utilisés dans un procédé de fabrication cyclique de l'eau oxygénée |
| US3424696A (en) * | 1964-12-30 | 1969-01-28 | Oxysynthese | Method for regenerating catalysts used for reconverting worn solutions in the cyclic method of manufacture of hydrogen peroxide |
| FR2195590A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1972-08-09 | 1974-03-08 | Fmc Corp |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0025746A1 (fr) | 1981-03-25 |
| BR8005475A (pt) | 1981-03-24 |
| ES8107121A1 (es) | 1981-08-16 |
| FI66541C (fi) | 1984-11-12 |
| YU40781B (en) | 1986-06-30 |
| IN154551B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1984-11-10 |
| FI66541B (fi) | 1984-07-31 |
| EP0025746B1 (fr) | 1983-12-14 |
| US4351820A (en) | 1982-09-28 |
| JPS635137B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-02-02 |
| DE3065891D1 (en) | 1984-01-19 |
| YU226380A (en) | 1983-04-30 |
| FI802798A7 (fi) | 1981-03-07 |
| JPS5670834A (en) | 1981-06-13 |
| FR2464745B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1982-09-03 |
| ES494795A0 (es) | 1981-08-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |