FR2439747A1 - Procede de preparation d'alumine spherique a partir de gibbsite - Google Patents

Procede de preparation d'alumine spherique a partir de gibbsite

Info

Publication number
FR2439747A1
FR2439747A1 FR7926381A FR7926381A FR2439747A1 FR 2439747 A1 FR2439747 A1 FR 2439747A1 FR 7926381 A FR7926381 A FR 7926381A FR 7926381 A FR7926381 A FR 7926381A FR 2439747 A1 FR2439747 A1 FR 2439747A1
Authority
FR
France
Prior art keywords
aluminum
weight
gibbsite
aluminum chloride
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7926381A
Other languages
English (en)
Other versions
FR2439747B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nikki Universal Co Ltd
Original Assignee
Nikki Universal Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nikki Universal Co Ltd filed Critical Nikki Universal Co Ltd
Publication of FR2439747A1 publication Critical patent/FR2439747A1/fr
Application granted granted Critical
Publication of FR2439747B1 publication Critical patent/FR2439747B1/fr
Granted legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/50Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/51Spheres
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/06Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a liquid medium
    • B01J2/08Gelation of a colloidal solution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00Compounds of aluminium
    • C01F7/02Aluminium oxide; Aluminium hydroxide; Aluminates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00Compounds of aluminium
    • C01F7/02Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/20Preparation of aluminium oxide or hydroxide from aluminous ores using acids or salts
    • C01F7/22Preparation of aluminium oxide or hydroxide from aluminous ores using acids or salts with halides or halogen acids
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/10Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/32Spheres
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/11Powder tap density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Structural Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Catalysts (AREA)

Abstract

L'INVENTION CONCERNE UN PROCEDE DE PRODUCTION D'ALUMINE SPHERIQUE QUI CONSISTE A PREPARER UNE SOLUTION BASIQUE DE CHLORURE D'ALUMINIUM AYANT UNE CONCENTRATION EN ALUMINIUM DE 7 A 12 EN POIDS ET UN RAPPORT PONDERAL ALUMINIUMCHLORURE DE 0,3 A 0,8 EN FAISANT REAGIR DE LA GIBBSITE AVEC UNE SOLUTION AQUEUSE D'ACIDE CHLORHYDRIQUE A TEMPERATURE ELEVEE, A PREPARER UN HYDROSOL D'ALUMINIUM AYANT UNE CONCENTRATION EN ALUMINIUM DE 9 A 15 EN POIDS, ET UN RAPPORT PONDERAL ALUMINIUMCHLORURE DE L'ORDRE DE 0,8 A 1,5, EN FAISANT REAGIR LA SOLUTION AINSI PREPAREE AVEC DE L'ALUMINIUM METALLIQUE A UNE TEMPERATURE ELEVEE, A MELANGER CET HYDROSOL AVEC UN AGENT GELIFIANT, A DISPERSER LE MELANGE RESULTANT SOUS LA FORME DE GOUTTELETTES DANS UN MILIEU DE SUSPENSION AFIN DE FORMER DES PARTICULES D'HYDROGEL, A VIEILLIR LES PARTICULES AINSI OBTENUES DANS LE MILIEU DE SUSPENSION, PUIS DANS LE L'AMMONIAC AQUEUX, A LAVER A L'EAU, SECHER ET CALCINER. L'ALUMINE SPHERIQUE AINSI OBTENUE EST PRATIQUEMENT EXEMPTE DE SODIUM, MALGRE L'EMPLOI DE GIBBSITE COMME MATIERE PREMIERE.
FR7926381A 1978-10-26 1979-10-24 Procede de preparation d'alumine spherique a partir de gibbsite Granted FR2439747A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP13177978A JPS5560022A (en) 1978-10-26 1978-10-26 Production of spherical alumina

Publications (2)

Publication Number Publication Date
FR2439747A1 true FR2439747A1 (fr) 1980-05-23
FR2439747B1 FR2439747B1 (fr) 1982-10-29

Family

ID=15065946

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7926381A Granted FR2439747A1 (fr) 1978-10-26 1979-10-24 Procede de preparation d'alumine spherique a partir de gibbsite

Country Status (6)

Country Link
US (1) US4309312A (fr)
JP (1) JPS5560022A (fr)
DE (1) DE2942768C2 (fr)
FR (1) FR2439747A1 (fr)
GB (1) GB2035280B (fr)
IT (1) IT1121490B (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2491053A1 (fr) * 1980-09-29 1982-04-02 Nikki Universal Co Ltd Procede de fabrication d'alumine spherique a partir de gibbsite

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3212249C2 (de) * 1982-04-02 1986-08-21 Condea Chemie GmbH, 2212 Brunsbüttel Verfahren zur Herstellung von kugelförmiger Tonerde
US4837069A (en) * 1987-01-07 1989-06-06 Minnesota Mining And Manufacturing Company Transparent alumina microspheres
DE4042594A1 (de) * 1990-11-05 1992-07-02 Nukem Gmbh Verfahren zur herstellung von aluminiumoxidkugeln
DE4035089C1 (en) * 1990-11-05 1992-04-23 Degussa Ag, 6000 Frankfurt, De Aluminium oxide spheres for adsorbent, chromatography, catalyst etc. - with defined surface area, density, pore vol, breaking strength and narrow particles size distribution etc.
JPH1017321A (ja) * 1996-06-27 1998-01-20 Catalysts & Chem Ind Co Ltd アルミナ小球体およびその製造方法
KR100387218B1 (ko) * 1996-12-20 2003-10-04 주식회사 효성 알루미나 촉매지지체의 기공량 증진방법
CN103204526B (zh) * 2012-01-15 2016-02-17 晟通科技集团有限公司 一种制备氧化铝溶胶的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2620314A (en) * 1950-03-08 1952-12-02 Universal Oil Prod Co Spheroidal alumina
LU67121A1 (fr) * 1972-03-01 1973-05-03
DE2504463A1 (de) * 1975-02-04 1976-08-05 Kali Chemie Ag Verfahren zur herstellung von kugelfoermigen tonerdehaltigen teilchen
US4032472A (en) * 1976-01-07 1977-06-28 Uop Inc. Manufacture of alumina sol

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RO63835A (fr) * 1972-03-01 1979-08-15 Procede pour la preparation du chlorure d'aluminium basique
JPS5311796B2 (fr) * 1972-08-31 1978-04-24
US3979334A (en) * 1975-04-16 1976-09-07 Universal Oil Products Company Manufacture of spheroidal alumina particles
JPS53104597A (en) * 1977-02-25 1978-09-11 Nitsuki Yunibaasaru Kk Method of making spherical alumina

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2620314A (en) * 1950-03-08 1952-12-02 Universal Oil Prod Co Spheroidal alumina
LU67121A1 (fr) * 1972-03-01 1973-05-03
DE2504463A1 (de) * 1975-02-04 1976-08-05 Kali Chemie Ag Verfahren zur herstellung von kugelfoermigen tonerdehaltigen teilchen
US4032472A (en) * 1976-01-07 1977-06-28 Uop Inc. Manufacture of alumina sol

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2491053A1 (fr) * 1980-09-29 1982-04-02 Nikki Universal Co Ltd Procede de fabrication d'alumine spherique a partir de gibbsite

Also Published As

Publication number Publication date
GB2035280A (en) 1980-06-18
JPS5560022A (en) 1980-05-06
DE2942768A1 (de) 1980-05-08
DE2942768C2 (de) 1986-05-07
FR2439747B1 (fr) 1982-10-29
JPS627125B2 (fr) 1987-02-16
GB2035280B (en) 1982-09-29
IT1121490B (it) 1986-04-02
IT7969053A0 (it) 1979-10-22
US4309312A (en) 1982-01-05

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Legal Events

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