FR2405930A1 - Procede de preparation de nitroguanidine - Google Patents

Procede de preparation de nitroguanidine

Info

Publication number
FR2405930A1
FR2405930A1 FR7829460A FR7829460A FR2405930A1 FR 2405930 A1 FR2405930 A1 FR 2405930A1 FR 7829460 A FR7829460 A FR 7829460A FR 7829460 A FR7829460 A FR 7829460A FR 2405930 A1 FR2405930 A1 FR 2405930A1
Authority
FR
France
Prior art keywords
nitroguanidine
acid
water
preparing
explosives
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7829460A
Other languages
English (en)
Other versions
FR2405930B1 (fr
Inventor
Matthias Thoma
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nigu Chemie GmbH
Original Assignee
Nigu Chemie GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nigu Chemie GmbH filed Critical Nigu Chemie GmbH
Publication of FR2405930A1 publication Critical patent/FR2405930A1/fr
Application granted granted Critical
Publication of FR2405930B1 publication Critical patent/FR2405930B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C277/00—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
    • C07C277/08—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00—Compositions containing a nitrated organic compound
    • C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention concerne un procédé de préparation de nitroguanidine. Procédé caractérisé en ce qu'on utilise comme déshydratant l'acide nitrique à une concentration de 92 à 100 %, à raison de 2,5 à 5 moles par mole de nitrate de guanidine, en ce qu'on conduit la déshydratation pendant une heure trente à cinq heures entre 25 et 80 degrés C, en ce qu'on précipite la nitroguanidine formée en ajoutant de l'eau froide, et en ce qu'on la lave à l'eau pour éliminer l'acide. L'invention est plus particulièrement applicable dans le domaine de la fabrication de constituants de propergols et d'explosifs.
FR7829460A 1977-10-12 1978-10-09 Procede de preparation de nitroguanidine Granted FR2405930A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19772745774 DE2745774A1 (de) 1977-10-12 1977-10-12 Verfahren zur herstellung von nitroguanidin

Publications (2)

Publication Number Publication Date
FR2405930A1 true FR2405930A1 (fr) 1979-05-11
FR2405930B1 FR2405930B1 (fr) 1984-08-31

Family

ID=6021210

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7829460A Granted FR2405930A1 (fr) 1977-10-12 1978-10-09 Procede de preparation de nitroguanidine

Country Status (5)

Country Link
DE (1) DE2745774A1 (fr)
FR (1) FR2405930A1 (fr)
GB (1) GB2006201B (fr)
IT (1) IT1099364B (fr)
ZA (1) ZA785678B (fr)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19947332A1 (de) * 1999-10-01 2001-04-05 Nigu Chemie Gmbh Verfahren zur Herstellung von 3-Alkyl-N-nitro-4H-1,3,5-oxadiazin-3-iminen
EP1257529A2 (fr) * 1999-12-20 2002-11-20 Dynamit Nobel GmbH Explosivstoff- und Systemtechnik Procede pour la production de nitroguanidine
CN101497579B (zh) * 2009-03-26 2012-05-23 里程 一种生产硝基胍的工艺
CN102827038B (zh) * 2012-08-28 2014-02-05 西安近代化学研究所 一种硝基胍制备工艺
CN103787922B (zh) * 2014-03-04 2016-06-01 新昌县鸿吉电子科技有限公司 一种合成硝基取代化合物的工业催化方法
CN107721884B (zh) * 2017-11-06 2020-05-05 西安近代化学研究所 一种硝基胍工程化生产工艺
CN110204461B (zh) * 2019-05-15 2022-04-05 西安万德能源化学股份有限公司 一种硝基胍晶体及硝基胍的微通道结晶工艺和装置

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2878290A (en) * 1956-07-23 1959-03-17 American Cyanamid Co Nitroguanidine preparation

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2878290A (en) * 1956-07-23 1959-03-17 American Cyanamid Co Nitroguanidine preparation

Also Published As

Publication number Publication date
DE2745774A1 (de) 1979-04-19
GB2006201A (en) 1979-05-02
FR2405930B1 (fr) 1984-08-31
IT1099364B (it) 1985-09-18
ZA785678B (en) 1979-10-31
GB2006201B (en) 1982-02-24
IT7828659A0 (it) 1978-10-11

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Legal Events

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ST Notification of lapse