FI96181B - Förfarande för produktion av syre genom att separera genom adsorption från luft - Google Patents

Förfarande för produktion av syre genom att separera genom adsorption från luft Download PDF

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Publication number
FI96181B
FI96181B FI915172A FI915172A FI96181B FI 96181 B FI96181 B FI 96181B FI 915172 A FI915172 A FI 915172A FI 915172 A FI915172 A FI 915172A FI 96181 B FI96181 B FI 96181B
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FI
Finland
Prior art keywords
pressure
oxygen
cycle
adsorption device
downstream
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Application number
FI915172A
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English (en)
Finnish (fi)
Other versions
FI96181C (sv
FI915172A0 (sv
Inventor
Sylvie Eteve
L On Hay
Thomas Rottner
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Air Liquide
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Application filed by Air Liquide filed Critical Air Liquide
Publication of FI915172A0 publication Critical patent/FI915172A0/sv
Application granted granted Critical
Publication of FI96181B publication Critical patent/FI96181B/sv
Publication of FI96181C publication Critical patent/FI96181C/sv

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0476—Vacuum pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/116—Molecular sieves other than zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/12—Oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/102—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40013—Pressurization
    • B01D2259/40015—Pressurization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40013—Pressurization
    • B01D2259/40018—Pressurization with more than three sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/4002—Production
    • B01D2259/40022—Production with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028—Depressurization
    • B01D2259/4003—Depressurization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028—Depressurization
    • B01D2259/40032—Depressurization with three sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B01D2259/40037—Equalization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40043—Purging
    • B01D2259/4005—Nature of purge gas
    • B01D2259/40052—Recycled product or process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40067—Seven
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40073—Ten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40077—Direction of flow
    • B01D2259/40081—Counter-current
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/402—Further details for adsorption processes and devices using two beds

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)

Claims (14)

1. Förfarande för produktion av syre genom att separera det frän luft genom adsorption, vid vilket förfarande man använder sig av tvä adsorptionsanordningar 5 (1;2) samt syre (27) i en behällare och vid vilket förfarande man i bägge adsorp- tionsanordningama genomför en periodisk process ("cykel") som räcker tiden T, varvid dessa tvä cykler är förskjutna i förhällande tili varandra tiden T/2, och varvid de bägge tvä innefattar följande skeden: 10 a) ett första tryckhöjningsskede (A^) vid vilket man utgör frän det lägsta trycket i cykeln, vilket höjs tili det genomsnittliga trycket genom att leda producerat syre motströms; b) ett andra tryckhöjningsskede (Ag) utgäende frän nämnda genomsnittliga 15 tryck som höjs väsentligen tili det högsta trycket av cykeln genom att leda luft medströms, utan att avlägsna syre; c) ett produktionsskede (B^Bg) genom att leda luft och avlägsna syre medströms; 20 d) ett skede där syre avlägsnas (Bg) genom att sänka trycket delvis med-ströms, varvid man avbrutit luftströmmen; e) ett desorptionsskede (C^Cg) genom att sänka trycket motströms tili det 25 lägsta trycket av cykeln som är lägre än atmosfärstrycket, kännetecknat därav, att i skede a) härrör syret som används för tiyck-höjningen frän syrebehällaren samt frän den andra adsorptionsanordningen i skede d). 30
2. Förfarande enligt patentkrav 1, kännetecknat därav, att under hela skede a) leder man dit samtidigt syre bäde frän behällaren (27) och frän den 15 96181 andra adsorptionsanordningen.
3. Förfarande enligt patentkrav 1, kännetecknat därav, att skede a) innefattar ett preliminärt delskede (Α’^,Α^) där tiycket höjs med syre som 5 härrör frän den andra adsorptionsanordningen, samt ett slutgiltigt delskede (A^2»A’-j2)’ där trycket höjs med syre frän syrebehällaren (27).
4. Förfarande enligt patentkrav 3, kännetecknat därav, att under det slutgiltiga delskedet (A12) där trycket höjs leder man dit ocksä luft medströms. 10
5. Förfarande enligt patentkrav 3, kännetecknat därav, att under det slutgiltiga delskedet (A’^2) där trycket höjs leder man dit ocksä syre medströms som härrör frän den andra adsorptionsanordningen i skede d). 15
6. Förfarande enligt nägot av patentkraven 1-5, kännetecknat därav, att i slutet av skede a) är det genomsnittliga trycket väsentligen lika högt som i slutet av skede d).
7. Förfarande enligt patentkrav 6, kännetecknat därav, att nämnda 20 genomsnittliga tryck är lika högt som eller högre än 1 x 10^ Pa.
« : 8. Förfarande enligt nägot av ovanstäende patentkrav, kännetecknat därav, att tiycket som räder i skede c) hälls väsentligen isobariskt vid det högsta trycket av cykeln. 25
9. Förfarande enligt nägot av ovanstäende patentkrav, kännetecknat därav, att det innefattar ett elueringsskede (Cg) i slutet av skede c) som genom-förs genom pumpning, där trycker som räder hälls väsentligen isobariskt vid det * lägsta trycket av cykeln. 30
10. Förfarande enligt patentkrav 9, kännetecknat därav, att i slutet av elueringsskedet (Cg) leder man dit motströms producerat syre, som erhälls frän 96181 16 slutet (Bg) av produktionsskedet av den andra absorptionsanordningen.
11. Förfarande enligt patentkrav 10, kännetecknat därav, att i slutet (Bg) av produktionsskedet leds en del av det producerade syret samtidigt till 5 behällaren (27).
12. Förfarande enligt nägot av ovanstäende patentkrav, kännetecknat därav, att cykelns högsta tryck är inom omrädet 1,2-2 x 10® Pa. 10
13. Förfarande enligt nägot av ovanstäende patentkrav, kännetecknat därav, att cykelns lägsta tryck är inom omrädet 0,3-0,7 x 10® Pa. 15 «
FI915172A 1990-03-02 1991-11-01 Förfarande för produktion av syre genom att separera genom adsorption från luft FI96181C (sv)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
FR9002617 1990-03-02
FR9002617 1990-03-02
FR9100164 1991-03-01
PCT/FR1991/000164 WO1991012874A1 (fr) 1990-03-02 1991-03-01 Procede de production d'oxygene par separation d'air par adsorption

Publications (3)

Publication Number Publication Date
FI915172A0 FI915172A0 (sv) 1991-11-01
FI96181B true FI96181B (sv) 1996-02-15
FI96181C FI96181C (sv) 1996-05-27

Family

ID=9394307

Family Applications (1)

Application Number Title Priority Date Filing Date
FI915172A FI96181C (sv) 1990-03-02 1991-11-01 Förfarande för produktion av syre genom att separera genom adsorption från luft

Country Status (7)

Country Link
US (1) US5223004A (sv)
EP (1) EP0471064B1 (sv)
JP (1) JPH04505448A (sv)
CA (1) CA2054199A1 (sv)
ES (1) ES2089202T3 (sv)
FI (1) FI96181C (sv)
WO (1) WO1991012874A1 (sv)

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Also Published As

Publication number Publication date
CA2054199A1 (fr) 1991-09-03
FI96181C (sv) 1996-05-27
JPH04505448A (ja) 1992-09-24
US5223004A (en) 1993-06-29
ES2089202T3 (es) 1996-10-01
FI915172A0 (sv) 1991-11-01
EP0471064A1 (fr) 1992-02-19
WO1991012874A1 (fr) 1991-09-05
EP0471064B1 (fr) 1996-07-10

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