FI127163B - Valoherkiste - Google Patents

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Publication number
FI127163B
FI127163B FI20165867A FI20165867A FI127163B FI 127163 B FI127163 B FI 127163B FI 20165867 A FI20165867 A FI 20165867A FI 20165867 A FI20165867 A FI 20165867A FI 127163 B FI127163 B FI 127163B
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FI
Finland
Prior art keywords
phthalocyanine
formula
tetrakis
mixture
pyridyl
Prior art date
Application number
FI20165867A
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English (en)
Swedish (sv)
Other versions
FI20165867A (fi
Inventor
Alexander Efimov
Lijo George
Ville Santala
Original Assignee
Tty-Säätiö
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tty-Säätiö filed Critical Tty-Säätiö
Priority to FI20165867A priority Critical patent/FI127163B/fi
Priority to US16/349,893 priority patent/US10875871B2/en
Priority to CN201780071239.XA priority patent/CN109996801B/zh
Priority to PCT/FI2017/050775 priority patent/WO2018091774A1/en
Priority to RU2019115122A priority patent/RU2019115122A/ru
Priority to EP17871183.4A priority patent/EP3541818A4/en
Application granted granted Critical
Publication of FI127163B publication Critical patent/FI127163B/fi
Publication of FI20165867A publication Critical patent/FI20165867A/fi

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/22—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains four or more hetero rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
    • A01N25/10—Macromolecular compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
    • A61L2/02—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using physical phenomena
    • A61L2/08—Radiation
    • A61L2/088—Radiation using a photocatalyst or photosensitiser
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
    • A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
    • A61L2/23—Solid substances, e.g. granules, powders, blocks, tablets
    • A61L2/232—Solid substances, e.g. granules, powders, blocks, tablets layered or coated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/57—Nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/06—Zinc compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B47/00—Porphines; Azaporphines
    • C09B47/04—Phthalocyanines abbreviation: Pc
    • C09B47/06—Preparation from carboxylic acids or derivatives thereof, e.g. anhydrides, amides, mononitriles, phthalimide, o-cyanobenzamide
    • C09B47/067—Preparation from carboxylic acids or derivatives thereof, e.g. anhydrides, amides, mononitriles, phthalimide, o-cyanobenzamide from phthalodinitriles naphthalenedinitriles, aromatic dinitriles prepared in situ, hydrogenated phthalodinitrile
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B47/00—Porphines; Azaporphines
    • C09B47/04—Phthalocyanines abbreviation: Pc
    • C09B47/08—Preparation from other phthalocyanine compounds, e.g. cobaltphthalocyanineamine complex
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B47/00—Porphines; Azaporphines
    • C09B47/04—Phthalocyanines abbreviation: Pc
    • C09B47/30—Metal-free phthalocyanines

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Medicinal Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Toxicology (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catalysts (AREA)

Claims (11)

1. Ftalosyaniini, jolla on kaava I: Kaava I:
jossa M on metalli-ioni tai kaksi vetyatomia, ja jossa substituenttiparit R1 ja R1, R2 ja R4, R5 ja R6, sekä R7 ja R8, muista substituenttipareista riippumatta, ovat - vety ja - toinen substituentti on sama kaikissa substituenttipareissa ja on valittu seu-raavista:
jossa R9 on Ci-C-i8-alkyyli. 1 Patenttivaatimuksen 1 mukainen yhdiste, joka on valittu seuraavista: 2 - tetrakis[a-pyridyyli]ftalosyaniini, jolla on kaava II:
- tetrakis[a-pyridyyli]sinkkiftalosyaniini, jolla on kaava III:
- tetrakis[metyyli-a-pyridyylijodoniumsuola]ftalosyaniini, jolla on kaava IV:
tetrakis[metyyli-a-pyridyylijodoniumsuola]sinkkiftalosyaniini, jolla on kaava V:
3. Esine, joka on päällystetty tai kyllästetty jonkin edellisen patenttivaatimuksen mukaisella ftalosyaniinilla, joka esine on sopivimmin valittu seuraa-vista: esineet, jotka käsittävät kuitumateriaalia, kuten paperi, suodatin, tekstiili tai kangas; huokoinen materiaali; helmet, rakeet, mikrohiukkaset, nanohiuk-kaset; seinä: lasipinta; metallipinta; muovipinta; ja keraaminen pinta.
4. Menetelmä reaktiivisen happilajin aikaansaamiseksi, jossa menetelmässä - järjestetään saataville patenttivaatimuksen 1 tai 2 mukaista ftalosyaniinia tai patenttivaatimuksen 3 mukainen esine ja - säteilytetään ftalosyaniinia tai esinettä valolla reaktiivisen happilajin saamiseksi.
5. Menetelmä mikro-organismien inaktivoimiseksi, jossa menetelmässä järjestetään saataville reaktiivinen happilaji patenttivaatimuksen 4 mukaisella menetelmällä mikro-organismien inaktivoimiseksi hapettamalla. 6. 3-(pyridiini-4-yyli)bentseeni-1,2-dikarbonitriili.
7. Menetelmä 3-(pyridiini-4-yyli)bentseeni-1,2-dikarbonitriilin valmistamiseksi, jossa menetelmässä - järjestetään saataville seos, jossa on pyridiiniboronaattiesteriä, triflaatti-ftalonitriiliä, palladiumkatalyyttiä ja K3PC>4:a liuoksena, lämmitetään ja sekoitetaan, kuten 90-100°C:n lämpötilassa noin 1-3 tunnin ajan, ja - otetaan liuoksesta talteen 3-(pyridiini-4-yyli)bentseeni-1,2-dikarbonitriili.
8. Menetelmä kaavan II mukaisen tetrakis[a-pyridyyli]ftalosyaniinin valmistamiseksi, Kaava II:
jossa menetelmässä: - järjestetään saataville litiumia liuotettuna liuottimeen, sopivimmin 90-100°C:n lämpötilassa argonkaasussa, -jäähdytetään seos huoneenlämpötilaan, - lisätään 3-(pyridiini-4-yyli)bentseeni-1,2-dikarbonitriiliä, sopivimmin argonkaasussa, - annetaan reagoida lämmitettäessä, kuten noin 90-100°C:n lämpötilassa, sopivimmin samalla sekoittaen, ja - otetaan talteen saatu tetrakis[a-pyridyyli]ftalosyaniini, jolla on kaava II.
9. Patenttivaatimuksen 8 mukainen menetelmä, jossa -järjestetään saataville seos, jossa on saatu ftalosyaniini, jolla on kaava II, ja Zn(0Ac)2-2H20 liuottimessa, ja - otetaan talteen saatu tetrakis[a-pyridyyli]sinkkiftalosyaniini, jolla on kaava III
10. Patenttivaatimuksen 9 mukainen menetelmä, jossa - järjestetään saataville seos, jossa on saatu tetrakis[a-pyridyyli]sinkkiftalo-syaniini, jolla on kaava III, ja metyylijodidia liuottimessa, - sekoitetaan samalla lämmittäen, kuten 40-60°C:n lämpötilassa noin 6-24 tunnin ajan, -jäähdytetään seos, ja - otetaan talteen saatu tetrakis[metyyli-a-pyridyylijodoniumsuola]sinkkiftalo-syaniini, jolla on kaava V
11. Patenttivaatimuksen 8 mukainen menetelmä, jossa - järjestetään saataville seos, jossa on saatu ftalosyaniini ja metyylijodidia liuottimessa, - annetaan seoksen reagoida samalla lämmittäen, kuten 40-60°C:n lämpötilassa noin 6-24 tunnin ajan, -jäähdytetään seos, ja - otetaan talteen saatu tetrakis[metyyli-a-pyridyylijodoniumsuola]ftalosyaniini, jolla on kaava IV
12. Menetelmä kaavan III mukaisen tetrakis[a-pyridyyli]sinkkiftalosyaniinin valmistamiseksi,
jossa menetelmässä -järjestetään saataville 3-(pyridiini-4-yyli)bentseeni-1,2-dikarbonitriiliä, - lämmitetään 3-(pyridiini-4-yyli)bentseeni-1,2-dikarbonitriili ja sinkkiasetaat-tia dimetyyliaminoetanolissa takaisinvirtauksessa, kuten 120-150°C:n lämpötilassa noin 6-24 tunnin ajan, -jäähdytetään seos, ja - otetaan talteen saatu tetrakis[a-pyridyyli]sinkkiftalosyaniini, jolla on kaava III.
13. Patenttivaatimuksen 12 mukainen menetelmä, jossa - järjestetään saataville seos, jossa on saatu tetrakis[a-pyridyyli]sinkkiftalo-syaniini ja metyylijodidia liuottimessa, - sekoitetaan samalla lämmittäen, kuten 40-60°C:n lämpötilassa noin 6-24 tunnin ajan, -jäähdytetään seos, ja - otetaan talteen saatu tetrakis[metyyli-a-pyridyylijodoniumsuola]sinkkiftalo-syaniini, jolla on kaava V
FI20165867A 2016-11-17 2016-11-17 Valoherkiste FI127163B (fi)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FI20165867A FI127163B (fi) 2016-11-17 2016-11-17 Valoherkiste
US16/349,893 US10875871B2 (en) 2016-11-17 2017-11-09 Photosensitizer
CN201780071239.XA CN109996801B (zh) 2016-11-17 2017-11-09 光敏剂
PCT/FI2017/050775 WO2018091774A1 (en) 2016-11-17 2017-11-09 Photosensitizer
RU2019115122A RU2019115122A (ru) 2016-11-17 2017-11-09 Фотосенсибилизатор
EP17871183.4A EP3541818A4 (en) 2016-11-17 2017-11-09 PHOTOSENSITIZER

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FI20165867A FI127163B (fi) 2016-11-17 2016-11-17 Valoherkiste

Publications (2)

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FI127163B true FI127163B (fi) 2017-12-29
FI20165867A FI20165867A (fi) 2017-12-29

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US (1) US10875871B2 (fi)
EP (1) EP3541818A4 (fi)
CN (1) CN109996801B (fi)
FI (1) FI127163B (fi)
RU (1) RU2019115122A (fi)
WO (1) WO2018091774A1 (fi)

Families Citing this family (7)

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Publication number Priority date Publication date Assignee Title
CA3145595A1 (en) * 2019-07-01 2021-01-07 Chemical Intelligence Limited Antimicrobial dyes for healthcare apparel
CN114375317A (zh) * 2019-07-01 2022-04-19 化学智能公司 口罩用抗微生物染料
CN111912977B (zh) * 2020-06-23 2023-09-12 杜旭忠 一种光敏检测系统及其制作方法和应用
CN112014383B (zh) * 2020-06-30 2024-03-29 杜旭忠 一种用于均相化学发光的光敏剂及其制备方法和应用
DE102020121204B3 (de) * 2020-08-12 2021-10-21 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung eingetragener Verein Selbstdesinfizierendes antivirales Filtermaterial, dessen Herstellung und Anwendung, sowie Luftfiltereinrichtung mit dem Filtermaterial
CN113018436B (zh) * 2021-03-10 2022-08-16 西华师范大学 一种抗菌金属离子-酞菁/聚多巴胺纳米球及其制备方法
CN115286638B (zh) * 2022-08-08 2024-03-08 王佳玉 一种基于共轭酞菁框架的单原子Ag抗菌材料及其制备方法

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DE765583C (fi) 1938-10-25
GB522293A (en) 1938-12-08 1940-06-13 Eric Flower Bradbrook Colouring matters of the phthalocyanine series
US2277628A (en) 1938-12-08 1942-03-24 Ici Ltd Coloring matters of the phthalocyanine series
GB530881A (en) 1939-06-21 1940-12-24 Norman Hulton Haddock Manufacturing of colouring matters of the phthalocyanine series
DK1164135T3 (da) * 2000-06-15 2004-06-21 Molteni & C Substituerede metal-phthalocyaniner, fremstilling deraf og anvendelse deraf
WO2002096913A1 (en) * 2001-05-25 2002-12-05 Gentian As Substituted di(hydroxy/alkoxy)silicon phthalocyanines and their uses
DE60205085T2 (de) 2002-04-25 2006-04-20 L. Molteni & C. dei Fratelli Alitti Società di Esercizio S.p.A. Metallphthalocyanin-analoge enthaltende antibakterielle Zusammensetzungen
DE102004001457A1 (de) * 2004-01-08 2005-09-01 Basf Ag Verfahren zur Herstellung von Phthaloxyaninen
EP1904060B1 (en) 2005-06-29 2011-06-01 L. Molteni & C. Dei Fratelli Alitti Societa' Di Esercizio Societa' Per Azioni Use of phthalocyanine derivates for the non-photodynamic treatment of diseases
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JP2012528101A (ja) * 2009-05-26 2012-11-12 ビーエーエスエフ ソシエタス・ヨーロピア アリール又はヘタリール置換基を有するフタロシアニン化合物を、有機太陽電池で用いる使用
WO2012102395A1 (ja) 2011-01-28 2012-08-02 東洋インキＳｃホールディングス株式会社 カラーフィルタ用着色組成物、およびカラーフィルタ
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CN105315289A (zh) * 2015-11-17 2016-02-10 南京师范大学 一种锌酞菁氢碘酸盐光敏剂及其制备方法和应用

Also Published As

Publication number Publication date
RU2019115122A (ru) 2020-12-17
US10875871B2 (en) 2020-12-29
US20190337958A1 (en) 2019-11-07
CN109996801B (zh) 2022-03-22
WO2018091774A1 (en) 2018-05-24
CN109996801A (zh) 2019-07-09
FI20165867A (fi) 2017-12-29
EP3541818A1 (en) 2019-09-25
EP3541818A4 (en) 2020-07-29
RU2019115122A3 (fi) 2021-02-19

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