FI122939B - Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa - Google Patents

Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa Download PDF

Info

Publication number
FI122939B
FI122939B FI20090238A FI20090238A FI122939B FI 122939 B FI122939 B FI 122939B FI 20090238 A FI20090238 A FI 20090238A FI 20090238 A FI20090238 A FI 20090238A FI 122939 B FI122939 B FI 122939B
Authority
FI
Finland
Prior art keywords
solution
extraction
hydroxylamine
process according
reaction
Prior art date
Application number
FI20090238A
Other languages
English (en)
Finnish (fi)
Swedish (sv)
Other versions
FI20090238A0 (fi
FI20090238A (fi
Inventor
Erkki Paatero
Kai Jyrkkae
Sami Virolainen
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=40825290&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=FI122939(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Outotec Oyj filed Critical Outotec Oyj
Priority to FI20090238A priority Critical patent/FI122939B/fi
Publication of FI20090238A0 publication Critical patent/FI20090238A0/fi
Priority to MX2011013135A priority patent/MX2011013135A/es
Priority to PE2011002059A priority patent/PE20121073A1/es
Priority to AU2010258522A priority patent/AU2010258522B2/en
Priority to PCT/FI2010/050425 priority patent/WO2010142841A1/fr
Priority to US13/376,907 priority patent/US8974673B2/en
Priority to CA2762946A priority patent/CA2762946C/fr
Priority to ES10785790.6T priority patent/ES2688656T3/es
Priority to BRPI1011120A priority patent/BRPI1011120A2/pt
Priority to CN201080025520.8A priority patent/CN102459662B/zh
Priority to EP10785790.6A priority patent/EP2440678B1/fr
Priority to EA201190317A priority patent/EA021085B1/ru
Publication of FI20090238A publication Critical patent/FI20090238A/fi
Priority to CL2011003102A priority patent/CL2011003102A1/es
Priority to ZA2012/00220A priority patent/ZA201200220B/en
Publication of FI122939B publication Critical patent/FI122939B/fi
Application granted granted Critical
Priority to US14/611,466 priority patent/US20150144540A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/30—Oximes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/02—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor with moving adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D21/00—Separation of suspended solid particles from liquids by sedimentation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/114—Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections
    • B01F27/1145—Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections ribbon shaped with an open space between the helical ribbon flight and the rotating axis
    • B01F27/11451—Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections ribbon shaped with an open space between the helical ribbon flight and the rotating axis forming open frameworks or cages
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/92—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80—Mixing plants; Combinations of mixers
    • B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80—Mixing plants; Combinations of mixers
    • B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
    • B01F33/811—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/14—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0084—Treating solutions
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B15/00—Obtaining copper
    • C22B15/0063—Hydrometallurgy
    • C22B15/0084—Treating solutions
    • C22B15/0089—Treating solutions by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/02—Apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/40—Mixtures
    • C22B3/402—Mixtures of acyclic or carbocyclic compounds of different types
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Physical Water Treatments (AREA)
FI20090238A 2009-06-11 2009-06-11 Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa FI122939B (fi)

Priority Applications (15)

Application Number Priority Date Filing Date Title
FI20090238A FI122939B (fi) 2009-06-11 2009-06-11 Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa
EA201190317A EA021085B1 (ru) 2009-06-11 2010-05-26 Способ регенерации экстракционного раствора в процессах экстракции металлов
ES10785790.6T ES2688656T3 (es) 2009-06-11 2010-05-26 Método y aparato para la regeneración de la disolución de extracción en procedimientos de extracción de metales
EP10785790.6A EP2440678B1 (fr) 2009-06-11 2010-05-26 Procédé et appareil pour la régénération d'une solution d'extraction dans des procédés d'extraction de métaux
AU2010258522A AU2010258522B2 (en) 2009-06-11 2010-05-26 Method and apparatus for regeneration of extraction solution in metal extraction processes
PCT/FI2010/050425 WO2010142841A1 (fr) 2009-06-11 2010-05-26 Procédé et appareil pour la régénération d'une solution d'extraction dans des procédés d'extraction de métaux
US13/376,907 US8974673B2 (en) 2009-06-11 2010-05-26 Method of regeneration an organic extraction solution that has been used in a liquid-liquid extraction process
CA2762946A CA2762946C (fr) 2009-06-11 2010-05-26 Procede et appareil pour la regeneration d'une solution d'extraction dans des procedes d'extraction de metaux
MX2011013135A MX2011013135A (es) 2009-06-11 2010-05-26 Metodo y aparato para la regeneracion de una solucion de extraccion en procesos de extraccion de metal.
BRPI1011120A BRPI1011120A2 (pt) 2009-06-11 2010-05-26 método e aparelho para regeneração de solução de extração em extração de metal
CN201080025520.8A CN102459662B (zh) 2009-06-11 2010-05-26 在金属萃取过程中对萃取溶液进行再生的方法和装置
PE2011002059A PE20121073A1 (es) 2009-06-11 2010-05-26 Metodo y aparato para la regeneracion de una solucion de extraccion en procesos de extraccion de metal
CL2011003102A CL2011003102A1 (es) 2009-06-11 2011-12-07 Metodo para tratar solucion organica de extraccion utilizada en extraccion liquido-liquido que comprende etapa de reaccion en la cual solucion de extraccion se pone en contacto con solucion acuosa de hidroxilamina, etapa de separacion y etapa de purificacion por adsorcion de sustancias dañinas de reacciones de re-oximacion, y aparato.
ZA2012/00220A ZA201200220B (en) 2009-06-11 2012-01-11 Mehtod and apparatus for regeneration of extraction solution in metal extraction processes
US14/611,466 US20150144540A1 (en) 2009-06-11 2015-02-02 Method and apparatus for regeneration of extraction solution in metal extraction processes

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20090238 2009-06-11
FI20090238A FI122939B (fi) 2009-06-11 2009-06-11 Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa

Publications (3)

Publication Number Publication Date
FI20090238A0 FI20090238A0 (fi) 2009-06-11
FI20090238A FI20090238A (fi) 2010-12-12
FI122939B true FI122939B (fi) 2012-09-14

Family

ID=40825290

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20090238A FI122939B (fi) 2009-06-11 2009-06-11 Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa

Country Status (14)

Country Link
US (2) US8974673B2 (fr)
EP (1) EP2440678B1 (fr)
CN (1) CN102459662B (fr)
AU (1) AU2010258522B2 (fr)
BR (1) BRPI1011120A2 (fr)
CA (1) CA2762946C (fr)
CL (1) CL2011003102A1 (fr)
EA (1) EA021085B1 (fr)
ES (1) ES2688656T3 (fr)
FI (1) FI122939B (fr)
MX (1) MX2011013135A (fr)
PE (1) PE20121073A1 (fr)
WO (1) WO2010142841A1 (fr)
ZA (1) ZA201200220B (fr)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102775326B (zh) * 2012-08-07 2015-08-26 中国石油化工股份有限公司 一种减少羟胺无机液失活的方法
FI124666B (en) * 2012-12-20 2014-11-28 Outotec Finland Oy Process and system for removing fluoride from sulphate solutions
CN103572054A (zh) * 2013-11-25 2014-02-12 重庆浩康医药化工集团有限公司 湿法冶金萃取系统中醛肟类萃取剂的再生工艺
FI20155195A (fi) 2015-03-20 2016-09-21 Outotec Finland Oy Hajonneiden oksiimimetalliuuttojen käsittely orgaanisissa prosessiliuoksissa
CN105219961B (zh) * 2015-09-15 2017-03-22 南昌航空大学 一种老化c272有机相的再生方法
CN105200234B (zh) * 2015-09-21 2017-04-12 南昌航空大学 一种老化环烷酸有机相的再生方法
DE102016203293A1 (de) * 2016-03-01 2017-09-07 Sandvik Materials Technology Deutschland Gmbh Vorrichtung, Anlage und Verfahren zum Zumischen wenigstens eines ersten Stoffs und eines zweiten Stoffes zu einem Grundstoff zur Bildung einer Mischung
CN106693462B (zh) * 2016-12-23 2022-07-08 灵宝金源矿业股份有限公司 铜溶剂萃取澄清室的第三相清理装置
CN106831486B (zh) * 2017-03-03 2019-03-29 山东省化工研究院 一种合成酮肟的工艺方法
CN111349785A (zh) * 2018-12-24 2020-06-30 格林美（江苏）钴业股份有限公司 一种再生铜萃取剂的制备方法及其生产装置
CN110652744B (zh) * 2019-10-24 2021-04-16 西南化工研究设计院有限公司 一种分离卤化物和碳酸盐的有机萃取剂及方法
CN113476895B (zh) * 2021-07-13 2022-08-26 孚迪斯石油化工（葫芦岛）有限公司 一种润滑油精制提取装置
CN115430172B (zh) * 2022-08-17 2023-07-04 河北喜之郎食品有限公司 一种通过膨润土调控颗粒度的茶叶萃取设备及工艺

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3764622A (en) * 1969-07-14 1973-10-09 Texaco Inc Purification process
US4104359A (en) * 1977-02-28 1978-08-01 Amax Inc. Regeneration of organic extractants containing α-hydroxyoximes
DE3607997A1 (de) * 1986-03-11 1987-09-17 Basf Ag Verfahren zur reinigung von ammoniumsulfat enthaltendem cyclohexanoxim
FI88773C (fi) 1990-04-04 1993-07-12 Outokumpu Oy Saett att blanda ihop och separera tvao loesningsfaser samt apparatur foer detta
US5488161A (en) * 1992-03-20 1996-01-30 Henkel Corporation Oximation process
FI96968C (fi) 1993-12-02 1996-09-25 Outokumpu Eng Contract Menetelmä metallien uuttamiseksi suurista liuosvirtauksista ja laitteisto tämän toteuttamiseksi
CN1110329A (zh) * 1994-04-04 1995-10-18 江西铜业公司科研设计所 一种从lix萃取铜过程产生的界面絮凝物中回收萃取剂的方法
US5993757A (en) * 1997-03-03 1999-11-30 Henkel Corporation Reoximation of metal extraction circuit organics
FI112328B (fi) 2002-05-16 2003-11-28 Outokumpu Oy Menetelmä ja laitteisto neste-nesteuuton dispersion ohjaamiseksi
JP4659731B2 (ja) * 2003-01-30 2011-03-30 ディーエスエム アイピー アセッツ ビー．ブイ． シクロヘキサノンオキシム、シクロヘキサノン、および有機溶媒を含む有機溶液の処理方法
CN101259357A (zh) * 2007-12-14 2008-09-10 华南理工大学 从印刷行业废气中吸附回收有机溶剂的方法及装置
CN101417208A (zh) * 2008-11-14 2009-04-29 清华大学 一种利用膜分离技术回收水相中萃取剂的方法

Also Published As

Publication number Publication date
EP2440678A1 (fr) 2012-04-18
WO2010142841A1 (fr) 2010-12-16
PE20121073A1 (es) 2012-08-28
CN102459662A (zh) 2012-05-16
ZA201200220B (en) 2012-09-26
EA021085B1 (ru) 2015-04-30
FI20090238A0 (fi) 2009-06-11
ES2688656T3 (es) 2018-11-06
CL2011003102A1 (es) 2012-07-06
CN102459662B (zh) 2014-02-19
US8974673B2 (en) 2015-03-10
FI20090238A (fi) 2010-12-12
BRPI1011120A2 (pt) 2016-03-15
CA2762946C (fr) 2017-06-27
CA2762946A1 (fr) 2010-12-16
EP2440678A4 (fr) 2017-03-29
US20150144540A1 (en) 2015-05-28
AU2010258522A1 (en) 2011-12-15
EA201190317A1 (ru) 2013-01-30
AU2010258522B2 (en) 2015-07-30
US20120080382A1 (en) 2012-04-05
EP2440678B1 (fr) 2018-07-18
MX2011013135A (es) 2012-01-20

Similar Documents

Publication Publication Date Title
FI122939B (fi) Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa
AU699079B2 (en) Method of recovering extractant
US6113804A (en) Composition and use of the composition for the extraction of metals from aqueous solution
AU2010227442B2 (en) Apparatus and method for removing impurities in connection with liquid-liquid extraction of copper
Laki et al. Separation of manganese from aqueous solution using an emulsion liquid membrane
Kumbasar Extraction of cadmium from solutions containing various heavy metal ions by Amberlite LA-2
Valenzuela et al. Use of a surfactant liquid membrane contactor for zinc uptake from an acid aqueous effluent
US10662499B2 (en) Treatment of degraded oxime metal extractants in process organic solutions
Valenzuela et al. A kinetics analysis applied to the recovery of Zn (II) content from mine drainage by using a surfactant liquid membrane
US11648512B2 (en) Enhanced emulsion liquid membranes for extraction of pollutants from water
Navarro et al. Experimental study of phase entrainment in copper solvent extraction
US20190062867A1 (en) Methods and systems for removing polar compounds from a metal-containing solution
US7193114B1 (en) Extraction of metals by mercaptans attached to silica gel by azeotropic distillation
Hachemaoui et al. Emulsion liquid membrane extraction of cerium ions from acidic solution using CYANEX 301
Kondo et al. Extraction of precious and base metals with microcapsules containing an extractant
WO2020190822A1 (fr) Procédés de réduction de la nitration d'agents d'extraction dans des systèmes d'extraction au solvant
Cole A HOLISTIC APPROACH TO ORGANIC QUALITY IN COPPER SOLVENT EXTRACTION
CHICAN et al. BEHAVIOR OF COBALT-NICKEL SEPARATION ON LIQUID MEMBRANE
MXPA97005123A (en) Extract recovery method

Legal Events

Date Code Title Description
FG Patent granted

Ref document number: 122939

Country of ref document: FI

Kind code of ref document: B

MM Patent lapsed