ES8703827A1 - Procedimeinto quimico para la racemiracion de un x-aminoacido. - Google Patents
Procedimeinto quimico para la racemiracion de un x-aminoacido.Info
- Publication number
- ES8703827A1 ES8703827A1 ES546489A ES546489A ES8703827A1 ES 8703827 A1 ES8703827 A1 ES 8703827A1 ES 546489 A ES546489 A ES 546489A ES 546489 A ES546489 A ES 546489A ES 8703827 A1 ES8703827 A1 ES 8703827A1
- Authority
- ES
- Spain
- Prior art keywords
- racemization
- alpha
- amino acid
- resolution
- amino acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B55/00—Racemisation; Complete or partial inversion
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B57/00—Separation of optically-active compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PROCEDIMIENTO QUIMICO PARA LA RACEMIZACION DE UN A-AMINOACIDO. CONSISTE EN TRATAR UN A-AMINOACIDO OPTICAMENTE ACTIVO, DE FORMULA GENERAL (I), EN LA QUE R REPRESENTA UN GRUPO HIDROCARBILO O HETEROCICLICO OPCIONALMENTE SUSTITUIDO, CON UNA CETONA, DE FORMULA GENERAL (II), EN LA QUE R1 Y R2 SON IGUALES O DIFERENTES Y CADA UNO DE ELLOS REPRESENTA UN GRUPO HIDROCARBILO O HETEROCICLICO O BIEN R1 Y R2 UNIDAS COMPLETAN UN ANILLO DE CICLOALCANONA, EN PRESENCIA DE UN ACIDO ORGANICO Y, OPCIONALMENTE, SI SE DESEA, SE RESUELVE EL A-AMINOACIDO RACEMICO PARA OBTENER EL A-AMINOACIDO OPTICAMENTE ACTIVO, POR TRATAMIENTO CON UN AGENTE DE RESOLUCION QUE ORIGINA LA CRISTALIZACION DE LA SAL DEL A-AMINOACIDO, EN PRESENCIA DE UNA CETONA Y DE UN ACIDO ORGANICO. DE APLICACION EN LA SINTESIS DE COMPUESTOS FISIOLOGICAMENTE ACTIVOS, EN ESPECIAL COMO CADENAS LATERALES EN LOS ANTIBIOTICOS DE PENICILINA.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB848421964A GB8421964D0 (en) | 1984-08-30 | 1984-08-30 | Chemical process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES546489A0 ES546489A0 (es) | 1987-03-01 |
| ES8703827A1 true ES8703827A1 (es) | 1987-03-01 |
Family
ID=10566049
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES546489A Expired ES8703827A1 (es) | 1984-08-30 | 1985-08-28 | Procedimeinto quimico para la racemiracion de un x-aminoacido. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4647692A (es) |
| EP (1) | EP0173921B1 (es) |
| JP (1) | JPS6169748A (es) |
| AT (1) | ATE34381T1 (es) |
| AU (1) | AU4682585A (es) |
| DE (1) | DE3562772D1 (es) |
| DK (1) | DK391585A (es) |
| ES (1) | ES8703827A1 (es) |
| GB (1) | GB8421964D0 (es) |
| GR (1) | GR852076B (es) |
| PT (1) | PT81043B (es) |
| ZA (1) | ZA856540B (es) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0499376A1 (en) * | 1991-01-31 | 1992-08-19 | Hoechst Celanese Corporation | Precipitation-induced asymmetric transformation of chiral alpha-amino acids and salts thereof |
| DE4407197A1 (de) * | 1994-03-04 | 1995-09-07 | Hoechst Schering Agrevo Gmbh | Verfahren zur Herstellung von /L/-Homoalanin-4-yl-(methyl)phosphinsäure und deren Salze durch Racematspaltung |
| CA2201780C (en) * | 1994-10-07 | 2007-01-09 | Ulrich Conrad Dyer | Racemisation of precursors to levobupivacaine and analogues thereof |
| US6156900A (en) * | 1994-10-07 | 2000-12-05 | Darwin Discovery Limited | Racemization of precursors to levobupivacaine and analogues thereof |
| US6812363B2 (en) * | 2002-10-15 | 2004-11-02 | Usv Limited | Racemization of optically active 2-substituted phenyl glycine esters |
| JP2011024572A (ja) * | 2009-06-29 | 2011-02-10 | Mitsubishi Gas Chemical Co Inc | 光学活性アミノ酸の製造法 |
| KR20170029965A (ko) * | 2015-09-08 | 2017-03-16 | 주식회사 아미노로직스 | D-아르기닌의 제조 방법 |
| WO2018108797A1 (de) | 2016-12-15 | 2018-06-21 | Bayer Cropscience Aktiengesellschaft | Verfahren zur herstellung von l-glufosinat oder dessen salzen unter verwendung von ephedrin |
| WO2018108794A1 (de) | 2016-12-15 | 2018-06-21 | Bayer Cropscience Aktiengesellschaft | Verfahren zur herstellung von d-glufosinat oder dessen salzen unter verwendung von ephedrin |
| BR112021018995A2 (pt) | 2019-04-16 | 2021-11-30 | Basf Se | Método para preparar monoidrato de l-glufosinato de amônio cristalino e enzimas d-aminoácido oxidase mutantes |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3458568A (en) * | 1965-02-19 | 1969-07-29 | Toa Gosei Chem Ind | Process for preparing an optically inactive amino acid from an optically active amino acid |
| GB1417060A (en) * | 1972-10-19 | 1975-12-10 | Ajinomoto Kk | Racemization of optically active n-acyl amino acids |
| JPS54109912A (en) * | 1978-02-14 | 1979-08-29 | Ajinomoto Co Inc | Racemization of optically active amino acid ester |
| US4401820A (en) * | 1981-01-23 | 1983-08-30 | Tanabe Seiyaku Co., Ltd. | Process for racemizing optically active α-amino acids or a salt thereof |
| JPS5810544A (ja) * | 1981-07-09 | 1983-01-21 | Tanabe Seiyaku Co Ltd | 光学活性ｐ−ヒドロキシフエニルグリシン塩の製法 |
-
1984
- 1984-08-30 GB GB848421964A patent/GB8421964D0/en active Pending
-
1985
- 1985-08-22 DE DE8585110569T patent/DE3562772D1/de not_active Expired
- 1985-08-22 AT AT85110569T patent/ATE34381T1/de not_active IP Right Cessation
- 1985-08-22 EP EP85110569A patent/EP0173921B1/en not_active Expired
- 1985-08-28 JP JP60189331A patent/JPS6169748A/ja active Pending
- 1985-08-28 PT PT81043A patent/PT81043B/pt unknown
- 1985-08-28 GR GR852076A patent/GR852076B/el unknown
- 1985-08-28 US US06/770,508 patent/US4647692A/en not_active Expired - Fee Related
- 1985-08-28 DK DK391585A patent/DK391585A/da not_active Application Discontinuation
- 1985-08-28 ZA ZA856540A patent/ZA856540B/xx unknown
- 1985-08-28 ES ES546489A patent/ES8703827A1/es not_active Expired
- 1985-08-28 AU AU46825/85A patent/AU4682585A/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| ES546489A0 (es) | 1987-03-01 |
| ATE34381T1 (de) | 1988-06-15 |
| DK391585A (da) | 1986-03-01 |
| DK391585D0 (da) | 1985-08-28 |
| AU4682585A (en) | 1986-03-06 |
| GB8421964D0 (en) | 1984-10-03 |
| DE3562772D1 (en) | 1988-06-23 |
| JPS6169748A (ja) | 1986-04-10 |
| ZA856540B (en) | 1986-06-25 |
| GR852076B (es) | 1985-12-23 |
| US4647692A (en) | 1987-03-03 |
| EP0173921A1 (en) | 1986-03-12 |
| EP0173921B1 (en) | 1988-05-18 |
| PT81043A (en) | 1985-09-01 |
| PT81043B (en) | 1987-04-06 |
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