ES8504165A1 - Un procedimiento para el aislamiento de un compuesto de pirano - Google Patents

Un procedimiento para el aislamiento de un compuesto de pirano

Info

Publication number
ES8504165A1
ES8504165A1 ES518361A ES518361A ES8504165A1 ES 8504165 A1 ES8504165 A1 ES 8504165A1 ES 518361 A ES518361 A ES 518361A ES 518361 A ES518361 A ES 518361A ES 8504165 A1 ES8504165 A1 ES 8504165A1
Authority
ES
Spain
Prior art keywords
mixture
recovering
fraction
tetrahydrodibenzo
pyrans
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES518361A
Other languages
English (en)
Other versions
ES518361A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Aerojet Rocketdyne Inc
Original Assignee
Aerojet General Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aerojet General Corp filed Critical Aerojet General Corp
Publication of ES518361A0 publication Critical patent/ES518361A0/es
Publication of ES8504165A1 publication Critical patent/ES8504165A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/78—Ring systems having three or more relevant rings
    • C07D311/80—Dibenzopyrans; Hydrogenated dibenzopyrans

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PROCEDIMIENTO PARA EL AISLAMIENTO DE UN COMPUESTO DE PIRANO A PARTIR DE UNA MEZCLA DE SINTESIS CRUDA.COMPRENDE LAS SIGUIENTES OPERACIONES: PRIMERA, SE ESTERIFICA UNA PORCION DE LOS COMPONENTES DE DICHA MEZCLA, PARA FORMAR SUS ESTERES DEL ACIDO ALCANOICO PERFLUORADO; SEGUNDA, SE SEPARAN COMPONENTES DE BAJO PUNTO DE EBULLICION Y COMPONENTES NO VOLATILES A PARTIR DE DICHA MEZCLA; TERCERA, SE HACE PASAR DICHA MEZCLA A TRAVES DE UNA PRIMERA COLUMNA DE CROMATOGRAFIA DE GASES Y A TRAVES DE UNA SEGUNDA COLUMNA DE CROMATROGRAFIA DE GASES; Y POR ULTIMO, SE HIDROLIZA EL SUBPRODUCTO RECUPERADO PARA CONVERTIR LOS RESTOS DE ESTER ALCANOICO PERFLUORADO EN GRUPOS HIDROXILO.
ES518361A 1981-12-21 1982-12-20 Un procedimiento para el aislamiento de un compuesto de pirano Expired ES8504165A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/332,644 US4381399A (en) 1981-12-21 1981-12-21 Purification of tetrahydrodibenzo[b,d]pyrans from crude synthetic mixtures

Publications (2)

Publication Number Publication Date
ES518361A0 ES518361A0 (es) 1984-08-01
ES8504165A1 true ES8504165A1 (es) 1984-08-01

Family

ID=23299180

Family Applications (1)

Application Number Title Priority Date Filing Date
ES518361A Expired ES8504165A1 (es) 1981-12-21 1982-12-20 Un procedimiento para el aislamiento de un compuesto de pirano

Country Status (11)

Country Link
US (1) US4381399A (es)
EP (1) EP0098291A4 (es)
JP (1) JPS58502149A (es)
AR (1) AR230443A1 (es)
AU (1) AU1153983A (es)
DK (1) DK379683D0 (es)
ES (1) ES8504165A1 (es)
IE (1) IE54285B1 (es)
IT (1) IT1200512B (es)
WO (1) WO1983002275A1 (es)
ZA (1) ZA828462B (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2925753B2 (ja) * 1990-02-23 1999-07-28 ダイセル化学工業株式会社 光学異性体の分離方法
US5342971A (en) * 1992-12-29 1994-08-30 The Australian National University Process for the preparation of dibenzo[b,d]pyrans
CA2504743C (en) * 2002-11-12 2012-04-24 Mallinckrodt Inc. Cannabinoid crystalline derivatives and process of cannabinoid purification
AU2004230871A1 (en) * 2003-04-10 2004-10-28 Mallinckrodt Inc. Olivetol-cyclodextrin complexes and regio-selective process for preparing delta 9-tetrahydrocannabinol
EP1773801A1 (de) * 2004-07-19 2007-04-18 Cilag Ltd. Verfahren zur gewinnung von reinem tetrahydrocannabinol
US20060051824A1 (en) * 2004-09-03 2006-03-09 Haoyun An Tetrahydrocannabinoid antigens and method of use
US7323576B2 (en) * 2004-10-01 2008-01-29 Alphora Research Inc. Synthetic route to dronabinol
TWI436991B (zh) 2004-11-22 2014-05-11 Euro Celtique Sa 用於純化反-（-）-△９-四氫大麻酚與反-（＋）-△９-四氫大麻酚之方法
TWI366460B (en) 2005-06-16 2012-06-21 Euro Celtique Sa Cannabinoid active pharmaceutical ingredient for improved dosage forms
KR20080063800A (ko) * 2005-09-29 2008-07-07 에이엠알 테크놀로지, 인크. 델타-9-테트라히드로칸나비놀의 제조 방법
CA3117347A1 (en) 2018-10-31 2020-05-07 Enantia, S.L. Solid compositions of cocrystals of cannabinoids

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3920705A (en) * 1967-05-19 1975-11-18 Theodore Petrzilka 6a,10a-trans-6a,10,10a-tetrahydrodibenzo(b,d)-pyrans
CH481911A (de) * 1967-05-19 1969-11-30 Theodor Dr Petrzilka Verfahren zur Herstellung von tricyclischen Verbindungen
US3833616A (en) * 1968-09-16 1974-09-03 T Petrzilka 6a,10a-trans-6a,7,8,10a-tetrahydrodibenzo(b,d)-pyrans
US3668224A (en) * 1970-07-02 1972-06-06 Theodor Petrzilka PROCESS OF PRODUCING 6a, 10a-TRANS-6a,7,8,10a-TETRAHYDRODIBENZO (b,d)-PYRANS
US4025516A (en) * 1975-06-23 1977-05-24 The John C. Sheehan Institute For Research, Inc. Process for the preparation of (-)-6a,10a-trans-6a,7,8,10a-tetrahydrodibenzo[b,d]-pyrans
US4116979A (en) * 1975-06-23 1978-09-26 Sheehan Institute For Research, Inc. Process for the preparation of (-)-6a,10a-trans-6a,7,8,10a-tetrahydrodibenzo[b,d]-pyrans
US4036857A (en) * 1976-02-02 1977-07-19 Sharps Associates Benzopyrans having an unsaturated side chain

Also Published As

Publication number Publication date
ES518361A0 (es) 1984-08-01
EP0098291A1 (en) 1984-01-18
DK379683A (da) 1983-08-19
IT1200512B (it) 1989-01-18
AR230443A1 (es) 1984-04-30
AU1153983A (en) 1983-07-15
IT8249707A0 (it) 1982-12-20
US4381399A (en) 1983-04-26
DK379683D0 (da) 1983-08-19
EP0098291A4 (en) 1984-05-29
IE54285B1 (en) 1989-08-16
WO1983002275A1 (en) 1983-07-07
JPS58502149A (ja) 1983-12-15
ZA828462B (en) 1983-09-28
IE823008L (en) 1983-06-21

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