ES8406060A1 - Procedimiento de preparacion de cloruro de trifluoracetilo - Google Patents
Procedimiento de preparacion de cloruro de trifluoracetiloInfo
- Publication number
- ES8406060A1 ES8406060A1 ES527047A ES527047A ES8406060A1 ES 8406060 A1 ES8406060 A1 ES 8406060A1 ES 527047 A ES527047 A ES 527047A ES 527047 A ES527047 A ES 527047A ES 8406060 A1 ES8406060 A1 ES 8406060A1
- Authority
- ES
- Spain
- Prior art keywords
- preparation
- trifluoroacetyl chloride
- trifluoroacetaldehyde
- catalysis
- reactant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
Abstract
PROCEDIMIENTO DE PREPARACION DE CLORURO DE TRIFLUORACETILO. CONSISTE EN CLORAR EL TRIFLUORACETALDEHIDO (FLUORAL) CATALITICAMENTE CON EL CLORO EN FASE DE VAPOR SOBRE UN CARBON ACTIVO. LA RELACION MOLAR CLORO/FLUORAL ES DE 1 A 2. LA TEMPERATURA OSCILA ENTRE 13º C Y 250º C. LA CLORACION SE REALIZA: A) EN PRESENCIA DE UNA CANTIDAD DE ACIDO CLORHIDRICO TAL QUE LA RELACION MOLAR CLORHIDRICO/FLUORAL NO SEA SUPERIOR A 5; B) TAMBIEN SE REALIZA LA CLORACION EN PRESENCIA DE UNA CANTIDAD DE UN DILUYENTE INERTE DE FORMA QUE LA RELACION MOLAR DILUYENTE/FLUORAL NO SEA SUPERIOR A 5;C) LA CLORACION SE REALIZA EN PRESENCIA DE CANTIDADES DE ACIDO CLORHIDRICO Y DILUYENTE INERTE DE FORMA QUE LA SUMA DE LAS RELACIONES MOLARES ACIDO CLORHIDRICO/FLUORAL Y DILUYENTE INERTE/FLUORAL NO SEA SUPERIOR A 5. EL DILUYENTE INERTE ES NITROGENO Y CLOROTRIFLUORMETANO. EL TIEMPO DE CONTACTO CON EL LECHO DONDE SE REALIZA LA CLORACION ES DE 5 A 30 SEGUNDOS. LA VELOCIDAD DE LA MEZCLA GASEOSA DE LOS REACTIVOS ES TAL QUE CORRESPONDEA UN CAUDAL DE 1,5 A 3,0 VECES MAS ELEVADO QUE EL CAUDAL MINIMO DE FLUIDIFICACION DEL CATALIZADOR.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8218567A FR2535712A1 (fr) | 1982-11-05 | 1982-11-05 | Procede de preparation de chlorure de trifluoroacetyle |
Publications (2)
Publication Number | Publication Date |
---|---|
ES527047A0 ES527047A0 (es) | 1984-07-01 |
ES8406060A1 true ES8406060A1 (es) | 1984-07-01 |
Family
ID=9278929
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES527047A Expired ES8406060A1 (es) | 1982-11-05 | 1983-11-04 | Procedimiento de preparacion de cloruro de trifluoracetilo |
Country Status (9)
Country | Link |
---|---|
US (1) | US4643851A (es) |
EP (1) | EP0108675B1 (es) |
JP (1) | JPS5998031A (es) |
AU (1) | AU555457B2 (es) |
CA (1) | CA1197524A (es) |
DD (1) | DD210898A5 (es) |
DE (1) | DE3360355D1 (es) |
ES (1) | ES8406060A1 (es) |
FR (1) | FR2535712A1 (es) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5241113A (en) * | 1992-09-15 | 1993-08-31 | E. I. Du Pont De Nemours And Company | Process for producing trifluoroacetyl chloride |
WO1994025419A1 (en) * | 1993-04-30 | 1994-11-10 | E.I. Du Pont De Nemours And Company | AZEOTROPIC AND AZEOTROPE-LIKE COMPOSITIONS AND A PROCESS FOR SEPARATING HCl AND HALOCARBONS |
DE4427303A1 (de) * | 1994-08-02 | 1996-02-08 | Hoechst Ag | Verfahren zur Herstellung von Trichloracetylchlorid |
JP3887825B2 (ja) * | 1996-12-25 | 2007-02-28 | ダイキン工業株式会社 | ポリフルオロアルキル基を有する酸クロリドの製造方法 |
JP4940810B2 (ja) * | 2006-04-13 | 2012-05-30 | セントラル硝子株式会社 | 3,3,3−トリフルオロプロピオン酸クロリドの製造方法 |
EP2987782A1 (en) | 2014-08-22 | 2016-02-24 | Solvay SA | Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide |
EP3221289A1 (en) | 2014-11-17 | 2017-09-27 | Solvay SA | Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2922816A (en) * | 1960-01-26 | |||
GB515963A (en) * | 1938-06-16 | 1939-12-19 | Arthur Carpmael | Process for the manufacture of higher fatty acid chlorides |
FR1228408A (fr) * | 1958-04-30 | 1960-08-29 | Du Pont | Procédé de préparation de l'acide trifluoracétique |
DE1186844B (de) * | 1963-03-07 | 1965-02-11 | Hoechst Ag | Verfahren zur Herstellung von Trifluoracetylchlorid |
-
1982
- 1982-11-05 FR FR8218567A patent/FR2535712A1/fr active Granted
-
1983
- 1983-09-15 US US06/532,483 patent/US4643851A/en not_active Expired - Fee Related
- 1983-10-25 EP EP83402072A patent/EP0108675B1/fr not_active Expired
- 1983-10-25 DE DE8383402072T patent/DE3360355D1/de not_active Expired
- 1983-11-02 DD DD83256252A patent/DD210898A5/de unknown
- 1983-11-04 ES ES527047A patent/ES8406060A1/es not_active Expired
- 1983-11-04 CA CA000440459A patent/CA1197524A/fr not_active Expired
- 1983-11-04 AU AU21003/83A patent/AU555457B2/en not_active Ceased
- 1983-11-04 JP JP58206053A patent/JPS5998031A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
FR2535712B1 (es) | 1985-01-25 |
EP0108675A1 (fr) | 1984-05-16 |
JPH0253424B2 (es) | 1990-11-16 |
AU2100383A (en) | 1984-05-10 |
FR2535712A1 (fr) | 1984-05-11 |
ES527047A0 (es) | 1984-07-01 |
JPS5998031A (ja) | 1984-06-06 |
AU555457B2 (en) | 1986-09-25 |
DD210898A5 (de) | 1984-06-27 |
EP0108675B1 (fr) | 1985-07-03 |
DE3360355D1 (en) | 1985-08-08 |
CA1197524A (fr) | 1985-12-03 |
US4643851A (en) | 1987-02-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 19970612 |