ES8104213A1 - Procedimiento para la preparacion de acido 4,4'dinitro es- tilben-2,2'-disulfonico y sus sales - Google Patents
Procedimiento para la preparacion de acido 4,4'dinitro es- tilben-2,2'-disulfonico y sus salesInfo
- Publication number
- ES8104213A1 ES8104213A1 ES492243A ES492243A ES8104213A1 ES 8104213 A1 ES8104213 A1 ES 8104213A1 ES 492243 A ES492243 A ES 492243A ES 492243 A ES492243 A ES 492243A ES 8104213 A1 ES8104213 A1 ES 8104213A1
- Authority
- ES
- Spain
- Prior art keywords
- salts
- disulfonic acid
- dinitrostilbene
- preparing
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003839 salts Chemical class 0.000 title abstract 4
- UETHPMGVZHBAFB-OWOJBTEDSA-N 4,4'-dinitro-trans-stilbene-2,2'-disulfonic acid Chemical compound OS(=O)(=O)C1=CC([N+]([O-])=O)=CC=C1\C=C\C1=CC=C([N+]([O-])=O)C=C1S(O)(=O)=O UETHPMGVZHBAFB-OWOJBTEDSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- ZDTXQHVBLWYPHS-UHFFFAOYSA-N 4-nitrotoluene-2-sulfonic acid Chemical compound CC1=CC=C([N+]([O-])=O)C=C1S(O)(=O)=O ZDTXQHVBLWYPHS-UHFFFAOYSA-N 0.000 abstract 1
- GHBWBMDGBCKAQU-UHFFFAOYSA-N 5-amino-2-[2-(4-nitro-2-sulfophenyl)ethenyl]benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC(N)=CC=C1C=CC1=CC=C([N+]([O-])=O)C=C1S(O)(=O)=O GHBWBMDGBCKAQU-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- -1 alkali metal cation Chemical group 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH536979 | 1979-06-08 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES492243A0 ES492243A0 (es) | 1981-04-01 |
| ES8104213A1 true ES8104213A1 (es) | 1981-04-01 |
Family
ID=4292399
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES492243A Expired ES8104213A1 (es) | 1979-06-08 | 1980-06-07 | Procedimiento para la preparacion de acido 4,4'dinitro es- tilben-2,2'-disulfonico y sus sales |
Country Status (16)
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0083555B1 (de) * | 1981-12-31 | 1985-05-29 | Ciba-Geigy Ag | Verfahren zur Herstellung von p-Nitrotoluol-2-sulfonsäure |
| DE3519552A1 (de) * | 1985-05-31 | 1986-12-04 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von 4,4'-dinitrostilben-2,2'-disulfonsaeuresalzen |
| ATE51398T1 (de) * | 1987-08-12 | 1990-04-15 | Ciba Geigy Ag | Verfahren zur herstellung von 4,4'-dinitrostilben-2,2'-disulfonsaeure. |
| US4952725A (en) * | 1988-03-08 | 1990-08-28 | Ciba-Geigy Corporation | Process for the preparation of 4,4'dinitrostilbene-2,2'-disulfonic acid and its salts |
| US5021132A (en) * | 1990-08-07 | 1991-06-04 | Sandoz Ltd. | Electrochemical process for preparing 4,4'-dinitrostilbene-2,2'-disulfonic acid and the salts thereof |
| DE4330377A1 (de) * | 1993-09-08 | 1995-03-09 | Bayer Ag | Verfahren zur Herstellung von 4,4'-Dinitrostilben-2,2'-disulfonsäure |
| DE4418305A1 (de) * | 1994-05-26 | 1995-11-30 | Bayer Ag | Verfahren zur Herstellung von 4.4'-Dinitrostilben-2.2'-disulfonsäure und ihren Salzen |
| CN103626681B (zh) * | 2012-08-20 | 2015-09-09 | 中国中化股份有限公司 | 一种制备4,4′-二硝基二苯乙烯-2,2′-二磺酸的方法 |
| TWI567051B (zh) * | 2015-11-06 | 2017-01-21 | 財團法人工業技術研究院 | 二苯乙烯化合物的製備方法 |
| CN117362204A (zh) * | 2023-10-17 | 2024-01-09 | 衡水百纳化学有限公司 | 一种提高dsd酸含量的酸析工艺 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2212084A (en) * | 1940-08-20 | Nucleak alkylated diaminostilbene | ||
| US2821550A (en) * | 1956-12-27 | 1958-01-28 | Gen Aniline & Film Corp | Process of preparing 4-nitro-2-stilbene sulfonic acid salts |
| BE792103A (fr) * | 1971-12-01 | 1973-05-30 | Clayton Aniline Co Ltd | Nouveau procede de fabrication de l'acide dinitrostilbene disulfonique a l'echelle industrielle |
-
1980
- 1980-06-02 AT AT80810183T patent/ATE3974T1/de active
- 1980-06-02 DE DE8080810183T patent/DE3063958D1/de not_active Expired
- 1980-06-02 EP EP80810183A patent/EP0026154B1/de not_active Expired
- 1980-06-03 MX MX182625A patent/MX153817A/es unknown
- 1980-06-04 YU YU01485/80A patent/YU148580A/xx unknown
- 1980-06-06 BR BR8003536A patent/BR8003536A/pt not_active IP Right Cessation
- 1980-06-06 ZA ZA00803393A patent/ZA803393B/xx unknown
- 1980-06-06 SU SU802930005A patent/SU927112A3/ru active
- 1980-06-06 AR AR281315A patent/AR226180A1/es active
- 1980-06-06 DD DD80221653A patent/DD152545A5/de unknown
- 1980-06-06 PL PL1980224776A patent/PL125844B1/pl unknown
- 1980-06-06 AU AU59103/80A patent/AU538454B2/en not_active Ceased
- 1980-06-06 CA CA000353517A patent/CA1159082A/en not_active Expired
- 1980-06-07 ES ES492243A patent/ES8104213A1/es not_active Expired
- 1980-06-09 JP JP7677780A patent/JPS5629561A/ja active Granted
-
1986
- 1986-08-13 US US06/896,561 patent/US4719051A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| ATE3974T1 (de) | 1983-07-15 |
| BR8003536A (pt) | 1981-01-05 |
| ES492243A0 (es) | 1981-04-01 |
| DD152545A5 (de) | 1981-12-02 |
| US4719051A (en) | 1988-01-12 |
| JPH025741B2 (enrdf_load_stackoverflow) | 1990-02-05 |
| MX153817A (es) | 1987-01-19 |
| JPS5629561A (en) | 1981-03-24 |
| PL125844B1 (en) | 1983-06-30 |
| EP0026154B1 (de) | 1983-06-29 |
| EP0026154A1 (de) | 1981-04-01 |
| CA1159082A (en) | 1983-12-20 |
| AU538454B2 (en) | 1984-08-16 |
| YU148580A (en) | 1983-02-28 |
| SU927112A3 (ru) | 1982-05-07 |
| AR226180A1 (es) | 1982-06-15 |
| DE3063958D1 (en) | 1983-08-04 |
| ZA803393B (en) | 1981-05-27 |
| AU5910380A (en) | 1980-12-11 |
| PL224776A1 (enrdf_load_stackoverflow) | 1981-03-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PC1A | Transfer granted |