ES332252A1 - Un procedimiento para la preparacion de una oxima. - Google Patents
Un procedimiento para la preparacion de una oxima.Info
- Publication number
- ES332252A1 ES332252A1 ES0332252A ES332252A ES332252A1 ES 332252 A1 ES332252 A1 ES 332252A1 ES 0332252 A ES0332252 A ES 0332252A ES 332252 A ES332252 A ES 332252A ES 332252 A1 ES332252 A1 ES 332252A1
- Authority
- ES
- Spain
- Prior art keywords
- solvent
- stream
- oxime
- reaction zone
- zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000002904 solvent Substances 0.000 abstract 6
- 239000002253 acid Substances 0.000 abstract 4
- 150000002923 oximes Chemical class 0.000 abstract 4
- 150000003997 cyclic ketones Chemical class 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical class ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 150000002576 ketones Chemical class 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/44—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL6513426A NL6513426A (US07993877-20110809-P00003.png) | 1965-10-16 | 1965-10-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES332252A1 true ES332252A1 (es) | 1967-07-16 |
Family
ID=19794388
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES0332252A Expired ES332252A1 (es) | 1965-10-16 | 1966-10-14 | Un procedimiento para la preparacion de una oxima. |
Country Status (12)
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL135679C (US07993877-20110809-P00003.png) * | 1968-11-12 | 1900-01-01 | ||
| NL6914306A (US07993877-20110809-P00003.png) * | 1969-09-20 | 1971-03-23 | ||
| US3862230A (en) * | 1969-09-20 | 1975-01-21 | Stamicarbon | Continuous preparation of cyclohexanone oxime |
| DE2029114C2 (de) * | 1970-06-12 | 1982-07-01 | Stamicarbon B.V., 6160 Geleen | Verfahren zur Herstellung von Cyclohexanonoxim |
| US3625835A (en) * | 1970-06-15 | 1971-12-07 | Stamicarbon | Process for the recovery of cyclohexanone oxime by plural stage, vacuum distillation per a |
| NL7008838A (US07993877-20110809-P00003.png) * | 1970-06-17 | 1971-12-21 | ||
| DE2508247C3 (de) * | 1975-02-26 | 1981-03-12 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Cyclohexanonoxim |
| US4104359A (en) * | 1977-02-28 | 1978-08-01 | Amax Inc. | Regeneration of organic extractants containing α-hydroxyoximes |
| DE3942334A1 (de) * | 1989-12-21 | 1991-06-27 | Basf Ag | Verfahren zur aufarbeitung von salzsaeure, schwefelsaeure und deren hydroxylammonium- und ammoniumsalze enthaltenden waessrigen mutterlaugen |
| US5254734A (en) * | 1991-02-13 | 1993-10-19 | Mitsubishi Kasei Corporation | Method for preparing an oxime |
| US7005547B2 (en) | 2000-06-05 | 2006-02-28 | Dsm Ip Assets B.V. | Process for the preparation of cyclohexanone oxime |
| DE60138025D1 (de) * | 2000-06-05 | 2009-04-30 | Dsm Ip Assets Bv | Verfahren zur herstellung von cyclohexanonoxim |
| EP1318141A1 (en) | 2001-12-04 | 2003-06-11 | Dsm Nv | Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime |
| ATE322461T1 (de) * | 2001-12-04 | 2006-04-15 | Dsm Ip Assets Bv | Verfahren zur behandlung eines phosphatsalzes und organische verbindungen enthaltendes wässriges medium |
| MXPA04005414A (es) | 2001-12-04 | 2004-10-11 | Dsm Ip Assets Bv | Procedimiento para el tratamiento de un medio acuoso que contiene ciclohexanona oxima y ciclohexanona. |
| EP1663956A1 (en) * | 2003-01-30 | 2006-06-07 | DSM IP Assets B.V. | Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent |
| TW200829544A (en) * | 2007-01-05 | 2008-07-16 | China Petrochemical Dev Corp | Method for preparing cyclohexanone oxime |
| CN103193672B (zh) * | 2013-03-11 | 2014-09-17 | 浙江圣安化工有限公司 | 一种肟的蒸馏方法 |
| CN105384656B (zh) * | 2015-10-23 | 2017-08-25 | 中石化南京工程有限公司 | 一种环己酮肟化的方法 |
| CN105348145B (zh) * | 2015-10-23 | 2018-02-06 | 中石化南京工程有限公司 | 氨法烟气脱硫副产环己酮肟的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2270204A (en) * | 1938-11-28 | 1942-01-13 | Du Pont | Process of producing oximes |
| DE1081884B (de) * | 1959-02-13 | 1960-05-19 | Basf Ag | Verfahren zur Herstellung von Cyclododecanonoxim |
| GB972107A (en) * | 1962-09-01 | 1964-10-07 | Basf Ag | Production of oximes of cycloaliphatic ketones |
| NL301053A (US07993877-20110809-P00003.png) * | 1963-11-27 |
-
1965
- 1965-10-16 NL NL6513426A patent/NL6513426A/xx unknown
-
1966
- 1966-10-06 GB GB44743/66A patent/GB1138750A/en not_active Expired
- 1966-10-07 AT AT942866A patent/AT265240B/de active
- 1966-10-07 DE DEP1272A patent/DE1272288B/de active Pending
- 1966-10-10 IL IL26663A patent/IL26663A/xx unknown
- 1966-10-10 CH CH1454566A patent/CH481888A/de not_active IP Right Cessation
- 1966-10-12 FR FR79609A patent/FR1496435A/fr not_active Expired
- 1966-10-14 BE BE688260D patent/BE688260A/xx not_active IP Right Cessation
- 1966-10-14 SE SE14007/66A patent/SE338985B/xx unknown
- 1966-10-14 ES ES0332252A patent/ES332252A1/es not_active Expired
- 1966-10-14 NO NO165161A patent/NO125629B/no unknown
- 1966-10-17 DK DK535566AA patent/DK117701B/da unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE688260A (US07993877-20110809-P00003.png) | 1967-04-14 |
| IL26663A (en) | 1970-09-17 |
| NL6513426A (US07993877-20110809-P00003.png) | 1967-04-17 |
| DE1272288B (de) | 1968-07-11 |
| GB1138750A (en) | 1969-01-01 |
| CH481888A (de) | 1969-11-30 |
| AT265240B (de) | 1968-10-10 |
| DK117701B (da) | 1970-05-25 |
| FR1496435A (fr) | 1967-09-29 |
| NO125629B (US07993877-20110809-P00003.png) | 1972-10-09 |
| SE338985B (US07993877-20110809-P00003.png) | 1971-09-27 |
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