ES2729195T3 - Proceso para producir 1,1,2,3-tetracloropropeno a partir de 1,1,3-tricloropropeno y/o 3,3,3- tricloropropeno - Google Patents
Proceso para producir 1,1,2,3-tetracloropropeno a partir de 1,1,3-tricloropropeno y/o 3,3,3- tricloropropeno Download PDFInfo
- Publication number
- ES2729195T3 ES2729195T3 ES14754946T ES14754946T ES2729195T3 ES 2729195 T3 ES2729195 T3 ES 2729195T3 ES 14754946 T ES14754946 T ES 14754946T ES 14754946 T ES14754946 T ES 14754946T ES 2729195 T3 ES2729195 T3 ES 2729195T3
- Authority
- ES
- Spain
- Prior art keywords
- cstr
- reaction column
- trichloropropene
- hcc
- tubular reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000034 method Methods 0.000 title claims abstract description 22
- JFEVIPGMXQNRRF-UHFFFAOYSA-N 1,1,3-trichloroprop-1-ene Chemical compound ClCC=C(Cl)Cl JFEVIPGMXQNRRF-UHFFFAOYSA-N 0.000 title claims abstract description 6
- UMGQVBVEWTXECF-UHFFFAOYSA-N 1,1,2,3-tetrachloroprop-1-ene Chemical compound ClCC(Cl)=C(Cl)Cl UMGQVBVEWTXECF-UHFFFAOYSA-N 0.000 title claims abstract description 5
- VKEIPALYOJMDAC-UHFFFAOYSA-N 3,3,3-trichloroprop-1-ene Chemical compound ClC(Cl)(Cl)C=C VKEIPALYOJMDAC-UHFFFAOYSA-N 0.000 title claims abstract description 5
- 238000006243 chemical reaction Methods 0.000 claims abstract description 30
- 239000003054 catalyst Substances 0.000 claims abstract description 10
- 238000007033 dehydrochlorination reaction Methods 0.000 claims abstract description 5
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 4
- 239000000376 reactant Substances 0.000 claims abstract description 3
- 238000003786 synthesis reaction Methods 0.000 claims abstract description 3
- 239000000460 chlorine Substances 0.000 claims description 19
- 239000011368 organic material Substances 0.000 claims description 11
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 238000000746 purification Methods 0.000 claims description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 3
- 229910052801 chlorine Inorganic materials 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 2
- -1 iron halide compounds Chemical class 0.000 claims 2
- 150000001805 chlorine compounds Chemical class 0.000 claims 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- 239000012530 fluid Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- ZXPCCXXSNUIVNK-UHFFFAOYSA-N 1,1,1,2,3-pentachloropropane Chemical compound ClCC(Cl)C(Cl)(Cl)Cl ZXPCCXXSNUIVNK-UHFFFAOYSA-N 0.000 description 2
- FXRLMCRCYDHQFW-UHFFFAOYSA-N 2,3,3,3-tetrafluoropropene Chemical compound FC(=C)C(F)(F)F FXRLMCRCYDHQFW-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 239000012043 crude product Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000002274 desiccant Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/04—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361766405P | 2013-02-19 | 2013-02-19 | |
| US14/181,769 US8889929B2 (en) | 2013-02-19 | 2014-02-17 | Process to make 1,1,2,3-tetrachloropropene from 1,1,3-trichloropropene and/or 3,3,3-trichloropropene |
| PCT/US2014/016873 WO2014130445A1 (en) | 2013-02-19 | 2014-02-18 | Process to make 1,1,2,3-tetrachloropropene from 1,1,3-trichloropropene and/or 3,3,3- trichloropropene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2729195T3 true ES2729195T3 (es) | 2019-10-30 |
Family
ID=51351685
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES14754946T Active ES2729195T3 (es) | 2013-02-19 | 2014-02-18 | Proceso para producir 1,1,2,3-tetracloropropeno a partir de 1,1,3-tricloropropeno y/o 3,3,3- tricloropropeno |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US8889929B2 (enExample) |
| EP (1) | EP2958880B1 (enExample) |
| JP (1) | JP6364029B2 (enExample) |
| CN (1) | CN105073691A (enExample) |
| ES (1) | ES2729195T3 (enExample) |
| MX (1) | MX2015010687A (enExample) |
| WO (1) | WO2014130445A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9416073B2 (en) * | 2014-10-06 | 2016-08-16 | Honeywell International Inc. | Method to improve halogenation reactions |
| KR102606455B1 (ko) * | 2014-10-16 | 2023-11-29 | 스폴렉 프로 케미코우 어 허트니 비로부, 아크시오바 스폴렉노스트 | 공정 |
| TWI770558B (zh) | 2014-10-16 | 2022-07-11 | 捷克商史波克專業化學杭尼維洛普合股公司 | 用於製備高純度1,1,1,2,3-五氯丙烷產物之方法 |
| WO2016058568A1 (en) | 2014-10-16 | 2016-04-21 | Spolek Pro Chemickou A Hutni Vyrobu, Akciova Spolecnost | A process for producing highly pure chlorinated alkanes |
| WO2017028826A2 (en) | 2015-08-19 | 2017-02-23 | Spolek Pro Chemickou A Hutni Vyrobu, Akciova Spolecnost | Process for producing c3 chlorinated alkane and alkene compounds |
| US10546291B2 (en) * | 2015-09-09 | 2020-01-28 | Samsung Electronics Co., Ltd. | Method and apparatus for performing payment |
| US10793496B2 (en) | 2016-04-13 | 2020-10-06 | Spolek Pro Chemickou A Hutni Vyrobu A.S. | Process for producing a chlorinated alkane |
| KR20190008221A (ko) | 2016-04-13 | 2019-01-23 | 아르끄마 프랑스 | 2,3,3,3-테트라플루오로프로펜의 제조 방법 |
| CN109809959B (zh) | 2017-11-22 | 2021-10-01 | 江西天宇化工有限公司 | 一种1,1,1,2,3-五氯丙烷的制备方法 |
| US11118705B2 (en) | 2018-08-07 | 2021-09-14 | General Electric Company | Quick connect firewall seal for firewall |
| WO2020068119A1 (en) | 2018-09-28 | 2020-04-02 | General Electric Company | Method for manufacturing a telescoping wind turbine tower structure |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL160542C (nl) * | 1971-12-17 | 1979-11-15 | Monsanto Co | Werkwijze voor het bereiden van 1,1,2,3,-tetrachloorpro- peen. |
| US3926758A (en) | 1971-12-27 | 1975-12-16 | Monsanto Co | Preparation of 1,1,2,3-tetrachloropropene from 2,3-trichloropropane |
| US4535194A (en) | 1983-07-06 | 1985-08-13 | Monsanto Co. | Process for producing 1,1,2,3-tetrachloropropene |
| US4650914A (en) | 1983-07-06 | 1987-03-17 | Monsanto Company | Process for producing 1,1,2,3-tetrachloropropene |
| US5689020A (en) | 1996-03-11 | 1997-11-18 | Laroche Industries Inc. | High temperature chlorination process for the preparation of polychloroolefins |
| US8058486B2 (en) | 2004-04-29 | 2011-11-15 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
| US8258355B2 (en) * | 2007-07-25 | 2012-09-04 | Honeywell International Inc. | Processes for preparing 1,1,2,3-tetrachloropropene |
| US8115038B2 (en) | 2007-12-19 | 2012-02-14 | Occidental Chemical Corporation | Methods of making chlorinated hydrocarbons |
| JP5459320B2 (ja) | 2009-05-13 | 2014-04-02 | ダイキン工業株式会社 | 塩素含有フルオロカーボン化合物の製造方法 |
| EP2504299B1 (en) | 2009-11-27 | 2018-01-17 | Daikin Industries, Ltd. | Process for preparing 1,1,2,3-tetrachloropropene |
| US8889925B2 (en) | 2010-03-10 | 2014-11-18 | Arkema France | Process of fluorination in liquid phase |
| CN103717557A (zh) * | 2011-08-07 | 2014-04-09 | 陶氏环球技术有限责任公司 | 生产氯化的丙烯的方法 |
-
2014
- 2014-02-17 US US14/181,769 patent/US8889929B2/en active Active
- 2014-02-18 MX MX2015010687A patent/MX2015010687A/es unknown
- 2014-02-18 JP JP2015558905A patent/JP6364029B2/ja active Active
- 2014-02-18 ES ES14754946T patent/ES2729195T3/es active Active
- 2014-02-18 CN CN201480009084.3A patent/CN105073691A/zh active Pending
- 2014-02-18 WO PCT/US2014/016873 patent/WO2014130445A1/en not_active Ceased
- 2014-02-18 EP EP14754946.3A patent/EP2958880B1/en active Active
- 2014-10-07 US US14/508,207 patent/US8993816B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2958880A4 (en) | 2016-10-12 |
| JP6364029B2 (ja) | 2018-07-25 |
| CN105073691A (zh) | 2015-11-18 |
| EP2958880B1 (en) | 2019-04-10 |
| US8889929B2 (en) | 2014-11-18 |
| US20140235906A1 (en) | 2014-08-21 |
| US20150025282A1 (en) | 2015-01-22 |
| MX2015010687A (es) | 2015-12-16 |
| EP2958880A1 (en) | 2015-12-30 |
| WO2014130445A1 (en) | 2014-08-28 |
| US8993816B2 (en) | 2015-03-31 |
| JP2016511249A (ja) | 2016-04-14 |
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