ES2655507T3 - Método analítico para detectar marcadores de combustible - Google Patents

Método analítico para detectar marcadores de combustible Download PDF

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Publication number
ES2655507T3
ES2655507T3 ES14728762.7T ES14728762T ES2655507T3 ES 2655507 T3 ES2655507 T3 ES 2655507T3 ES 14728762 T ES14728762 T ES 14728762T ES 2655507 T3 ES2655507 T3 ES 2655507T3
Authority
ES
Spain
Prior art keywords
column
marker
capillary column
effluent stream
marker compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES14728762.7T
Other languages
English (en)
Spanish (es)
Inventor
Ronda L. GRAS
Jim C. LUONG
Warren E. SMITH
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Rohm and Haas Co
Original Assignee
Dow Global Technologies LLC
Rohm and Haas Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies LLC, Rohm and Haas Co filed Critical Dow Global Technologies LLC
Application granted granted Critical
Publication of ES2655507T3 publication Critical patent/ES2655507T3/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • G01N30/7206—Mass spectrometers interfaced to gas chromatograph
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/003—Marking, e.g. coloration by addition of pigments
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
    • G01N30/463—Flow patterns using more than one column with serial coupling of separation columns for multidimensional chromatography
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6052—Construction of the column body
    • G01N30/6073—Construction of the column body in open tubular form
    • G01N30/6078—Capillaries
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; Viscous liquids; Paints; Inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26—Oils; Viscous liquids; Paints; Inks
    • G01N33/28—Oils, i.e. hydrocarbon liquids
    • G01N33/2835—Specific substances contained in the oils or fuels
    • G01N33/2882—Markers
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N2030/042—Standards
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/884—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
    • G01N2030/8854—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving hydrocarbons
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
    • G01N30/465—Flow patterns using more than one column with serial coupling of separation columns with specially adapted interfaces between the columns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • G01N30/7233—Mass spectrometers interfaced to liquid or supercritical fluid chromatograph

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
ES14728762.7T 2013-05-02 2014-05-02 Método analítico para detectar marcadores de combustible Active ES2655507T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361818506P 2013-05-02 2013-05-02
US201361818506P 2013-05-02
PCT/US2014/036492 WO2014179646A1 (en) 2013-05-02 2014-05-02 Analytical method for detecting fuel markers

Publications (1)

Publication Number Publication Date
ES2655507T3 true ES2655507T3 (es) 2018-02-20

Family

ID=50896551

Family Applications (1)

Application Number Title Priority Date Filing Date
ES14728762.7T Active ES2655507T3 (es) 2013-05-02 2014-05-02 Método analítico para detectar marcadores de combustible

Country Status (10)

Country Link
US (1) US9759697B2 (enExample)
EP (1) EP2959290B1 (enExample)
JP (1) JP6360886B2 (enExample)
KR (1) KR102203505B1 (enExample)
CN (1) CN105593681B (enExample)
BR (1) BR112015026099B1 (enExample)
ES (1) ES2655507T3 (enExample)
MY (1) MY176136A (enExample)
TW (1) TWI591338B (enExample)
WO (1) WO2014179646A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB201517474D0 (en) * 2015-10-02 2015-11-18 Johnson Matthey Plc Identification of products
PL3504546T3 (pl) 2016-08-24 2022-05-09 United Color Manufacturing Inc. Sposób identyfikacji płynu węglowodorowego
US10414899B2 (en) 2016-11-30 2019-09-17 Dow Global Technologies Llc Markers for aqueous compositions
US10513594B2 (en) * 2016-11-30 2019-12-24 Dow Global Technologies Llc Markers for aqueous compositions
US10393724B2 (en) * 2017-05-23 2019-08-27 GM Global Technology Operations LLC Rapid identification of brake fluid
CA3073754C (en) * 2017-08-23 2025-02-11 United Color Manufacturing Inc. NITROGEN-BASED MARKER COMPOSITIONS, AND THEIR PROCESSES OF MANUFACTURE AND USE
JP6891772B2 (ja) * 2017-11-24 2021-06-18 株式会社島津製作所 マルチディメンジョナルガスクロマトグラフ
CN108318596B (zh) * 2018-01-24 2020-09-22 公安部物证鉴定中心 一种弹壳内挥发性有机含氮物质的检测方法
KR102241870B1 (ko) 2018-02-23 2021-04-16 주식회사 엘지화학 첨가제 분석을 위한 고속처리 가스 크로마토그래피 시스템 및 이를 이용한 분석방법
CN113176354A (zh) * 2021-04-16 2021-07-27 中国热带农业科学院橡胶研究所 一种检测高温热改性木材挥发性气味的方法

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JPS61225650A (ja) * 1985-03-29 1986-10-07 Nippon Oil & Fats Co Ltd 溶剤分析方法
US4675454A (en) * 1986-03-10 1987-06-23 Amoco Corporation Catalytic etherification of phenols to alkyl aryl ethers
US5268302A (en) * 1990-05-29 1993-12-07 Thermedics Inc. Selective, high speed detection of vapors with analysis of multiple GC-separated portions
AU640314B2 (en) * 1991-05-03 1993-08-19 Nalco Chemical Company Identification of liquid hydrocarbons using chemical markers
JP3247113B2 (ja) * 1992-01-29 2002-01-15 キング ザ セカンド アンダーソン，デビッド 非放射性同位体を用いて化学品を識別する方法
US5492555A (en) 1994-06-09 1996-02-20 Lovelace Biomedical & Environmental Research Institute, Inc. Automated two-dimensional interface for capillary gas chromatography
MXPA01011530A (es) * 2001-06-04 2004-04-21 Uziel Ben Itzhak Metodo y sistema para marcar un liquido.
US7530257B2 (en) 2002-09-27 2009-05-12 Honeywell International Inc. Phased micro analyzer VIII
US20050019939A1 (en) * 2003-07-25 2005-01-27 Dale Spall Combination marker for liquids and method identification thereof
CN1954208A (zh) * 2004-05-17 2007-04-25 弗门尼舍有限公司 新型多维气相色谱装置及使用多个冷却线连接件的分析物输送方法
US7858373B2 (en) * 2006-02-03 2010-12-28 Rohm And Haas Company Chemical markers
ATE466279T1 (de) * 2006-10-25 2010-05-15 Prad Res & Dev Ltd Kontaminierungsschätzung mit hoher genauigkeit in kohlenwasserstoffproben mit hilfe von gc x gc
US7823439B2 (en) * 2007-11-15 2010-11-02 Midwest Research Institute Method for identifying the composition of a sample
US8322189B2 (en) 2008-08-29 2012-12-04 Exxonmobil Research And Engineering Company Comprehensive two-dimensional gas chromatography method with one switching valve as the modulator
JP5332413B2 (ja) * 2008-09-02 2013-11-06 株式会社島津製作所 マルチディメンジョナルガスクロマトグラフ装置
WO2011032857A2 (de) * 2009-09-15 2011-03-24 Basf Se Verwendung von derivaten aromatischer verbindungen als markierstoffe für flüssigkeiten
FR2971254B1 (fr) * 2011-02-08 2014-05-30 Total Raffinage Marketing Compositions liquides pour marquer les carburants et combustibles hydrocarbones liquides, carburants et combustibles les contenant et procede de detection des marqueurs
JP2012177987A (ja) * 2011-02-25 2012-09-13 Nec Corp 監視システムおよび監視方法
CN102253149A (zh) * 2011-05-05 2011-11-23 辽宁省刑事科学技术研究所 对火案现场助燃剂中碳氢化合物及硫化物燃烧残留物同步分析方法
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US9341604B2 (en) * 2011-11-09 2016-05-17 The Regents Of The University Of Michigan Devices and methods for adaptive micro-gas chromatography

Also Published As

Publication number Publication date
KR102203505B1 (ko) 2021-01-15
JP6360886B2 (ja) 2018-07-18
EP2959290A1 (en) 2015-12-30
KR20160002878A (ko) 2016-01-08
BR112015026099A2 (pt) 2017-07-25
EP2959290B1 (en) 2017-12-06
TW201502510A (zh) 2015-01-16
CN105593681A (zh) 2016-05-18
US20160077066A1 (en) 2016-03-17
BR112015026099B1 (pt) 2020-05-05
WO2014179646A1 (en) 2014-11-06
CN105593681B (zh) 2018-01-30
US9759697B2 (en) 2017-09-12
TWI591338B (zh) 2017-07-11
JP2016522898A (ja) 2016-08-04
MY176136A (en) 2020-07-24

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