ES263202A1 - Procedimiento de obtenciën de ciclohexanona y ciclohexanol - Google Patents
Procedimiento de obtenciën de ciclohexanona y ciclohexanolInfo
- Publication number
- ES263202A1 ES263202A1 ES0263202A ES263202A ES263202A1 ES 263202 A1 ES263202 A1 ES 263202A1 ES 0263202 A ES0263202 A ES 0263202A ES 263202 A ES263202 A ES 263202A ES 263202 A1 ES263202 A1 ES 263202A1
- Authority
- ES
- Spain
- Prior art keywords
- alkaline solution
- cyclohexanol
- cyclohexanone
- inorganic salt
- oil phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 title abstract 2
- 230000003647 oxidation Effects 0.000 title abstract 2
- 238000007254 oxidation reaction Methods 0.000 title abstract 2
- 238000000746 purification Methods 0.000 title 1
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 8
- 239000012670 alkaline solution Substances 0.000 abstract 6
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 4
- 239000012071 phase Substances 0.000 abstract 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 abstract 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 2
- 238000005406 washing Methods 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 abstract 1
- 235000019270 ammonium chloride Nutrition 0.000 abstract 1
- 239000008346 aqueous phase Substances 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000010908 decantation Methods 0.000 abstract 1
- 230000003247 decreasing effect Effects 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000007935 neutral effect Effects 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 229940072033 potash Drugs 0.000 abstract 1
- 239000001103 potassium chloride Substances 0.000 abstract 1
- 235000011164 potassium chloride Nutrition 0.000 abstract 1
- 239000011698 potassium fluoride Substances 0.000 abstract 1
- 235000003270 potassium fluoride Nutrition 0.000 abstract 1
- 235000011118 potassium hydroxide Nutrition 0.000 abstract 1
- 235000010289 potassium nitrite Nutrition 0.000 abstract 1
- 239000004304 potassium nitrite Substances 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 235000015424 sodium Nutrition 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 235000011121 sodium hydroxide Nutrition 0.000 abstract 1
- 229910052938 sodium sulfate Inorganic materials 0.000 abstract 1
- 235000011152 sodium sulphate Nutrition 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US85910959A | 1959-12-14 | 1959-12-14 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES263202A1 true ES263202A1 (es) | 1961-04-01 |
Family
ID=25330056
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES0263202A Expired ES263202A1 (es) | 1959-12-14 | 1960-12-13 | Procedimiento de obtenciën de ciclohexanona y ciclohexanol |
Country Status (6)
Country | Link |
---|---|
BE (1) | BE598095A (en(2012)) |
CH (1) | CH397653A (en(2012)) |
ES (1) | ES263202A1 (en(2012)) |
GB (1) | GB972443A (en(2012)) |
LU (1) | LU39532A1 (en(2012)) |
NL (1) | NL259027A (en(2012)) |
-
0
- NL NL259027D patent/NL259027A/xx unknown
-
1960
- 1960-12-13 LU LU39532D patent/LU39532A1/xx unknown
- 1960-12-13 ES ES0263202A patent/ES263202A1/es not_active Expired
- 1960-12-13 BE BE598095A patent/BE598095A/fr unknown
- 1960-12-14 GB GB4308660A patent/GB972443A/en not_active Expired
- 1960-12-14 CH CH1396560A patent/CH397653A/fr unknown
Also Published As
Publication number | Publication date |
---|---|
BE598095A (fr) | 1961-03-31 |
NL259027A (en(2012)) | |
LU39532A1 (en(2012)) | 1961-02-14 |
GB972443A (en) | 1964-10-14 |
CH397653A (fr) | 1965-08-31 |
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