CH397653A - Procédé de purification d'un mélange impur de cyclohexanone et de cyclohexanol - Google Patents
Procédé de purification d'un mélange impur de cyclohexanone et de cyclohexanolInfo
- Publication number
- CH397653A CH397653A CH1396560A CH1396560A CH397653A CH 397653 A CH397653 A CH 397653A CH 1396560 A CH1396560 A CH 1396560A CH 1396560 A CH1396560 A CH 1396560A CH 397653 A CH397653 A CH 397653A
- Authority
- CH
- Switzerland
- Prior art keywords
- cyclohexanone
- cyclohexanol
- solution
- aqueous
- aqueous phase
- Prior art date
Links
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 title claims description 50
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 title claims description 19
- 239000000203 mixture Substances 0.000 title claims description 11
- 238000000034 method Methods 0.000 title claims description 9
- 238000000746 purification Methods 0.000 title claims description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 27
- 239000000243 solution Substances 0.000 claims description 18
- 238000005406 washing Methods 0.000 claims description 15
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical group [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 14
- 239000008346 aqueous phase Substances 0.000 claims description 14
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 13
- 235000011152 sodium sulphate Nutrition 0.000 claims description 13
- 239000012071 phase Substances 0.000 claims description 9
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
- 239000012670 alkaline solution Substances 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 229910017053 inorganic salt Inorganic materials 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 241000220225 Malus Species 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 3
- 239000007832 Na2SO4 Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US85910959A | 1959-12-14 | 1959-12-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH397653A true CH397653A (fr) | 1965-08-31 |
Family
ID=25330056
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH1396560A CH397653A (fr) | 1959-12-14 | 1960-12-14 | Procédé de purification d'un mélange impur de cyclohexanone et de cyclohexanol |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE598095A (en(2012)) |
| CH (1) | CH397653A (en(2012)) |
| ES (1) | ES263202A1 (en(2012)) |
| GB (1) | GB972443A (en(2012)) |
| LU (1) | LU39532A1 (en(2012)) |
| NL (1) | NL259027A (en(2012)) |
-
0
- NL NL259027D patent/NL259027A/xx unknown
-
1960
- 1960-12-13 LU LU39532D patent/LU39532A1/xx unknown
- 1960-12-13 ES ES0263202A patent/ES263202A1/es not_active Expired
- 1960-12-13 BE BE598095A patent/BE598095A/fr unknown
- 1960-12-14 GB GB4308660A patent/GB972443A/en not_active Expired
- 1960-12-14 CH CH1396560A patent/CH397653A/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE598095A (fr) | 1961-03-31 |
| NL259027A (en(2012)) | |
| LU39532A1 (en(2012)) | 1961-02-14 |
| GB972443A (en) | 1964-10-14 |
| ES263202A1 (es) | 1961-04-01 |
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