ES2357335T3 - Utilización de evaporadores de tubos helicoidales en la fabricación de poliamidas. - Google Patents
Utilización de evaporadores de tubos helicoidales en la fabricación de poliamidas. Download PDFInfo
- Publication number
- ES2357335T3 ES2357335T3 ES07821551T ES07821551T ES2357335T3 ES 2357335 T3 ES2357335 T3 ES 2357335T3 ES 07821551 T ES07821551 T ES 07821551T ES 07821551 T ES07821551 T ES 07821551T ES 2357335 T3 ES2357335 T3 ES 2357335T3
- Authority
- ES
- Spain
- Prior art keywords
- polyamide
- range
- extracts
- concentration
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000004519 manufacturing process Methods 0.000 title abstract description 7
- 239000004952 Polyamide Substances 0.000 claims abstract description 40
- 229920002647 polyamide Polymers 0.000 claims abstract description 40
- 229920002292 Nylon 6 Polymers 0.000 claims abstract description 30
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims abstract description 30
- 238000006243 chemical reaction Methods 0.000 claims abstract description 27
- 238000000605 extraction Methods 0.000 claims abstract description 22
- 239000007791 liquid phase Substances 0.000 claims abstract description 16
- 239000011541 reaction mixture Substances 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 12
- FHKPTEOFUHYQFY-UHFFFAOYSA-N 2-aminohexanenitrile Chemical compound CCCCC(N)C#N FHKPTEOFUHYQFY-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims description 30
- 239000012071 phase Substances 0.000 claims description 28
- 239000000284 extract Substances 0.000 claims description 27
- 239000007864 aqueous solution Substances 0.000 claims description 17
- 239000007789 gas Substances 0.000 claims description 14
- 239000000049 pigment Substances 0.000 claims description 8
- 238000000926 separation method Methods 0.000 claims description 8
- 238000001704 evaporation Methods 0.000 claims description 7
- 230000008020 evaporation Effects 0.000 claims description 7
- 238000005469 granulation Methods 0.000 claims description 7
- 230000003179 granulation Effects 0.000 claims description 7
- LRQKBLKVPFOOQJ-UHFFFAOYSA-N 2-aminohexanoic acid Chemical compound CCCCC(N)C(O)=O LRQKBLKVPFOOQJ-UHFFFAOYSA-N 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 4
- 239000012159 carrier gas Substances 0.000 claims description 2
- 239000006286 aqueous extract Substances 0.000 abstract description 5
- 239000007792 gaseous phase Substances 0.000 abstract description 4
- 239000012141 concentrate Substances 0.000 abstract description 2
- 230000002051 biphasic effect Effects 0.000 abstract 2
- SLXKOJJOQWFEFD-UHFFFAOYSA-N 6-aminohexanoic acid Chemical compound NCCCCCC(O)=O SLXKOJJOQWFEFD-UHFFFAOYSA-N 0.000 abstract 1
- 229960002684 aminocaproic acid Drugs 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 33
- 150000003951 lactams Chemical class 0.000 description 11
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 238000006116 polymerization reaction Methods 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 6
- 239000000178 monomer Substances 0.000 description 6
- 239000003643 water by type Substances 0.000 description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 5
- 150000001991 dicarboxylic acids Chemical class 0.000 description 5
- 230000005484 gravity Effects 0.000 description 5
- -1 likewise Chemical compound 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 4
- 229960000250 adipic acid Drugs 0.000 description 4
- 239000002585 base Substances 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- 150000004985 diamines Chemical class 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 239000002638 heterogeneous catalyst Substances 0.000 description 3
- 229910044991 metal oxide Inorganic materials 0.000 description 3
- 150000004706 metal oxides Chemical class 0.000 description 3
- 239000012074 organic phase Substances 0.000 description 3
- 238000004062 sedimentation Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000012808 vapor phase Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910052787 antimony Inorganic materials 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- VHRGRCVQAFMJIZ-UHFFFAOYSA-N cadaverine Chemical compound NCCCCCN VHRGRCVQAFMJIZ-UHFFFAOYSA-N 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000000539 dimer Substances 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- WLJVNTCWHIRURA-UHFFFAOYSA-N pimelic acid Chemical compound OC(=O)CCCCCC(O)=O WLJVNTCWHIRURA-UHFFFAOYSA-N 0.000 description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- KIDHWZJUCRJVML-UHFFFAOYSA-N putrescine Chemical compound NCCCCN KIDHWZJUCRJVML-UHFFFAOYSA-N 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- PWGJDPKCLMLPJW-UHFFFAOYSA-N 1,8-diaminooctane Chemical compound NCCCCCCCCN PWGJDPKCLMLPJW-UHFFFAOYSA-N 0.000 description 1
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 1
- FTVFPPFZRRKJIH-UHFFFAOYSA-N 2,2,6,6-tetramethylpiperidin-4-amine Chemical compound CC1(C)CC(N)CC(C)(C)N1 FTVFPPFZRRKJIH-UHFFFAOYSA-N 0.000 description 1
- 241001550224 Apha Species 0.000 description 1
- 229910052582 BN Inorganic materials 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- 229920002302 Nylon 6,6 Polymers 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000001361 adipic acid Substances 0.000 description 1
- 235000011037 adipic acid Nutrition 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910001508 alkali metal halide Inorganic materials 0.000 description 1
- 150000008045 alkali metal halides Chemical class 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000002956 ash Substances 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- YQLZOAVZWJBZSY-UHFFFAOYSA-N decane-1,10-diamine Chemical compound NCCCCCCCCCCN YQLZOAVZWJBZSY-UHFFFAOYSA-N 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000010494 dissociation reaction Methods 0.000 description 1
- 230000005593 dissociations Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- PWSKHLMYTZNYKO-UHFFFAOYSA-N heptane-1,7-diamine Chemical compound NCCCCCCCN PWSKHLMYTZNYKO-UHFFFAOYSA-N 0.000 description 1
- 239000004611 light stabiliser Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 235000012243 magnesium silicates Nutrition 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/02—Evaporators with heating coils
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/04—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
- C08G69/18—Anionic polymerisation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/46—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyamides (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP06122862 | 2006-10-24 | ||
| EP06122862 | 2006-10-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2357335T3 true ES2357335T3 (es) | 2011-04-25 |
Family
ID=38941907
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES07821551T Active ES2357335T3 (es) | 2006-10-24 | 2007-10-19 | Utilización de evaporadores de tubos helicoidales en la fabricación de poliamidas. |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US8263733B2 (enExample) |
| EP (1) | EP2084212B1 (enExample) |
| JP (1) | JP5312338B2 (enExample) |
| KR (1) | KR101444965B1 (enExample) |
| CN (1) | CN101528811B (enExample) |
| AT (1) | ATE492584T1 (enExample) |
| BR (1) | BRPI0718502B1 (enExample) |
| CA (1) | CA2666422A1 (enExample) |
| DE (1) | DE502007006056D1 (enExample) |
| ES (1) | ES2357335T3 (enExample) |
| MX (1) | MX2009004018A (enExample) |
| PL (1) | PL2084212T3 (enExample) |
| WO (1) | WO2008049786A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5661616B2 (ja) * | 2008-06-20 | 2015-01-28 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | ポリアミドペレットの多段階乾燥及び後縮合を連続的に行う方法 |
| WO2010066769A2 (de) | 2008-12-12 | 2010-06-17 | Basf Se | Verfahren zur kontinuierlichen herstellung von copolyamiden aus lactamen und salzen aus diaminen und dicarbonsäuren |
| CN101786987B (zh) * | 2010-03-23 | 2011-08-17 | 清华大学 | 一种己内酰胺萃取设备 |
| EP2682417A1 (de) * | 2012-07-06 | 2014-01-08 | Basf Se | Verfahren zur Reinigung von Polyamidteilchen |
| SI2725052T1 (sl) * | 2012-10-23 | 2019-06-28 | Uhde Inventa-Fischer Gmbh | Repolimerizacijska naprava |
| PL2725051T3 (pl) * | 2012-10-23 | 2015-08-31 | Uhde Inventa Fischer Gmbh | Ciągły sposób wytwarzania poliamidu 6 i urządzenia do tego celu |
| ES2564676T3 (es) * | 2013-03-26 | 2016-03-28 | Uhde Inventa-Fischer Gmbh | Procedimiento y dispositivo para la devolución continua de aguas de extracción en el proceso de preparación de poliamida |
| TW201502163A (zh) * | 2013-05-01 | 2015-01-16 | Invista Tech Sarl | 包含多重後段製程之聚醯胺合成 |
| CN111100287B (zh) * | 2018-10-26 | 2023-01-20 | 中国石油化工股份有限公司 | 一种生产高粘度聚酰胺的方法 |
| JP2023550514A (ja) | 2020-11-24 | 2023-12-01 | ベーアーエスエフ・エスエー | ラクタム、ジアミンおよびダイマー酸からコポリアミドを連続的に調製する方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2443566A1 (de) * | 1974-09-12 | 1976-04-01 | Basf Ag | Verfahren zum kontinuierlichen herstellen von polyamiden |
| DE3311260A1 (de) * | 1983-03-28 | 1984-10-04 | Basf Ag, 6700 Ludwigshafen | Verfahren zum kontinuierlichen eindampfen von caprolactam und dessen oligomere enthaltenden waessrigen loesungen |
| DE3710803A1 (de) | 1987-03-31 | 1988-10-20 | Basf Ag | Verfahren zur entfernung von caprolactam und dessen oligomeren aus solches enthaltendem polyamidgranulat |
| US5077381A (en) * | 1990-06-01 | 1991-12-31 | Basf Corporation | Constant compositioin recycle of nylon 6 polymerization wash water |
| DE4321683A1 (de) | 1993-06-30 | 1995-01-12 | Basf Ag | Verfahren zum kontinuierlichen Herstellen von niedermolekularen Polyamiden |
| DE19519819A1 (de) * | 1995-05-31 | 1996-12-05 | Bayer Ag | Verfahren zur Wiederverwertung von wäßrigen Extraktlösungen, die bei der Herstellung von PA 6 oder Copolyamiden anfallen |
| DE19531990A1 (de) * | 1995-08-30 | 1997-05-15 | Polymer Eng Gmbh | Verfahren zur kontinuierlichen Herstellung von Polyamid 6 unter Verwendung von Rücklactam |
| JPH09188758A (ja) * | 1995-11-06 | 1997-07-22 | Mitsubishi Chem Corp | カプロラクタムよりポリアミド樹脂を製造する方法 |
| BR9814444A (pt) * | 1997-08-28 | 2001-10-23 | Du Pont | Processo para a preparação de pré-polìmeros de poliamida, processo para a preparação de polìmero de poliamida, processo para processamento rápido de fase sólida e extração em fase de vapor de impurezas de polìmeros de poliamida e produto |
| DE19804020A1 (de) * | 1998-02-02 | 1999-08-05 | Basf Ag | Verfahren zur Herstellung von Polyamiden aus Aminonitrilen |
| DE19808190A1 (de) | 1998-02-26 | 1999-09-02 | Basf Ag | Verfahren zur Herstellung von Polyamiden |
| DE19925906A1 (de) * | 1999-06-07 | 2000-12-14 | Basf Ag | Verfahren zur Herstellung von Polyamiden aus Lactamen und Polyamid-Extrakten |
| DE19962573A1 (de) * | 1999-12-23 | 2001-07-05 | Basf Ag | Verfahren zur Herstellung von Polyamiden |
| DE10335451A1 (de) * | 2003-08-02 | 2005-03-10 | Bayer Materialscience Ag | Verfahren zur Entfernung von flüchtigen Verbindungen aus Stoffgemischen mittels Mikroverdampfer |
| JP2005162927A (ja) * | 2003-12-04 | 2005-06-23 | Mitsubishi Chemicals Corp | カプロラクタムよりポリアミド樹脂を製造する方法 |
-
2007
- 2007-10-19 KR KR1020097008273A patent/KR101444965B1/ko not_active Expired - Fee Related
- 2007-10-19 CN CN2007800397033A patent/CN101528811B/zh not_active Expired - Fee Related
- 2007-10-19 MX MX2009004018A patent/MX2009004018A/es active IP Right Grant
- 2007-10-19 WO PCT/EP2007/061187 patent/WO2008049786A1/de not_active Ceased
- 2007-10-19 JP JP2009533795A patent/JP5312338B2/ja not_active Expired - Fee Related
- 2007-10-19 AT AT07821551T patent/ATE492584T1/de active
- 2007-10-19 DE DE502007006056T patent/DE502007006056D1/de active Active
- 2007-10-19 BR BRPI0718502-2A patent/BRPI0718502B1/pt not_active IP Right Cessation
- 2007-10-19 PL PL07821551T patent/PL2084212T3/pl unknown
- 2007-10-19 EP EP07821551A patent/EP2084212B1/de active Active
- 2007-10-19 ES ES07821551T patent/ES2357335T3/es active Active
- 2007-10-19 CA CA002666422A patent/CA2666422A1/en not_active Abandoned
- 2007-10-19 US US12/446,274 patent/US8263733B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE502007006056D1 (de) | 2011-02-03 |
| KR101444965B1 (ko) | 2014-09-26 |
| KR20090083345A (ko) | 2009-08-03 |
| ATE492584T1 (de) | 2011-01-15 |
| MX2009004018A (es) | 2009-04-27 |
| BRPI0718502A2 (pt) | 2013-12-03 |
| BRPI0718502B1 (pt) | 2018-06-26 |
| WO2008049786A1 (de) | 2008-05-02 |
| JP5312338B2 (ja) | 2013-10-09 |
| EP2084212A1 (de) | 2009-08-05 |
| CA2666422A1 (en) | 2008-05-02 |
| CN101528811A (zh) | 2009-09-09 |
| US20100317810A1 (en) | 2010-12-16 |
| US8263733B2 (en) | 2012-09-11 |
| EP2084212B1 (de) | 2010-12-22 |
| CN101528811B (zh) | 2012-01-18 |
| PL2084212T3 (pl) | 2011-05-31 |
| JP2010507701A (ja) | 2010-03-11 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES2357335T3 (es) | Utilización de evaporadores de tubos helicoidales en la fabricación de poliamidas. | |
| ES2373182T3 (es) | Procedimiento de preparación de poliamida. | |
| RU2144048C1 (ru) | Способ непрерывного получения полиамидов, способ получения высокомолекулярного поликапролактама и поликапролактам с молекулярным весом 3000-14000 г/моль | |
| ES2392572T3 (es) | Procedimiento para la obtención de poliamidas | |
| ES2444766T3 (es) | Método para la producción de poliamida | |
| KR101289551B1 (ko) | 폴리아미드 제조 방법 | |
| KR20110110164A (ko) | 락탐 및 디아민과 디카르복실산의 염으로부터 코폴리아미드의 연속 제조 방법 | |
| AU745310B2 (en) | Process for preparing polyamides | |
| US6759505B2 (en) | Single-phase or multi-phase continuous polyamide polymerization processes | |
| ES2198313T3 (es) | Procedimiento para la preparacion de poliamidas a partir de lactamas y extractos de poliamida. | |
| TW412551B (en) | Preparation of polyamides from one lactam with or without further monomers and customary additives and fillers | |
| US5030709A (en) | Continuous preparation of copolyamides | |
| US5051491A (en) | Process for the preparation of a linear polyamide having ether bridges in the polymer chain | |
| BR112012027871B1 (pt) | processo de fabricação de poliamida | |
| JP2008081634A (ja) | ポリアミドプレポリマーおよびポリアミドの製造方法 | |
| US4994550A (en) | Process for the continuous preparation of nylon 4,6 from aqueous salt solution | |
| JP2008080267A (ja) | 複合式熱交換型反応器およびそれを用いたポリカプロアミドプレポリマーの製造方法 | |
| JP2023550514A (ja) | ラクタム、ジアミンおよびダイマー酸からコポリアミドを連続的に調製する方法 | |
| JP2002060486A (ja) | ポリアミドの製造方法 | |
| JPH09316193A (ja) | ポリアミドの製造方法 | |
| JPH09316192A (ja) | ポリアミドの製造方法 |