ES2191646T3 - Procedimiento para la obtencion de cloruros de 3,5-bis-(trifluormetil)-benzoilo y nuevos halogenuros de 3,5-bis-(trihalogenometil)- y (3,5)-dimetilbenzoilo. - Google Patents
Procedimiento para la obtencion de cloruros de 3,5-bis-(trifluormetil)-benzoilo y nuevos halogenuros de 3,5-bis-(trihalogenometil)- y (3,5)-dimetilbenzoilo.Info
- Publication number
- ES2191646T3 ES2191646T3 ES01101158T ES01101158T ES2191646T3 ES 2191646 T3 ES2191646 T3 ES 2191646T3 ES 01101158 T ES01101158 T ES 01101158T ES 01101158 T ES01101158 T ES 01101158T ES 2191646 T3 ES2191646 T3 ES 2191646T3
- Authority
- ES
- Spain
- Prior art keywords
- bis
- new
- obtaining
- procedure
- trihalogenometil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title 1
- 210000005100 blood-tumour barrier Anatomy 0.000 abstract 3
- WAKMMQSMEDJRRI-UHFFFAOYSA-N 3,5-bis(trifluoromethyl)benzoyl chloride Chemical class FC(F)(F)C1=CC(C(Cl)=O)=CC(C(F)(F)F)=C1 WAKMMQSMEDJRRI-UHFFFAOYSA-N 0.000 abstract 2
- -1 3,5-dimethylbenzoyl halides Chemical class 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 2
- LJMNEQZBOODJQR-UHFFFAOYSA-N 2-(trichloromethyl)benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1C(Cl)(Cl)Cl LJMNEQZBOODJQR-UHFFFAOYSA-N 0.000 abstract 1
- UMVOQQDNEYOJOK-UHFFFAOYSA-N 3,5-dimethylbenzoic acid Chemical class CC1=CC(C)=CC(C(O)=O)=C1 UMVOQQDNEYOJOK-UHFFFAOYSA-N 0.000 abstract 1
- 239000003905 agrochemical Substances 0.000 abstract 1
- 150000004820 halides Chemical class 0.000 abstract 1
- 239000000543 intermediate Substances 0.000 abstract 1
- 239000013067 intermediate product Substances 0.000 abstract 1
- 239000011968 lewis acid catalyst Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229920002120 photoresistant polymer Polymers 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/68—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings containing halogen
- C07C63/70—Monocarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/62—Preparation of carboxylic acid halides by reactions not involving the carboxylic acid halide group
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Procedimiento para la obtención de cloruros de 3, 5 - bis - (triflúormetil) - benzoilo y nuevos halogenuros de 3, 5 - bis - (trihalogenometil) - y 3, 5 - dimetilbenzoilo. La presente invención se refiere a un procedimiento para la obtencion de cloruros de 3, 5 - bis - (triflúormetil) - benzoilo a partir de los correspondientes ácidos 3, 5 - dimetilbenzoicos y a los nuevos halogenuros de 3, 5 - bis - (trihalógenometil) - y de 3, 5 - dimetilbenzoilo, que se presentan en este caso como productos intermedios. A continuación se designarán también como BTB los cloruros de 3, 5 - bis - (triflúormetil) - benzoilo. Los BTB son productos intermedios para la obtención de productos activos farmacéuticos y agroquímicos así como de composiciones fotorresistentes. Se conoce la obtención de los BTB a partir del correspondiente cloruro de triclorometil - benzoilo en presencia de ácido fluorhídrico y de un catalizador de ácido de Lewis.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10004717A DE10004717A1 (de) | 2000-02-03 | 2000-02-03 | V.z.H.v.3,5-Bis-(trifluormethyl)-benzoylchloriden u.neue 3,5-Dimethyl-benzoylchloride u.3,5-Bis-(trichlormethyl)-benzoylchloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2191646T3 true ES2191646T3 (es) | 2003-09-16 |
Family
ID=7629689
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES01101158T Expired - Lifetime ES2191646T3 (es) | 2000-02-03 | 2001-01-23 | Procedimiento para la obtencion de cloruros de 3,5-bis-(trifluormetil)-benzoilo y nuevos halogenuros de 3,5-bis-(trihalogenometil)- y (3,5)-dimetilbenzoilo. |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US6420601B2 (es) |
| EP (1) | EP1125913B1 (es) |
| JP (1) | JP2001294551A (es) |
| KR (1) | KR20010078281A (es) |
| CN (1) | CN1216028C (es) |
| AT (1) | ATE236868T1 (es) |
| CA (1) | CA2333444A1 (es) |
| CZ (1) | CZ2001416A3 (es) |
| DE (2) | DE10004717A1 (es) |
| DK (1) | DK1125913T3 (es) |
| ES (1) | ES2191646T3 (es) |
| HU (1) | HUP0100512A2 (es) |
| IL (1) | IL141197A0 (es) |
| MX (1) | MXPA01001319A (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003321406A (ja) * | 2002-04-30 | 2003-11-11 | Mitsubishi Gas Chem Co Inc | 高純度フルオロアルキルベンゼン誘導体及びその製造法 |
| CN101973865A (zh) * | 2010-09-14 | 2011-02-16 | 华东理工大学 | 利用环境污染物四氯化碳将羧酸氯化为相应酰氯的方法 |
| JP6311946B2 (ja) | 2013-09-13 | 2018-04-18 | ファイニングス シーオー． エルティーディーＦｉｎｉｎｇｓ Ｃｏ． Ｌｔｄ | トリクロロメチル置換ベンゼンを調製するための方法 |
| CN105384640B (zh) * | 2015-10-26 | 2017-07-04 | 安徽广信农化股份有限公司 | 一种对硝基苯甲酰氯的尾气处理工艺 |
| CN107400052B (zh) * | 2017-07-21 | 2020-05-01 | 淄博飞源化工有限公司 | 一种邻、间、对-三氟甲基苯甲酸甲酯的合成方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR820696A (fr) * | 1936-04-17 | 1937-11-16 | Ig Farbenindustrie Ag | Chlorures d'acides benzène-carboxyliques contenant des groupes trichloro-méthyliques et procédé de préparation de ces composés |
| DE707955C (de) * | 1936-04-19 | 1941-07-08 | I G Farbenindustrie Akt Ges | Verfahren zur Darstellung von fluorhaltigen Benzolcarbonsaeurederivaten |
| US4500471A (en) * | 1980-04-16 | 1985-02-19 | Occidental Chemical Corporation | Preparation of trifluoromethyl-benzoyl halides |
-
2000
- 2000-02-03 DE DE10004717A patent/DE10004717A1/de not_active Withdrawn
-
2001
- 2001-01-23 DE DE50100142T patent/DE50100142D1/de not_active Expired - Fee Related
- 2001-01-23 EP EP01101158A patent/EP1125913B1/de not_active Expired - Lifetime
- 2001-01-23 ES ES01101158T patent/ES2191646T3/es not_active Expired - Lifetime
- 2001-01-23 AT AT01101158T patent/ATE236868T1/de not_active IP Right Cessation
- 2001-01-23 DK DK01101158T patent/DK1125913T3/da active
- 2001-01-25 US US09/769,797 patent/US6420601B2/en not_active Expired - Fee Related
- 2001-01-30 JP JP2001021329A patent/JP2001294551A/ja not_active Withdrawn
- 2001-01-31 CA CA002333444A patent/CA2333444A1/en not_active Abandoned
- 2001-01-31 IL IL14119701A patent/IL141197A0/xx unknown
- 2001-02-01 CZ CZ2001416A patent/CZ2001416A3/cs unknown
- 2001-02-02 HU HU0100512A patent/HUP0100512A2/hu unknown
- 2001-02-02 KR KR1020010005053A patent/KR20010078281A/ko not_active Application Discontinuation
- 2001-02-02 MX MXPA01001319A patent/MXPA01001319A/es not_active Application Discontinuation
- 2001-02-05 CN CN011032103A patent/CN1216028C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| HUP0100512A2 (hu) | 2002-05-29 |
| KR20010078281A (ko) | 2001-08-20 |
| CA2333444A1 (en) | 2001-08-03 |
| CZ2001416A3 (cs) | 2001-09-12 |
| DE50100142D1 (de) | 2003-05-15 |
| DE10004717A1 (de) | 2001-08-09 |
| ATE236868T1 (de) | 2003-04-15 |
| US6420601B2 (en) | 2002-07-16 |
| US20010014759A1 (en) | 2001-08-16 |
| IL141197A0 (en) | 2002-02-10 |
| MXPA01001319A (es) | 2002-08-06 |
| DK1125913T3 (da) | 2003-07-21 |
| CN1308050A (zh) | 2001-08-15 |
| CN1216028C (zh) | 2005-08-24 |
| EP1125913B1 (de) | 2003-04-09 |
| EP1125913A1 (de) | 2001-08-22 |
| HU0100512D0 (en) | 2001-04-28 |
| JP2001294551A (ja) | 2001-10-23 |
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