ES2089152T3 - Procedimiento de purificacion de acetato de metilo. - Google Patents

Procedimiento de purificacion de acetato de metilo.

Info

Publication number
ES2089152T3
ES2089152T3 ES91310620T ES91310620T ES2089152T3 ES 2089152 T3 ES2089152 T3 ES 2089152T3 ES 91310620 T ES91310620 T ES 91310620T ES 91310620 T ES91310620 T ES 91310620T ES 2089152 T3 ES2089152 T3 ES 2089152T3
Authority
ES
Spain
Prior art keywords
distillation
water
methyl acetate
ester
phase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES91310620T
Other languages
English (en)
Inventor
Mark O Scates
Russel K Gibbs Jr
G Paull Torrence
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CNA Holdings LLC
Original Assignee
Hoechst Celanese Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Celanese Corp filed Critical Hoechst Celanese Corp
Application granted granted Critical
Publication of ES2089152T3 publication Critical patent/ES2089152T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/41—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrogenolysis or reduction of carboxylic groups or functional derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

ESTERES TALES COMO EL ACETATO DE METIL QUE CONTENGAN IMPUREZAS DE CARBONIL INCLUYENDO ALDEHIDOS, SE PURIFICAN MEDIANTE LA ADICION A LOS ESTERES DE UN COMPUESTO AMINO QUE REACCIONA CON LOS CARBONILES PARA FORMAR DERIVADOS NITROGENACEOS SOLUBLES EN AGUA, LA SEPARACION DE LA FASE DEL ESTER ORGANICO DE LA FASE DEL DERIVADO ACUOSO, Y LA DESTILACION DE LA FASE DEL ESTER PARA SEPARAR LAS IMPUREZAS MAS PESADAS. LA FORMACION DE NITRILO A PARTIR DE LOS DERIVADOS NITROGENACEOS SE MINIMIZA MEDIANTE LA ADICION DE AGUA A LA COLUMNA DE DESTILACION O LAVANDO LOS FONDOS ACUOSOS DE LA DESTILACION CON AGUA PARA, DE ESTA FORMA, SEPARAR LOS DERIVADOS DE CUALQUIER ESTER CONTENIDO EN EL FONDO. LA FASE ORGANICA RECUERADA DEL FONDO PUEDE RECICLARSE POR DESTILACION PARA RECUPERAR EL ESTER.
ES91310620T 1990-11-19 1991-11-18 Procedimiento de purificacion de acetato de metilo. Expired - Lifetime ES2089152T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/615,939 US5206434A (en) 1990-11-19 1990-11-19 Purification process for methyl acetate

Publications (1)

Publication Number Publication Date
ES2089152T3 true ES2089152T3 (es) 1996-10-01

Family

ID=24467400

Family Applications (1)

Application Number Title Priority Date Filing Date
ES91310620T Expired - Lifetime ES2089152T3 (es) 1990-11-19 1991-11-18 Procedimiento de purificacion de acetato de metilo.

Country Status (14)

Country Link
US (1) US5206434A (es)
EP (1) EP0487285B1 (es)
JP (1) JP2928003B2 (es)
KR (1) KR100191079B1 (es)
CN (1) CN1029845C (es)
AU (1) AU8790291A (es)
BR (1) BR9104987A (es)
CA (1) CA2055551A1 (es)
DE (1) DE69120508T2 (es)
ES (1) ES2089152T3 (es)
NO (1) NO914506L (es)
NZ (1) NZ240632A (es)
TW (1) TW198020B (es)
ZA (1) ZA919152B (es)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW283702B (es) * 1993-07-08 1996-08-21 Daicel Chem
EP0952141B1 (en) 1998-04-25 2002-06-05 BP Chemicals Limited Purification process
US6211405B1 (en) 1998-10-23 2001-04-03 Celanese International Corporation Addition of iridium to the rhodium/inorganic iodide catalyst system
US7115772B2 (en) * 2002-01-11 2006-10-03 Celanese International Corporation Integrated process for producing carbonylation acetic acid, acetic anhydride, or coproduction of each from a methyl acetate by-product stream
US7390919B1 (en) * 2007-10-01 2008-06-24 Lyondell Chemical Technology, L.P. Methyl acetate purification and carbonylation
US8858659B2 (en) * 2010-02-02 2014-10-14 Celanese International Corporation Processes for producing denatured ethanol
US8460405B2 (en) 2010-02-02 2013-06-11 Celanese International Corporation Ethanol compositions
US8747492B2 (en) 2010-02-02 2014-06-10 Celanese International Corporation Ethanol/fuel blends for use as motor fuels
US8668750B2 (en) 2010-02-02 2014-03-11 Celanese International Corporation Denatured fuel ethanol compositions for blending with gasoline or diesel fuel for use as motor fuels
US8541633B2 (en) * 2010-02-02 2013-09-24 Celanese International Corporation Processes for producing anhydrous ethanol compositions
US8728179B2 (en) 2010-02-02 2014-05-20 Celanese International Corporation Ethanol compositions
US8932372B2 (en) 2010-02-02 2015-01-13 Celanese International Corporation Integrated process for producing alcohols from a mixed acid feed
US8697802B2 (en) 2011-11-28 2014-04-15 Celanese International Corporation Process for producing polyvinyl alcohol or a copolymer thereof
US8703868B2 (en) 2011-11-28 2014-04-22 Celanese International Corporation Integrated process for producing polyvinyl alcohol or a copolymer thereof and ethanol
US8853469B2 (en) 2012-11-20 2014-10-07 Celanese International Corporation Combined column for separating products of different hydrogenation reactors
CN109369393A (zh) * 2018-10-26 2019-02-22 洪湖市泰科技有限公司 草铵膦工艺副产物乙酸乙酯粗品的无害化处理回收方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1963968A (en) * 1932-02-16 1934-06-26 Du Pont Purification of esters
US2770644A (en) * 1954-12-29 1956-11-13 Monsanto Chemicals Purification of acrylonitrile
US3578689A (en) * 1969-01-10 1971-05-11 Ethyl Corp Ester purification process
US4252748A (en) * 1978-12-29 1981-02-24 Halcon Research And Development Corporation Recovery of acetone produced by carbonylation
EP0070180B1 (en) * 1981-07-13 1985-09-25 Mitsubishi Gas Chemical Company, Inc. Process for producing acetic anhydride

Also Published As

Publication number Publication date
AU8790291A (en) 1992-05-21
ZA919152B (en) 1993-05-19
EP0487285A3 (en) 1993-04-28
JPH04266847A (ja) 1992-09-22
EP0487285A2 (en) 1992-05-27
NO914506D0 (no) 1991-11-18
CA2055551A1 (en) 1992-05-20
KR100191079B1 (ko) 1999-06-15
US5206434A (en) 1993-04-27
EP0487285B1 (en) 1996-06-26
NO914506L (no) 1992-05-20
BR9104987A (pt) 1992-06-23
CN1029845C (zh) 1995-09-27
DE69120508T2 (de) 1996-12-05
DE69120508D1 (de) 1996-08-01
KR920009761A (ko) 1992-06-25
TW198020B (es) 1993-01-11
CN1061590A (zh) 1992-06-03
NZ240632A (en) 1993-05-26
JP2928003B2 (ja) 1999-07-28

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