EP3797898B1 - Formflussmittel und verwendung davon - Google Patents
Formflussmittel und verwendung davon Download PDFInfo
- Publication number
- EP3797898B1 EP3797898B1 EP19199984.6A EP19199984A EP3797898B1 EP 3797898 B1 EP3797898 B1 EP 3797898B1 EP 19199984 A EP19199984 A EP 19199984A EP 3797898 B1 EP3797898 B1 EP 3797898B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- mould flux
- mould
- present
- sio
- flux
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 230000004907 flux Effects 0.000 title claims description 52
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 36
- 229910052681 coesite Inorganic materials 0.000 claims description 18
- 229910052906 cristobalite Inorganic materials 0.000 claims description 18
- 239000000377 silicon dioxide Substances 0.000 claims description 18
- 229910052682 stishovite Inorganic materials 0.000 claims description 18
- 229910052905 tridymite Inorganic materials 0.000 claims description 18
- 229910045601 alloy Inorganic materials 0.000 claims description 15
- 239000000956 alloy Substances 0.000 claims description 15
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 13
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 12
- 229910052593 corundum Inorganic materials 0.000 claims description 12
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 12
- 239000011734 sodium Substances 0.000 claims description 10
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 claims description 7
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 5
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims description 5
- 239000010433 feldspar Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- NOTVAPJNGZMVSD-UHFFFAOYSA-N potassium monoxide Inorganic materials [K]O[K] NOTVAPJNGZMVSD-UHFFFAOYSA-N 0.000 claims description 4
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 13
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 13
- 239000000292 calcium oxide Substances 0.000 description 12
- 230000015572 biosynthetic process Effects 0.000 description 10
- 239000010936 titanium Substances 0.000 description 10
- 239000002585 base Substances 0.000 description 9
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 5
- 239000000395 magnesium oxide Substances 0.000 description 5
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 5
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 5
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 229910000990 Ni alloy Inorganic materials 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 229910052664 nepheline Inorganic materials 0.000 description 1
- 239000010434 nepheline Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/10—Supplying or treating molten metal
- B22D11/108—Feeding additives, powders, or the like
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21C—PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- C21C7/00—Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
- C21C7/10—Handling in a vacuum
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21C—PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- C21C7/00—Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
- C21C7/0037—Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00 by injecting powdered material
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21C—PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- C21C7/00—Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
- C21C7/0075—Treating in a ladle furnace, e.g. up-/reheating of molten steel within the ladle
Definitions
- the present disclosure relates to a mould flux and to a method of manufacturing a nickel-base alloy.
- KR2019009901 relates to a flux to be employed by casting of steels, said flux comprising SiO 2 37.6-39.6 wt%, CaO 27.2-29.2 wt %, MgO 2.6-3.6 wt%, Al 2 O 3 1-3 wt %, Na 2 O 15.1-16.1 wt%, K 2 O 0.16-0.18 wt%, Fe 2 O 3 0.56-0.83 wt%, Li 2 O 2.57-2.85 wt%.
- the present disclosure therefore provides a mould flux having a composition of, in weight% SiO 2 15-25; CaO 15-35; Al 2 O 3 1-7; Na 2 O 18-30; K 2 O 15-25; Fe 2 O 3 0-5; C 0-4; TiO 2 0-2; MnO 0-2; MgO 0-2; Li 2 O 0-10; and wherein the melting point of the mould flux is less than or equal to 1300°C.
- Mould fluxes are synthetic slags constituted by a complex mix of oxides, minerals and carbonaceous materials.
- the main oxides are silica (SiO 2 ), calcium oxide (CaO), sodium oxide (Na 2 O), alumina (Al 2 O 3 ) and magnesium oxide (MgO).
- the liquid slag formed by the flux constitutes a barrier to avoid steel re-oxidation by contact with air and the entrapment of other gases, such as nitrogen.
- the fluxes can be added through the top of the mould on the liquid steel, manually or automatically.
- the mould flux is provided as a powder having the above-mentioned or below-mentioned composition. The flux will then melt in contact with the molten alloy.
- the present composition limits the CaO content in the mould powder compared to conventional mould fluxes.
- Perovskite phase formation is assumed to be as follows: SiO 2 +Ti ⁇ TiO 2 +Si.
- TiO 2 may together with CaO form Perovskite as a solution of Ca 2 Ti 2 O 5 and Ca 2 Ti 2 O 6 .
- CaO in the flux contributes to the formation of Perovskite.
- the mould flux according to the present disclosure suppresses the formation of a Perovskite phase compared to mould fluxes of prior art.
- At least a part of Na 2 O, SiO 2 and Al 2 O 3 present in the mould flux are in the form of Sodium Feldspar (Na 0.33 Al 0.35 Si 1.13 O 2.95 ).
- at least 25%, or at least 40% of Na 2 O, SiO 2 and Al 2 O 3 present in the mould flux are in the form of Sodium Feldspar (Na 0.33 Al 0.35 Si 1.13 O 2.95 ).
- at least 50%, or at least 90% of the Na 2 O present in the mould flux is in the form of Sodium Feldspar, (Na 0.33 Al 0.35 Si 1.13 O 2.95 ).
- At least a part of K 2 O, SiO 2 and Al 2 O 3 present in the mould flux is present in the form of Potassium Feldspar (K 0.33 Al 0.35 Si 1.13 O 2.95 ).
- at least 25%, or at least 40% of K 2 O, SiO 2 and Al 2 O 3 present in the mould flux is present in the form of Potassium Feldspar (K 0.33 Al 0.35 Si 1.13 O 2.95 ).
- at least 50%, or at least 90%, of the K 2 O present in the mould flux is present in the form of Potassium Feldspar (K 0.33 Al 0.35 Si 1.13 O 2.95 ).
- the content of Na 2 O in the mould flux is 18-25 weight%.
- the content of K 2 O in the mould flux is 15-22 weight%.
- the content of TiO 2 in the mould flux is >0.05 weight%.
- the content of Li 2 O in the mould flux is >1.0 weight%.
- the ratio of CaO and SiO 2 (CaO/SiO 2 )- is in the range of 3:4 to 4:3, such as 1:1. These oxides are important to control the viscosity and the melting point of the mould flux.
- a CaO content greater than 35 weight% will promote the formation of Perovskite and CaO less than 15 % might induce high viscosity in the molten mould powder.
- the content of SiO 2 should be controlled on the basis of CaO.
- Na 2 O, K 2 O and Li 2 O will stabilize Ti in the melt and thereby as mentioned above will contribute to the prevention of Perovskite formation. This is best results are achieved when each of Na 2 O and K 2 O is present in an amount of 18-22 weight%, preferably around 20 weight%, in the mould mixture.
- these alkali oxides promote the formation of Nepheline phase which is beneficial during casting. A very high content of these oxides will make the flux mould too fluid and a too low content would result in formation of Perovskite phase.
- the objective of the present disclosure is also achieved by means of a method of moulding a piece of a Ni-base alloy wherein a mould flux as defined hereinabove or hereinafter is applied on a surface of the molten alloy during moulding thereof.
- the Ni-base alloy comprises, in weight%: C ⁇ 0.05; Cr 17-23; Ni 35-63; Mo 2.5-9.5; Ti 0.3-3.0; Al 0-0.7; Si 0-0.5; Nb 0-4.5; Cu 0-3; Mn 0-0.1; S 0-0.003; P: 0-0.02; balance Fe.
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Nonmetallic Welding Materials (AREA)
- Treatment Of Steel In Its Molten State (AREA)
Claims (14)
- Formflussmittel, das in Gewichts-% eine Zusammensetzung wie folgt aufweist:
SiO2 15 - 25; CaO 15 - 35; Al2O3 1 - 7; Na2O 18 - 30; K2O 15 - 25; Fe2O3 0 - 5; C 0 - 4; TiO2 0 - 2; MnO 0-2; MgO 0-2; Li2O 0 -10; - Formflussmittel nach Anspruch 1, wobei mindestens ein Teil von in dem Formflussmittel vorhandenen Na2O, SiO2 und Al2O3 in der Form von Natriumfeldspat, Na0,33Al0,35Si1,13O3,95, vorhanden ist.
- Formflussmittel nach Anspruch 1 oder 2, wobei mindestens ein Teil von in dem Formflussmittel vorhandenen K2O, SiO2 und Al2O3 in der Form von Kaliumfeldspat, K0,33Al0,35Si1,13O2,95, vorhanden ist.
- Formflussmittel nach einem der Ansprüche 1 - 3, wobei mindestens 50 % des in dem Formflussmittel vorhandenen Na2O in der Form von Natriumfeldspat, Na0,33Al0,35Si1,13O2,95, ist.
- Formflussmittel nach einem der Ansprüche 1 - 4, wobei mindestens 50 % des in dem Formflussmittel vorhandenen K2O in der Form von Kaliumfeldspat, K0,33Al0,35Si1,13O2,95, vorhanden ist.
- Formflussmittel nach einem der Ansprüche 1 - 5, wobei der Gehalt an Na2O in Gewichts-% 18 - 25 beträgt.
- Formflussmittel nach einem der Ansprüche 1 - 6, wobei der Gehalt an K2O in Gewichts-% 15 - 22 beträgt..
- Formflussmittel nach einem der Ansprüche 1 - 7, wobei der Gehalt an TiO2 > 0,05 Gewichts-% beträgt.
- Formflussmittel nach einem der Ansprüche 1 - 8, wobei der Gehalt an Li2O > 1,0 Gewichts-% beträgt.
- Formflussmittel nach einem der Ansprüche 1 - 9, wobei SiO2/(CaO+Al2O3) > 1.
- Formflussmittel nach einem der Ansprüche 1 - 10, wobei das Verhältnis zwischen CaO und SiO2 im Bereich von 3:4 - 4:3 liegt.
- Formflussmittel nach einem der Ansprüche 1-11, wobei das Formflussmittel ein Pulver ist, das eine Zusammensetzung nach einem der Ansprüche 1-11 aufweist.
- Verfahren zum Herstellen einer Nickelbasislegierung, wobei ein Formflussmittel nach einem der Ansprüche 1 - 12 auf eine Oberfläche der geschmolzenen Nickelbasislegierung während deren Formen angewendet wird.
- Verfahren nach Anspruch 13, wobei die Ni - Basislegierung in Gewichts-% Folgendes umfasst:
C < 0,05; Cr 17 - 23; Ni 35 - 63; Mo 2,5 - 9,5; Ti 0,3 - 3,0; Al 0 - 0,7; Si 0 - 0,5; Nb 0-4,5; Cu 0 - 3; Mn 0-0,1; S 0 - 0,003; P: 0 - 0,02;
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP19199984.6A EP3797898B1 (de) | 2019-09-26 | 2019-09-26 | Formflussmittel und verwendung davon |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP19199984.6A EP3797898B1 (de) | 2019-09-26 | 2019-09-26 | Formflussmittel und verwendung davon |
Publications (2)
Publication Number | Publication Date |
---|---|
EP3797898A1 EP3797898A1 (de) | 2021-03-31 |
EP3797898B1 true EP3797898B1 (de) | 2022-07-27 |
Family
ID=68072196
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP19199984.6A Active EP3797898B1 (de) | 2019-09-26 | 2019-09-26 | Formflussmittel und verwendung davon |
Country Status (1)
Country | Link |
---|---|
EP (1) | EP3797898B1 (de) |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA1016724A (en) * | 1972-09-18 | 1977-09-06 | Smc Corporation | Flux for continuous casting of steel |
JP2994718B2 (ja) * | 1990-09-29 | 1999-12-27 | 株式会社神戸製鋼所 | 連続鋳造用フラックス |
EP2035169B1 (de) * | 2006-06-22 | 2017-03-15 | Posco | Giesspulver und dieses verwendendes stranggiessverfahren |
JP5585347B2 (ja) * | 2010-09-27 | 2014-09-10 | 品川リフラクトリーズ株式会社 | 鋼の連続鋳造用モールドパウダー |
KR102073318B1 (ko) * | 2015-11-05 | 2020-02-03 | 닛폰세이테츠 가부시키가이샤 | 연속 주조용 몰드 플럭스 및 연속 주조 방법 |
KR102033641B1 (ko) * | 2018-02-13 | 2019-10-18 | 주식회사 포스코 | 몰드 플럭스 및 주조방법 |
-
2019
- 2019-09-26 EP EP19199984.6A patent/EP3797898B1/de active Active
Also Published As
Publication number | Publication date |
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EP3797898A1 (de) | 2021-03-31 |
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