EP3423179B1 - Vorrichtung, anlage und verfahren zum zumischen wenigstens eines ersten stoffs und eines zweiten stoffs zu einem grundstoff zur bildung einer mischung - Google Patents

Vorrichtung, anlage und verfahren zum zumischen wenigstens eines ersten stoffs und eines zweiten stoffs zu einem grundstoff zur bildung einer mischung Download PDF

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Publication number
EP3423179B1
EP3423179B1 EP17706750.1A EP17706750A EP3423179B1 EP 3423179 B1 EP3423179 B1 EP 3423179B1 EP 17706750 A EP17706750 A EP 17706750A EP 3423179 B1 EP3423179 B1 EP 3423179B1
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EP
European Patent Office
Prior art keywords
mixing
substance
mixing vessel
admixing
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Application number
EP17706750.1A
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German (de)
English (en)
French (fr)
Other versions
EP3423179A1 (de
EP3423179C0 (de
Inventor
Stefan Sanwald
Bernhard Roth
Bernd Fischer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IPCO Germany GmbH
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IPCO Germany GmbH
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Filing date
Publication date
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Publication of EP3423179A1 publication Critical patent/EP3423179A1/de
Application granted granted Critical
Publication of EP3423179B1 publication Critical patent/EP3423179B1/de
Publication of EP3423179C0 publication Critical patent/EP3423179C0/de
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/53Mixing liquids with solids using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/59Mixing systems, i.e. flow charts or diagrams
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/81Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
    • B01F33/811Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/715Feeding the components in several steps, e.g. successive steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/92Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/32Mixing fertiliser ingredients

Definitions

  • the invention relates to a device for admixing at least one first substance and one second substance to a base substance for the continuous formation of a mixture.
  • the invention also relates to a system with a device according to the invention.
  • the invention relates to a method for admixing a first substance and a second substance to a base substance to form a mixture.
  • the device according to the invention, the system according to the invention and the method according to the invention are particularly suitable for admixing a first substance and a second substance to a urea melt, a dispersion then being formed from the first substance, the second substance and the urea melt. This dispersion can then be processed into pastilles in the plant according to the invention.
  • the invention is therefore particularly suitable for producing a fertilizer that is easy to handle, in particular urea fertilizer.
  • a device for admixing at least a first substance and a second substance to a base substance for the continuous formation of a mixture is known.
  • the device has a first mixing container and a second mixing container.
  • the first and second mixing containers each have an inlet opening, an introduction opening for admixing the first or second substance, and an outlet opening.
  • the first and the second mixing tank are each provided with an agitator.
  • the outlet opening of the first mixing container and the inlet opening of the second mixing container are connected to one another by means of a connecting line, the connecting line being open during mixing operation of the device.
  • the mixing containers of the device should be operated with the exclusion of air. Since the system works with the exclusion of air and the components to be emulsified are continuously introduced into the mixing device, the components located in the mixing device are continuously transported away in the direction of the discharge line.
  • a device for admixing at least a first substance and a second substance to a flowable base substance has two mixing containers connected in series, each with an agitator.
  • a return line is provided to return fluid from the second tank to the first tank.
  • a device for admixing at least a first substance and a second substance to a flowable base substance has a first mixing tank and a second mixing tank, each of the mixing tanks being provided with an agitator.
  • a mixture is mixed in either the first mixing tank and the second mixing tank and then transported via a discharge line to a downstream processor. While one of the containers is being emptied, another container is being loaded or is on hold. The transport of fluid from the first mixing container into the second mixing container is not provided.
  • the aim of the invention is to improve the production of mixtures from a first substance, a second substance and a base substance.
  • a device for admixing a first substance and a second substance to a base substance to form a mixture in particular for admixing a first substance and a second substance to a urea melt to form a dispersion according to claim 1, is provided for this purpose, the device for admixing the following features
  • the admixing device has a first mixing container and a second mixing container.
  • the first and second mixing containers each have an inlet opening for admitting a base material or an intermediate mixture, an outlet opening for letting out the intermediate mixture or the mixture, an inlet opening for admixing the first or second substance and a pressure equalization opening.
  • the pressure equalization openings of the first and second mixing containers are connected to one another by means of a pressure equalization line, with the pressure equalization openings being above the fluid levels present in the mixing containers when the device is in operation when the device is in operation, so that the interior of the first mixing container and the interior of the second mixing container the same pressure is present, and the outlet opening of the first mixing tank and the inlet opening of the second mixing tank are connected to one another by means of a connecting line, which enables flow during operation of the device, with the outlet opening of the first mixing tank, the connecting line and the inlet opening of the second mixing tank being connected during operation of the device Mixing tanks are below the fluid level in the mixing tanks, so that fluid can pass from the first mixing tank into the second mixing tank.
  • a first and a second mixing container are provided in the device according to the invention and fluid can flow from the first mixing container into the second mixing container through the connecting line, which is open during operation, an intermediate mixing stage is thus produced in the first mixing container and this intermediate mixing stage is then fed to the second mixing container , where a second substance is then added.
  • This achieves particularly good and rapid mixing of the first substance with the base substance and then subsequently of the second substance with the intermediate mixing stage.
  • the multi-stage admixing prevents the admixed substances from influencing one another and/or the admixing of the at least one further substance is facilitated.
  • the mixing intermediate stage gets from the first mixing container into the second mixing container only by gravity, it can be ensured that a mixing time in the first mixing container is long enough to achieve a particularly uniform mixture between the first substance and the base substance. A sufficiently long mixing time to produce a particularly uniform mixture can also be achieved in the second mixing container. Due to the connecting line, which is open during operation of the device and lies below the fluid level, the fluid levels in the two mixing containers are always essentially at the same level. If, for example, the fluid level in the second mixing tank is higher than in the first mixing tank, then fluid can also reach the first mixing tank through the connecting line from the second mixing tank. As a rule, however, the intermediate mixture stage produced in the first mixing container flows through the connecting line into the second mixing container as a result of gravity. Continuous mixing operation is possible with the device according to the invention.
  • the mixing containers and/or agitators can be designed differently.
  • the first mixing container and the second mixing container each have an essentially the same basic shape with essentially the same volume, and the first mixing container and the second mixing container are arranged essentially at the same height.
  • the inlet openings and/or outlet openings of the first and the second mixing container merge within the mixing container into an angled piece of pipe, preferably into a piece of pipe bent at an angle of 90°, and the center planes of the angled pieces of pipe are each aligned essentially perpendicularly to a center longitudinal axis of the first or second mixing container.
  • Fluid thus emerges from the inlet openings perpendicularly to the central longitudinal axis of the containers and also enters the outlet openings again perpendicularly to the central longitudinal axis of the containers.
  • the inlet openings can, for example, also be aligned in such a way that they support a flow movement within the mixing container around the central longitudinal axis.
  • it can also be useful to direct the inlet openings against the flow generated by the agitator and also to align the outlet openings against the flow generated in the container by the agitator.
  • the inlet into the second mixing container is preferably in the direction of flow.
  • the angled pipe sections can also be left out at the outlet openings.
  • the openings of the angled pipe sections which form the inlet opening or the outlet opening within the mixing container, point in the same tangential direction when viewed parallel to the central longitudinal axis of the first or second mixing container.
  • either a flow around the central longitudinal axis of the respective mixing container can be supported by appropriate arrangement of the inlet opening.
  • the inlet opening can be directed against the flow generated by an agitator in the respective mixing container, and the outlet opening can also be directed either in or against a direction of flow within the respective mixing container.
  • the inlet opening of the first mixing container is connected to a raw material feed, in particular to a feed for urea melt
  • the outlet opening of the second mixing container is connected to a device for further processing the mixture, in particular to a pastillation device.
  • the first mixing container and the second mixing container are each provided with an agitator.
  • the first mixing container, the second mixing container, the through-line and/or the connecting line have a double-walled structure, with gaps formed by means of the double-walled structure are designed for the passage of heating or cooling media.
  • the melt can be kept in the flowable state or heated within the mixing container and also within the pressure equalization line and the connecting line.
  • first and/or the second mixing container have external thermal insulation.
  • the intermediate spaces are connected to a heating device for the heating medium.
  • heating devices are also referred to as trace heating.
  • the invention also relates to a system with a device according to the invention, the system having a base material feed, the system having a first metering device for a first substance to be mixed with the base material, and a second metering device for a second substance to be mixed with the base material, the system having a line with a pump arranged in its course for transferring the finished mixture from the second mixing container to a pastillating device for pastillating the mixture, with a return line being provided for partially returning the mixture to the second mixing tank, which is fed into this second mixing tank below or above the fluid level opens out and wherein the pastillating device has a rotating and perforated drum and a rotating cooling belt.
  • melts in particular can be mixed and then pelletized.
  • the system according to the invention is particularly suitable for pastillating a urea melt, a first substance and a second substance being admixed to the urea melt. This is of great advantage, especially in the production of fertilizers.
  • the melt Inside the mixing container, the melt can be kept in a good flowable state, so that a very even mixture can be produced with the two substances supplied.
  • the mixture of the melt and the at least two admixed substances is then fed to the pastillation device.
  • the return line makes it possible to maintain a comparatively high flow rate within the feed line, so that there is no risk of the melt partially solidifying in the connecting line.
  • the melt is fed to the pelletizing device in the liquid state but at a temperature which is only slightly above its solidification temperature. This makes it possible to produce qualitatively high-quality pastilles, which solidify essentially immediately after being deposited in the form of liquid melt droplets on the cooling belt and thus essentially retain their almost spherical droplet shape on the cooling belt.
  • a basic substance, in particular a urea melt, is supplied to a first mixing container , the first substance to be mixed is fed to the base material in the first mixing tank to form an intermediate mixture, the intermediate mixture from the first mixing tank is fed to the second mixing tank, the second substance to be mixed is fed to the intermediate mixture in the second mixing tank to form the mixture, with the supply the intermediate mixing stage from the first mixing tank into the second mixing tank using gravity by means of a connecting line between the mixing tanks located below the fluid level in the mixing tanks.
  • the base material is advantageously a melt, in particular a urea melt.
  • the device according to the invention shown partially in section, for admixing a first substance and a second substance to a base substance to form a mixture has a first mixing container 12 and a second mixing container 14 .
  • the two mixing containers 12, 14 have the same basic shape and the same volume and are also arranged at the same height above a machine frame 16. However, within the scope of the invention, the mixing containers 12, 14 can certainly have different basic shapes and different volumes.
  • Both mixing containers 12, 14 are each provided with an agitator 18, which is shown only schematically and which can be driven by a motor 20 in each case.
  • the two mixing containers 12, 14 each have a cylindrical shape with a bulging bottom.
  • the agitator extends parallel to the central longitudinal axis of the mixing container 12, 14 and a drive shaft of the agitator lies on the central longitudinal axis 22, 24 of the respective mixing container 12, 14.
  • the mixing container 12 has an inlet opening 26 for admitting a base substance. For example, a urea melt is introduced into the first mixing container 12 via the inlet opening 26 .
  • the first mixing container 12 has an outlet opening 28 .
  • the outlet opening 28 is opposite the inlet opening 26 and is also arranged at the same level as the inlet opening 26 .
  • the outlet opening 28 must be below a fluid level that is reached in the first mixing container 12 during operation.
  • the first mixing container 12 also has a pressure equalization opening 30 which is arranged above the outlet opening 28 and which must be above a fluid level within the first mixing container 12 during operation.
  • the second mixing container 14 is constructed identically to the first mixing container 12 and has an inlet opening 32 for letting in an intermediate mixture stage from the first mixing container 12 and an outlet opening 34 for letting out the finished mixture.
  • the outlet opening 34 is arranged opposite the inlet opening 32 and at the same height as the inlet opening 32, although this is not mandatory, as has already been explained with reference to the first mixing container 12.
  • the second mixing vessel 14 also includes a pressure equalization port 36 located above the inlet port 32 and the outlet port 34 .
  • the Pressure compensation opening 36 should be above a fluid level in the second mixing container 14 and the outlet opening 34 should be below a fluid level in the second mixing container 14 .
  • the pressure equalization openings 30, 36 are at the same height and are connected to a pressure equalization line 38.
  • the outlet opening 28 of the first mixing container 12 and the inlet opening 32 of the second mixing container 14 are at the same level and are connected to a connecting line 40 .
  • the connecting line 40 lies below a fluid level in the first mixing container 12 and below a fluid level in the second mixing container 14 over its entire length.
  • the inlet opening 32 of the second mixing container 14 must also be below a fluid level in the second mixing container 14 .
  • a transport of fluid from the first mixing container 12 into the second mixing container 14 and optionally from the second mixing container 14 into the first mixing container 12 can thereby take place by means of gravity.
  • a fluid level provided during operation is indicated with the reference numeral 42.
  • a fluid level present during operation is indicated with the reference numeral 44.
  • the two fluid levels 42, 44 are practically at the same level or at least at a similar level, since the two mixing containers 12, 14 communicate with one another via the connecting line 40.
  • a base material is fed in via the inlet opening 26 of the first mixing container 12 , for example a urea melt
  • the fluid level 42 in the first mixing container 12 will rise slightly.
  • the slightly increased liquid pressure at the outlet opening 28 of the first mixing container 12 causes the fluid in the first mixing container 12, which forms an intermediate mixing stage, to be transported via the connecting line 40 into the second mixing container 14, so that the fluid levels 42, 44 equalize again .
  • the first mixing container 12 has a lid in which an insertion opening 46 is provided for mixing in a first substance.
  • an additive or another substance can be introduced into the base material, specifically the urea melt, in the first mixing container 14 via the introduction opening 46 . Solids may need to be preheated.
  • the first Fabric is preferably introduced continuously via the insertion port 46 . As a result, an intermediate mixture of the base material and the first material is produced within the first mixing container.
  • the second mixing container 14 also has a lid with an insertion opening 48 through which a second substance can be admixed.
  • the second substance passes through the introduction opening 48 into the second mixing container and is mixed there with the intermediate mixture stage, which consists of the base substance and the first substance and has reached the second mixing container 48 via the connecting line 40 .
  • the finished mixture is present within the second mixing container 14 and can then be removed via the outlet opening 34 .
  • the device according to the invention works continuously. During operation, base material is thus continuously supplied via the introduction opening 26, the first substance is continuously supplied via the inlet opening 46 and the second substance is continuously supplied via the inlet opening 48, and the finished mixture can be continuously removed via the outlet opening 34.
  • Sufficient mixing time can be ensured both within the first mixing container 12 and within the second mixing container 14 because the fluid is transported from the first mixing container 12 into the second mixing container 14 by the influence of gravity via the connecting line 40 .
  • This ensures a particularly uniform mixture of the first material with the base material for producing an intermediate mixture and then of the second material and the intermediate mixture in the second mixing container.
  • the agitators 18 provided in each mixing container 12, 14 support the production of a particularly uniform mixture.
  • Each of the mixing containers 12, 14 has a further outlet opening 50 at its bottom.
  • This further outlet opening 50 is provided, for example, for completely emptying the mixing container 12, 14 as part of an inspection or as part of a shutdown of the device.
  • the connecting line 40 is provided with branches and can also, like the pressure compensation line 38, be provided with a shut-off valve. During operation of the device, however, both the pressure equalization line 38 and the connecting line 40 should be open in order to allow pressure equalization between the mixing containers 12, 14 and fluid transport between the two mixing containers 12, 14.
  • the two mixing containers 12, 14 are each double-walled, so that an intermediate space 52 is formed in which a heating medium or cooling medium can be transported. If by means of the device according to the invention a mixture of a If urea melt and two other substances are produced, a heating medium is applied to the intermediate space 52 in each case in order to ensure that the melt does not already partially solidify within the mixing container 12, 14.
  • the pressure-equalizing line 38 and the connecting line 40 are each double-walled, so that the heating medium can also heat the pressure-equalizing line 38 and the connecting line 40 .
  • connection pieces of the inlet opening 26, the outlet opening 28, the inlet opening 32 and the outlet opening 34 are each double-walled in order to be able to heat them and to prevent the melt from solidifying in these areas, which could cause deposits to form. Solids may need to be preheated.
  • a heating medium is fed into the intermediate space 52 via a heating line 54, for example.
  • the representation of 2 shows the first mixing container 12 in a view from above, with the mixing container 12 only being partially indicated by dashed lines in order to also be able to show components lying underneath the lid.
  • the inlet opening 26 is provided with an angled piece of pipe 56 which deflects the melt entering through the inlet opening 26 by 90° and thereby introduces it into the interior of the first mixing container 12 approximately tangentially to the central longitudinal axis 24 .
  • the pipe section 56 has, in the representation of 2 in the clockwise direction. Depending on the direction of rotation of the agitator 18 about the central longitudinal axis 24, the melt flowing in via the inlet opening 26 and the pipe section 56 supports a flow movement of the melt about the central longitudinal axis 24 or is directed against this flow direction.
  • the intermediate mixture stage produced in the first mixing container 12 is removed through the outlet opening 28 .
  • the piece of pipe 56 is aligned with a direction of flow that prevails in the mixing container 12 .
  • In the representation of 2 would rotate the agitator 18 clockwise and thus also cause a flow movement within the mixing container 12 in the clockwise direction.
  • the representation of 3 shows the area of the inlet opening 26 on the first mixing container 12 in more detail and in a sectional view.
  • the pipe section 56 angled by 90° connects to the inlet opening 26 .
  • the inlet opening 26 bridges the intermediate space 52 which, as has already been described, is heated by means of a heating medium.
  • the intermediate space 52 also continues up to a connecting flange 60 .
  • the piece of pipe 62 between the connecting flange 60 and the inlet opening 26 can also be heated by means of the heating medium. This prevents the supplied melt from solidifying in this area.
  • the representation of 4 shows a system for pastillating a melt, in particular a urea melt, the system having a device 10 according to the invention for admixing a first substance and a second substance to a base substance.
  • Plant 70 is used to produce urea fertilizer.
  • the urea fertilizer can be removed downstream of the plant in the form of solidified pastilles.
  • the lozenges then consist of a mixture of urea with at least a first and a second substance, the first and the second substance being admixed in the device 10 .
  • a urea melt is supplied to the first mixing container 12 via the introduction opening 26 and mixed there with a first substance which is supplied via the introduction opening 46 .
  • the intermediate mixture stage consisting of the urea melt and the first substance reaches the second mixing container 14 and is mixed there with a second substance that is fed in via the introduction opening 48 .
  • the finished mixture is removed from the second mixing container 14 at the outlet opening 34 and fed to a grinding unit 74 by means of a pump 72 .
  • a particle size of the mixture, which forms a dispersion of the urea melt and the first material and the second material can be reduced.
  • the grinding unit 74 can also be omitted.
  • the mixture is then fed to a pastillating device 76 via a further connecting line.
  • the pastillation device 76 has a rotating, perforated drum 78 and a nozzle bar, which conveys the mixture against the perforated drum 78 from the inside.
  • the perforated drum produces melt droplets which are then deposited on a circulating cooling belt 80 .
  • the deposited product droplets solidify on the cooling belt 80 to form lozenges and can then be removed from the cooling belt 80 as solid lozenges.
  • a return line 82 leads from a branch 84 back to the second mixing container 14 .
  • the finished mixture can reach the branch 84 not only to the pastillation device 76, but back again into the second mixing container 14.
  • this makes it possible to circulate a larger quantity of the mixture in the connecting line and the return line 82 .
  • This can ensure, for example, that the mixture, which consists of a dispersion of a melt and other substances, does not separate again within the connecting line or partially solidify.
  • the mixing device 10 can continue to be operated even if the pastillating device 76 is temporarily stopped, for example.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Fertilizers (AREA)
  • Exhaust Gas After Treatment (AREA)
EP17706750.1A 2016-03-01 2017-02-22 Vorrichtung, anlage und verfahren zum zumischen wenigstens eines ersten stoffs und eines zweiten stoffs zu einem grundstoff zur bildung einer mischung Active EP3423179B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102016203293.3A DE102016203293A1 (de) 2016-03-01 2016-03-01 Vorrichtung, Anlage und Verfahren zum Zumischen wenigstens eines ersten Stoffs und eines zweiten Stoffes zu einem Grundstoff zur Bildung einer Mischung
PCT/EP2017/054014 WO2017148758A1 (de) 2016-03-01 2017-02-22 Vorrichtung, anlage und verfahren zum zumischen wenigstens eines ersten stoffs und eines zweiten stoffs zu einem grundstoff zur bildung einer mischung

Publications (3)

Publication Number Publication Date
EP3423179A1 EP3423179A1 (de) 2019-01-09
EP3423179B1 true EP3423179B1 (de) 2023-08-09
EP3423179C0 EP3423179C0 (de) 2023-08-09

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EP17706750.1A Active EP3423179B1 (de) 2016-03-01 2017-02-22 Vorrichtung, anlage und verfahren zum zumischen wenigstens eines ersten stoffs und eines zweiten stoffs zu einem grundstoff zur bildung einer mischung

Country Status (4)

Country Link
EP (1) EP3423179B1 (zh)
CN (1) CN109152996B (zh)
DE (1) DE102016203293A1 (zh)
WO (1) WO2017148758A1 (zh)

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Publication number Priority date Publication date Assignee Title
CN109225056A (zh) * 2018-09-17 2019-01-18 淮北惠源环保科技有限公司 一种车用尿素溶液加热装置
FR3090401B1 (fr) * 2018-12-21 2023-04-28 Seb Sa Appareil de fabrication, machine à mélange et/ou dispositif de réception pour la fabrication d’une composition à partir d’un mélange de formulations
CN110238966B (zh) * 2019-06-27 2023-08-15 四川宏华石油设备有限公司 一种混合装置

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GB125426A (en) * 1916-07-14 1919-04-24 Chance And Hunt Ltd An Improved Apparatus for the Treatment of One Liquid with Another.
GB1310725A (en) * 1970-09-28 1973-03-21 Cluett Peabody & Co Inc Method and apparatus for mixing volatile liquid with non-volatile material
DE3032384A1 (de) * 1980-08-28 1982-07-08 Sociedad Minera y Metalúrgica de Penarroya España S.A., Madrid Anlage zum emulgieren von schweroelen
DE4130413C2 (de) * 1991-09-10 1995-05-04 Mette Manfred Anlage zum Mischen und/oder Homogenisieren flüssiger Komponenten
DE10322998B4 (de) * 2003-02-28 2006-06-29 Dürr Systems GmbH Verfahren und Vorrichtung zur Herstellung eines Zweikomponenten-Lackgemischs
DE10361307A1 (de) * 2003-11-24 2005-06-30 Romaco Ag Frymakoruma Durchlauf-Misch-Dispergier-Verfahren und Durchlauf-Misch-Dispergier-Vorrichtung
FI122939B (fi) * 2009-06-11 2012-09-14 Outotec Oyj Menetelmä ja laitteisto uuttoliuoksen regeneroimiseksi metallien uuttoprosesseissa
DE102010028774A1 (de) * 2010-05-07 2011-11-10 Otc Gmbh Emulgiereinrichtung zur kontinuierlichen Herstellung von Emulsionen und/oder Dispersionen
CN104555975B (zh) * 2015-01-28 2017-01-18 江苏华东锂电技术研究院有限公司 磷酸铁锂连续制备装置及制备方法

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Publication number Publication date
CN109152996B (zh) 2022-03-04
WO2017148758A1 (de) 2017-09-08
EP3423179A1 (de) 2019-01-09
DE102016203293A1 (de) 2017-09-07
EP3423179C0 (de) 2023-08-09
CN109152996A (zh) 2019-01-04

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