EP3423179B1 - Device, system, and method for mixing at least one first material and a second material so as to form a base material for forming a mixture - Google Patents
Device, system, and method for mixing at least one first material and a second material so as to form a base material for forming a mixture Download PDFInfo
- Publication number
- EP3423179B1 EP3423179B1 EP17706750.1A EP17706750A EP3423179B1 EP 3423179 B1 EP3423179 B1 EP 3423179B1 EP 17706750 A EP17706750 A EP 17706750A EP 3423179 B1 EP3423179 B1 EP 3423179B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- mixing
- substance
- mixing vessel
- admixing
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000203 mixture Substances 0.000 title claims description 59
- 239000000463 material Substances 0.000 title claims description 20
- 238000000034 method Methods 0.000 title claims description 9
- 239000000126 substance Substances 0.000 claims description 94
- 239000012530 fluid Substances 0.000 claims description 34
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 26
- 239000004202 carbamide Substances 0.000 claims description 26
- 239000000155 melt Substances 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 9
- 239000006185 dispersion Substances 0.000 claims description 6
- 230000009969 flowable effect Effects 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 2
- 238000009434 installation Methods 0.000 claims 6
- 238000010276 construction Methods 0.000 claims 2
- 230000000694 effects Effects 0.000 claims 1
- 230000007704 transition Effects 0.000 claims 1
- 239000003337 fertilizer Substances 0.000 description 6
- 230000005484 gravity Effects 0.000 description 6
- 239000007788 liquid Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000000227 grinding Methods 0.000 description 3
- 238000003780 insertion Methods 0.000 description 3
- 230000037431 insertion Effects 0.000 description 3
- 239000007937 lozenge Substances 0.000 description 3
- 235000010603 pastilles Nutrition 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000007717 exclusion Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005453 pelletization Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
- B01F23/53—Mixing liquids with solids using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
- B01F23/59—Mixing systems, i.e. flow charts or diagrams
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
- B01F33/811—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/71—Feed mechanisms
- B01F35/715—Feeding the components in several steps, e.g. successive steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/32—Mixing fertiliser ingredients
Definitions
- the invention relates to a device for admixing at least one first substance and one second substance to a base substance for the continuous formation of a mixture.
- the invention also relates to a system with a device according to the invention.
- the invention relates to a method for admixing a first substance and a second substance to a base substance to form a mixture.
- the device according to the invention, the system according to the invention and the method according to the invention are particularly suitable for admixing a first substance and a second substance to a urea melt, a dispersion then being formed from the first substance, the second substance and the urea melt. This dispersion can then be processed into pastilles in the plant according to the invention.
- the invention is therefore particularly suitable for producing a fertilizer that is easy to handle, in particular urea fertilizer.
- a device for admixing at least a first substance and a second substance to a base substance for the continuous formation of a mixture is known.
- the device has a first mixing container and a second mixing container.
- the first and second mixing containers each have an inlet opening, an introduction opening for admixing the first or second substance, and an outlet opening.
- the first and the second mixing tank are each provided with an agitator.
- the outlet opening of the first mixing container and the inlet opening of the second mixing container are connected to one another by means of a connecting line, the connecting line being open during mixing operation of the device.
- the mixing containers of the device should be operated with the exclusion of air. Since the system works with the exclusion of air and the components to be emulsified are continuously introduced into the mixing device, the components located in the mixing device are continuously transported away in the direction of the discharge line.
- a device for admixing at least a first substance and a second substance to a flowable base substance has two mixing containers connected in series, each with an agitator.
- a return line is provided to return fluid from the second tank to the first tank.
- a device for admixing at least a first substance and a second substance to a flowable base substance has a first mixing tank and a second mixing tank, each of the mixing tanks being provided with an agitator.
- a mixture is mixed in either the first mixing tank and the second mixing tank and then transported via a discharge line to a downstream processor. While one of the containers is being emptied, another container is being loaded or is on hold. The transport of fluid from the first mixing container into the second mixing container is not provided.
- the aim of the invention is to improve the production of mixtures from a first substance, a second substance and a base substance.
- a device for admixing a first substance and a second substance to a base substance to form a mixture in particular for admixing a first substance and a second substance to a urea melt to form a dispersion according to claim 1, is provided for this purpose, the device for admixing the following features
- the admixing device has a first mixing container and a second mixing container.
- the first and second mixing containers each have an inlet opening for admitting a base material or an intermediate mixture, an outlet opening for letting out the intermediate mixture or the mixture, an inlet opening for admixing the first or second substance and a pressure equalization opening.
- the pressure equalization openings of the first and second mixing containers are connected to one another by means of a pressure equalization line, with the pressure equalization openings being above the fluid levels present in the mixing containers when the device is in operation when the device is in operation, so that the interior of the first mixing container and the interior of the second mixing container the same pressure is present, and the outlet opening of the first mixing tank and the inlet opening of the second mixing tank are connected to one another by means of a connecting line, which enables flow during operation of the device, with the outlet opening of the first mixing tank, the connecting line and the inlet opening of the second mixing tank being connected during operation of the device Mixing tanks are below the fluid level in the mixing tanks, so that fluid can pass from the first mixing tank into the second mixing tank.
- a first and a second mixing container are provided in the device according to the invention and fluid can flow from the first mixing container into the second mixing container through the connecting line, which is open during operation, an intermediate mixing stage is thus produced in the first mixing container and this intermediate mixing stage is then fed to the second mixing container , where a second substance is then added.
- This achieves particularly good and rapid mixing of the first substance with the base substance and then subsequently of the second substance with the intermediate mixing stage.
- the multi-stage admixing prevents the admixed substances from influencing one another and/or the admixing of the at least one further substance is facilitated.
- the mixing intermediate stage gets from the first mixing container into the second mixing container only by gravity, it can be ensured that a mixing time in the first mixing container is long enough to achieve a particularly uniform mixture between the first substance and the base substance. A sufficiently long mixing time to produce a particularly uniform mixture can also be achieved in the second mixing container. Due to the connecting line, which is open during operation of the device and lies below the fluid level, the fluid levels in the two mixing containers are always essentially at the same level. If, for example, the fluid level in the second mixing tank is higher than in the first mixing tank, then fluid can also reach the first mixing tank through the connecting line from the second mixing tank. As a rule, however, the intermediate mixture stage produced in the first mixing container flows through the connecting line into the second mixing container as a result of gravity. Continuous mixing operation is possible with the device according to the invention.
- the mixing containers and/or agitators can be designed differently.
- the first mixing container and the second mixing container each have an essentially the same basic shape with essentially the same volume, and the first mixing container and the second mixing container are arranged essentially at the same height.
- the inlet openings and/or outlet openings of the first and the second mixing container merge within the mixing container into an angled piece of pipe, preferably into a piece of pipe bent at an angle of 90°, and the center planes of the angled pieces of pipe are each aligned essentially perpendicularly to a center longitudinal axis of the first or second mixing container.
- Fluid thus emerges from the inlet openings perpendicularly to the central longitudinal axis of the containers and also enters the outlet openings again perpendicularly to the central longitudinal axis of the containers.
- the inlet openings can, for example, also be aligned in such a way that they support a flow movement within the mixing container around the central longitudinal axis.
- it can also be useful to direct the inlet openings against the flow generated by the agitator and also to align the outlet openings against the flow generated in the container by the agitator.
- the inlet into the second mixing container is preferably in the direction of flow.
- the angled pipe sections can also be left out at the outlet openings.
- the openings of the angled pipe sections which form the inlet opening or the outlet opening within the mixing container, point in the same tangential direction when viewed parallel to the central longitudinal axis of the first or second mixing container.
- either a flow around the central longitudinal axis of the respective mixing container can be supported by appropriate arrangement of the inlet opening.
- the inlet opening can be directed against the flow generated by an agitator in the respective mixing container, and the outlet opening can also be directed either in or against a direction of flow within the respective mixing container.
- the inlet opening of the first mixing container is connected to a raw material feed, in particular to a feed for urea melt
- the outlet opening of the second mixing container is connected to a device for further processing the mixture, in particular to a pastillation device.
- the first mixing container and the second mixing container are each provided with an agitator.
- the first mixing container, the second mixing container, the through-line and/or the connecting line have a double-walled structure, with gaps formed by means of the double-walled structure are designed for the passage of heating or cooling media.
- the melt can be kept in the flowable state or heated within the mixing container and also within the pressure equalization line and the connecting line.
- first and/or the second mixing container have external thermal insulation.
- the intermediate spaces are connected to a heating device for the heating medium.
- heating devices are also referred to as trace heating.
- the invention also relates to a system with a device according to the invention, the system having a base material feed, the system having a first metering device for a first substance to be mixed with the base material, and a second metering device for a second substance to be mixed with the base material, the system having a line with a pump arranged in its course for transferring the finished mixture from the second mixing container to a pastillating device for pastillating the mixture, with a return line being provided for partially returning the mixture to the second mixing tank, which is fed into this second mixing tank below or above the fluid level opens out and wherein the pastillating device has a rotating and perforated drum and a rotating cooling belt.
- melts in particular can be mixed and then pelletized.
- the system according to the invention is particularly suitable for pastillating a urea melt, a first substance and a second substance being admixed to the urea melt. This is of great advantage, especially in the production of fertilizers.
- the melt Inside the mixing container, the melt can be kept in a good flowable state, so that a very even mixture can be produced with the two substances supplied.
- the mixture of the melt and the at least two admixed substances is then fed to the pastillation device.
- the return line makes it possible to maintain a comparatively high flow rate within the feed line, so that there is no risk of the melt partially solidifying in the connecting line.
- the melt is fed to the pelletizing device in the liquid state but at a temperature which is only slightly above its solidification temperature. This makes it possible to produce qualitatively high-quality pastilles, which solidify essentially immediately after being deposited in the form of liquid melt droplets on the cooling belt and thus essentially retain their almost spherical droplet shape on the cooling belt.
- a basic substance, in particular a urea melt, is supplied to a first mixing container , the first substance to be mixed is fed to the base material in the first mixing tank to form an intermediate mixture, the intermediate mixture from the first mixing tank is fed to the second mixing tank, the second substance to be mixed is fed to the intermediate mixture in the second mixing tank to form the mixture, with the supply the intermediate mixing stage from the first mixing tank into the second mixing tank using gravity by means of a connecting line between the mixing tanks located below the fluid level in the mixing tanks.
- the base material is advantageously a melt, in particular a urea melt.
- the device according to the invention shown partially in section, for admixing a first substance and a second substance to a base substance to form a mixture has a first mixing container 12 and a second mixing container 14 .
- the two mixing containers 12, 14 have the same basic shape and the same volume and are also arranged at the same height above a machine frame 16. However, within the scope of the invention, the mixing containers 12, 14 can certainly have different basic shapes and different volumes.
- Both mixing containers 12, 14 are each provided with an agitator 18, which is shown only schematically and which can be driven by a motor 20 in each case.
- the two mixing containers 12, 14 each have a cylindrical shape with a bulging bottom.
- the agitator extends parallel to the central longitudinal axis of the mixing container 12, 14 and a drive shaft of the agitator lies on the central longitudinal axis 22, 24 of the respective mixing container 12, 14.
- the mixing container 12 has an inlet opening 26 for admitting a base substance. For example, a urea melt is introduced into the first mixing container 12 via the inlet opening 26 .
- the first mixing container 12 has an outlet opening 28 .
- the outlet opening 28 is opposite the inlet opening 26 and is also arranged at the same level as the inlet opening 26 .
- the outlet opening 28 must be below a fluid level that is reached in the first mixing container 12 during operation.
- the first mixing container 12 also has a pressure equalization opening 30 which is arranged above the outlet opening 28 and which must be above a fluid level within the first mixing container 12 during operation.
- the second mixing container 14 is constructed identically to the first mixing container 12 and has an inlet opening 32 for letting in an intermediate mixture stage from the first mixing container 12 and an outlet opening 34 for letting out the finished mixture.
- the outlet opening 34 is arranged opposite the inlet opening 32 and at the same height as the inlet opening 32, although this is not mandatory, as has already been explained with reference to the first mixing container 12.
- the second mixing vessel 14 also includes a pressure equalization port 36 located above the inlet port 32 and the outlet port 34 .
- the Pressure compensation opening 36 should be above a fluid level in the second mixing container 14 and the outlet opening 34 should be below a fluid level in the second mixing container 14 .
- the pressure equalization openings 30, 36 are at the same height and are connected to a pressure equalization line 38.
- the outlet opening 28 of the first mixing container 12 and the inlet opening 32 of the second mixing container 14 are at the same level and are connected to a connecting line 40 .
- the connecting line 40 lies below a fluid level in the first mixing container 12 and below a fluid level in the second mixing container 14 over its entire length.
- the inlet opening 32 of the second mixing container 14 must also be below a fluid level in the second mixing container 14 .
- a transport of fluid from the first mixing container 12 into the second mixing container 14 and optionally from the second mixing container 14 into the first mixing container 12 can thereby take place by means of gravity.
- a fluid level provided during operation is indicated with the reference numeral 42.
- a fluid level present during operation is indicated with the reference numeral 44.
- the two fluid levels 42, 44 are practically at the same level or at least at a similar level, since the two mixing containers 12, 14 communicate with one another via the connecting line 40.
- a base material is fed in via the inlet opening 26 of the first mixing container 12 , for example a urea melt
- the fluid level 42 in the first mixing container 12 will rise slightly.
- the slightly increased liquid pressure at the outlet opening 28 of the first mixing container 12 causes the fluid in the first mixing container 12, which forms an intermediate mixing stage, to be transported via the connecting line 40 into the second mixing container 14, so that the fluid levels 42, 44 equalize again .
- the first mixing container 12 has a lid in which an insertion opening 46 is provided for mixing in a first substance.
- an additive or another substance can be introduced into the base material, specifically the urea melt, in the first mixing container 14 via the introduction opening 46 . Solids may need to be preheated.
- the first Fabric is preferably introduced continuously via the insertion port 46 . As a result, an intermediate mixture of the base material and the first material is produced within the first mixing container.
- the second mixing container 14 also has a lid with an insertion opening 48 through which a second substance can be admixed.
- the second substance passes through the introduction opening 48 into the second mixing container and is mixed there with the intermediate mixture stage, which consists of the base substance and the first substance and has reached the second mixing container 48 via the connecting line 40 .
- the finished mixture is present within the second mixing container 14 and can then be removed via the outlet opening 34 .
- the device according to the invention works continuously. During operation, base material is thus continuously supplied via the introduction opening 26, the first substance is continuously supplied via the inlet opening 46 and the second substance is continuously supplied via the inlet opening 48, and the finished mixture can be continuously removed via the outlet opening 34.
- Sufficient mixing time can be ensured both within the first mixing container 12 and within the second mixing container 14 because the fluid is transported from the first mixing container 12 into the second mixing container 14 by the influence of gravity via the connecting line 40 .
- This ensures a particularly uniform mixture of the first material with the base material for producing an intermediate mixture and then of the second material and the intermediate mixture in the second mixing container.
- the agitators 18 provided in each mixing container 12, 14 support the production of a particularly uniform mixture.
- Each of the mixing containers 12, 14 has a further outlet opening 50 at its bottom.
- This further outlet opening 50 is provided, for example, for completely emptying the mixing container 12, 14 as part of an inspection or as part of a shutdown of the device.
- the connecting line 40 is provided with branches and can also, like the pressure compensation line 38, be provided with a shut-off valve. During operation of the device, however, both the pressure equalization line 38 and the connecting line 40 should be open in order to allow pressure equalization between the mixing containers 12, 14 and fluid transport between the two mixing containers 12, 14.
- the two mixing containers 12, 14 are each double-walled, so that an intermediate space 52 is formed in which a heating medium or cooling medium can be transported. If by means of the device according to the invention a mixture of a If urea melt and two other substances are produced, a heating medium is applied to the intermediate space 52 in each case in order to ensure that the melt does not already partially solidify within the mixing container 12, 14.
- the pressure-equalizing line 38 and the connecting line 40 are each double-walled, so that the heating medium can also heat the pressure-equalizing line 38 and the connecting line 40 .
- connection pieces of the inlet opening 26, the outlet opening 28, the inlet opening 32 and the outlet opening 34 are each double-walled in order to be able to heat them and to prevent the melt from solidifying in these areas, which could cause deposits to form. Solids may need to be preheated.
- a heating medium is fed into the intermediate space 52 via a heating line 54, for example.
- the representation of 2 shows the first mixing container 12 in a view from above, with the mixing container 12 only being partially indicated by dashed lines in order to also be able to show components lying underneath the lid.
- the inlet opening 26 is provided with an angled piece of pipe 56 which deflects the melt entering through the inlet opening 26 by 90° and thereby introduces it into the interior of the first mixing container 12 approximately tangentially to the central longitudinal axis 24 .
- the pipe section 56 has, in the representation of 2 in the clockwise direction. Depending on the direction of rotation of the agitator 18 about the central longitudinal axis 24, the melt flowing in via the inlet opening 26 and the pipe section 56 supports a flow movement of the melt about the central longitudinal axis 24 or is directed against this flow direction.
- the intermediate mixture stage produced in the first mixing container 12 is removed through the outlet opening 28 .
- the piece of pipe 56 is aligned with a direction of flow that prevails in the mixing container 12 .
- In the representation of 2 would rotate the agitator 18 clockwise and thus also cause a flow movement within the mixing container 12 in the clockwise direction.
- the representation of 3 shows the area of the inlet opening 26 on the first mixing container 12 in more detail and in a sectional view.
- the pipe section 56 angled by 90° connects to the inlet opening 26 .
- the inlet opening 26 bridges the intermediate space 52 which, as has already been described, is heated by means of a heating medium.
- the intermediate space 52 also continues up to a connecting flange 60 .
- the piece of pipe 62 between the connecting flange 60 and the inlet opening 26 can also be heated by means of the heating medium. This prevents the supplied melt from solidifying in this area.
- the representation of 4 shows a system for pastillating a melt, in particular a urea melt, the system having a device 10 according to the invention for admixing a first substance and a second substance to a base substance.
- Plant 70 is used to produce urea fertilizer.
- the urea fertilizer can be removed downstream of the plant in the form of solidified pastilles.
- the lozenges then consist of a mixture of urea with at least a first and a second substance, the first and the second substance being admixed in the device 10 .
- a urea melt is supplied to the first mixing container 12 via the introduction opening 26 and mixed there with a first substance which is supplied via the introduction opening 46 .
- the intermediate mixture stage consisting of the urea melt and the first substance reaches the second mixing container 14 and is mixed there with a second substance that is fed in via the introduction opening 48 .
- the finished mixture is removed from the second mixing container 14 at the outlet opening 34 and fed to a grinding unit 74 by means of a pump 72 .
- a particle size of the mixture, which forms a dispersion of the urea melt and the first material and the second material can be reduced.
- the grinding unit 74 can also be omitted.
- the mixture is then fed to a pastillating device 76 via a further connecting line.
- the pastillation device 76 has a rotating, perforated drum 78 and a nozzle bar, which conveys the mixture against the perforated drum 78 from the inside.
- the perforated drum produces melt droplets which are then deposited on a circulating cooling belt 80 .
- the deposited product droplets solidify on the cooling belt 80 to form lozenges and can then be removed from the cooling belt 80 as solid lozenges.
- a return line 82 leads from a branch 84 back to the second mixing container 14 .
- the finished mixture can reach the branch 84 not only to the pastillation device 76, but back again into the second mixing container 14.
- this makes it possible to circulate a larger quantity of the mixture in the connecting line and the return line 82 .
- This can ensure, for example, that the mixture, which consists of a dispersion of a melt and other substances, does not separate again within the connecting line or partially solidify.
- the mixing device 10 can continue to be operated even if the pastillating device 76 is temporarily stopped, for example.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Fertilizers (AREA)
- Exhaust Gas After Treatment (AREA)
Description
Die Erfindung betrifft eine Vorrichtung zum Zumischen wenigstens eines ersten Stoffs und eines zweiten Stoffs zu einem Grundstoff zur kontinuierlichen Bildung einer Mischung. Die Erfindung betrifft auch eine Anlage mit einer erfindungsgemäßen Vorrichtung. Schließlich betrifft die Erfindung ein Verfahren zum Zumischen eines ersten Stoffs und eines zweiten Stoffs zu einem Grundstoff zur Bildung einer Mischung. Die erfindungsgemäße Vorrichtung, die erfindungsgemäße Anlage und das erfindungsgemäße Verfahren sind besonders zum Zumischen eines ersten Stoffs und eines zweiten Stoffs zu einer Harnstoffschmelze geeignet, wobei dann aus dem ersten Stoff, dem zweiten Stoff und der Harnstoffschmelze eine Dispersion gebildet wird. Diese Dispersion kann dann in der erfindungsgemäßen Anlage zu Pastillen verarbeitet werden. Die Erfindung ist dadurch in besonderer Weise zur Herstellung eines einfach handhabbaren Düngers, insbesondere Harnstoffdünger, geeignet.The invention relates to a device for admixing at least one first substance and one second substance to a base substance for the continuous formation of a mixture. The invention also relates to a system with a device according to the invention. Finally, the invention relates to a method for admixing a first substance and a second substance to a base substance to form a mixture. The device according to the invention, the system according to the invention and the method according to the invention are particularly suitable for admixing a first substance and a second substance to a urea melt, a dispersion then being formed from the first substance, the second substance and the urea melt. This dispersion can then be processed into pastilles in the plant according to the invention. The invention is therefore particularly suitable for producing a fertilizer that is easy to handle, in particular urea fertilizer.
Aus der deutschen Offenlegungsschrift
Aus der deutschen Offenlegungsschrift
Aus der britischen Patentschrift
Aus der deutschen Offenlegungsschrift
Mit der Erfindung soll das Herstellen von Mischungen aus einem ersten Stoff, einem zweiten Stoff und einem Grundstoff verbessert werden.The aim of the invention is to improve the production of mixtures from a first substance, a second substance and a base substance.
Erfindungsgemäß ist hierzu eine Vorrichtung zum Zumischen eines ersten Stoffs und eines zweiten Stoffs zu einem Grundstoff zur Bildung einer Mischung, insbesondere zum Zumischen eines ersten Stoffs und eines zweiten Stoffs zu einer Harnstoffschmelze zur Bildung einer Dispersion gemäß Anspruch 1 vorgesehen, wobei die Vorrichtung zum Zumischen folgende Merkmale aufweistAccording to the invention, a device for admixing a first substance and a second substance to a base substance to form a mixture, in particular for admixing a first substance and a second substance to a urea melt to form a dispersion according to claim 1, is provided for this purpose, the device for admixing the following features
Die Vorrichtung zum Zumischen weist einen ersten Mischbehälter und einen zweiten Mischbehälter auf. Der erste und der zweite Mischbehälter weisen jeweils eine Einlassöffnung zum Einlassen eines Grundstoffs bzw. einer Mischungszwischenstufe, jeweils eine Auslassöffnung zum Auslassen der Mischungszwischenstufe bzw. der Mischung, jeweils eine Einführöffnung zum Zumischen des ersten bzw. zweiten Stoffs sowie jeweils eine Druckausgleichsöffnung auf. Die Druckausgleichsöffnungen des ersten und des zweiten Mischbehälters sind mittels einer Druckausgleichsleitung miteinander verbunden, wobei im Betrieb der Vorrichtung die Druckausgleichsöffnungen oberhalb von im Betrieb der Vorrichtung in den Mischbehältern vorliegenden Fluidspiegeln liegen, so dass also im Innenraum des ersten Mischbehälters und im Innenraum des zweiten Mischbehälters der gleiche Druck vorliegt, und die Auslassöffnung des ersten Mischbehälters und die Einlassöffnung des zweiten Mischbehälters sind mittels einer Verbindungsleitung miteinander verbunden, die im Betrieb der Vorrichtung einen Durchfluss ermöglicht, wobei im Betrieb der Vorrichtung die Auslassöffnung des ersten Mischbehälters, die Verbindungsleitung und die Einlassöffnung des zweiten Mischbehälters unterhalb der Fluidspiegel in den Mischbehältern liegen, so dass Fluid aus dem ersten Mischbehälter in den zweiten Mischbehälter gelangen kann.The admixing device has a first mixing container and a second mixing container. The first and second mixing containers each have an inlet opening for admitting a base material or an intermediate mixture, an outlet opening for letting out the intermediate mixture or the mixture, an inlet opening for admixing the first or second substance and a pressure equalization opening. The pressure equalization openings of the first and second mixing containers are connected to one another by means of a pressure equalization line, with the pressure equalization openings being above the fluid levels present in the mixing containers when the device is in operation when the device is in operation, so that the interior of the first mixing container and the interior of the second mixing container the same pressure is present, and the outlet opening of the first mixing tank and the inlet opening of the second mixing tank are connected to one another by means of a connecting line, which enables flow during operation of the device, with the outlet opening of the first mixing tank, the connecting line and the inlet opening of the second mixing tank being connected during operation of the device Mixing tanks are below the fluid level in the mixing tanks, so that fluid can pass from the first mixing tank into the second mixing tank.
Indem bei der erfindungsgemäßen Vorrichtung ein erster und ein zweiter Mischbehälter vorgesehen sind und durch die im Betrieb offene Verbindungsleitung Fluid aus dem ersten Mischbehälter in den zweiten Mischbehälter gelangen kann, wird also in dem ersten Mischbehälter eine Mischungszwischenstufe hergestellt und diese Mischungszwischenstufe wird dann dem zweiten Mischbehälter zugeführt, wo dann ein zweiter Stoff zugemischt wird. Dadurch wird eine besonders gute und dabei zügige Vermischung des ersten Stoffs mit dem Grundstoff und dann nachfolgend des zweiten Stoffs mit der Mischungszwischenstufe erreicht. Durch das mehrstufige Zumischen wird eine Beeinflussung der zugemischten Stoffe untereinander vermieden und/oder das Zumischen des wenigstens einen weiteren Stoffes wird erleichtert. Da die Mischungszwischenstufe lediglich mittels Schwerkraft aus dem ersten Mischbehälter in den zweiten Mischbehälter gelangt, kann sichergestellt werden, dass eine Mischzeit im ersten Mischbehälter ausreichend groß ist, um eine besonders gleichmäßige Mischung zwischen erstem Stoff und Grundstoff zu erreichen. Auch im zweiten Mischbehälter kann eine ausreichend große Mischzeit zur Herstellung einer besonders gleichmäßigen Mischung erreicht werden. Durch die im Betrieb der Vorrichtung offene Verbindungsleitung, die unterhalb der Fluidspiegel liegt, liegen die Fluidspiegel in den beiden Mischbehältern immer im Wesentlichen auf gleicher Höhe. Sollte beispielsweise im zweiten Mischbehälter ein höherer Fluidspiegel vorliegen als im ersten Mischbehälter, so kann Fluid durch die Verbindungsleitung vom zweiten Mischbehälter auch in den ersten Mischbehälter gelangen. In der Regel strömt aber die im ersten Mischbehälter hergestellte Mischungszwischenstufe der Schwerkraft folgend durch die Verbindungsleitung in den zweiten Mischbehälter. Mit der erfindungsgemäßen Vorrichtung ist ein kontinuierlicher Mischbetrieb möglich. Die Mischbehälter und/oder Rührwerke können unterschiedlich ausgebildet sein.Since a first and a second mixing container are provided in the device according to the invention and fluid can flow from the first mixing container into the second mixing container through the connecting line, which is open during operation, an intermediate mixing stage is thus produced in the first mixing container and this intermediate mixing stage is then fed to the second mixing container , where a second substance is then added. This achieves particularly good and rapid mixing of the first substance with the base substance and then subsequently of the second substance with the intermediate mixing stage. The multi-stage admixing prevents the admixed substances from influencing one another and/or the admixing of the at least one further substance is facilitated. Since the mixing intermediate stage gets from the first mixing container into the second mixing container only by gravity, it can be ensured that a mixing time in the first mixing container is long enough to achieve a particularly uniform mixture between the first substance and the base substance. A sufficiently long mixing time to produce a particularly uniform mixture can also be achieved in the second mixing container. Due to the connecting line, which is open during operation of the device and lies below the fluid level, the fluid levels in the two mixing containers are always essentially at the same level. If, for example, the fluid level in the second mixing tank is higher than in the first mixing tank, then fluid can also reach the first mixing tank through the connecting line from the second mixing tank. As a rule, however, the intermediate mixture stage produced in the first mixing container flows through the connecting line into the second mixing container as a result of gravity. Continuous mixing operation is possible with the device according to the invention. The mixing containers and/or agitators can be designed differently.
In Weiterbildung der Erfindung weisen der erste Mischbehälter und der zweite Mischbehälter jeweils eine im Wesentlichen gleiche Grundform mit im Wesentlichen gleichem Volumen auf und der erste Mischbehälter und der zweite Mischbehälter sind im Wesentlichen auf gleicher Höhe angeordnet.In a development of the invention, the first mixing container and the second mixing container each have an essentially the same basic shape with essentially the same volume, and the first mixing container and the second mixing container are arranged essentially at the same height.
Auf diese Weise kann sichergestellt werden, dass die Mischzeit im ersten Mischbehälter und die Mischzeit im zweiten Mischbehälter im Wesentlichen gleich sind, so dass eine sehr gleichmäßige Mischung aus dem Grundstoff und den beiden zugeführten Stoffen erreicht werden kann.In this way it can be ensured that the mixing time in the first mixing container and the mixing time in the second mixing container are essentially the same, so that a very uniform mixture of the base substance and the two supplied substances can be achieved.
In Weiterbildung der Erfindung gehen die Einlassöffnungen und/oder Auslassöffnungen des ersten und des zweiten Mischbehälters innerhalb der Mischbehälter jeweils in ein abgewinkeltes Rohrstück über, vorzugsweise in ein um einen Winkel von 90° abgewinkeltes Rohrstück, und die Mittelebenen der abgewinkelten Rohrstücke sind jeweils im Wesentlichen senkrecht zu einer Mittellängsachse des ersten bzw. des zweiten Mischbehälters ausgerichtet.In a further development of the invention, the inlet openings and/or outlet openings of the first and the second mixing container merge within the mixing container into an angled piece of pipe, preferably into a piece of pipe bent at an angle of 90°, and the center planes of the angled pieces of pipe are each aligned essentially perpendicularly to a center longitudinal axis of the first or second mixing container.
Damit tritt Fluid aus den Einlassöffnungen senkrecht zur Mittellängsachse der Behälter aus und tritt auch wieder senkrecht zur Mittellängsachse der Behälter in die Auslassöffnungen ein. Dies ist gerade dann besonders vorteilhaft, wenn in den Mischbehältern eine Strömungsbewegung um die Mittellängsachse erzeugt wird, beispielsweise mittels eines Rührwerks. Die Einlassöffnungen können beispielsweise auch so ausgerichtet werden, dass sie eine Strömungsbewegung innerhalb der Mischbehälter um die Mittellängsachse unterstützen. Zur Erzeugung von Turbulenz kann es aber auch sinnvoll sein, die Einlassöffnungen gegen die durch das Rührwerk erzeugte Strömung zu richten und auch die Auslassöffnungen entgegen der in dem Behälter durch das Rührwerk erzeugten Strömung auszurichten. Vorzugsweise erfolgt der Einlass in den zweiten Mischbehälter in Strömungsrichtung. An den Auslassöffnungen können die abgewinkelten Rohrstücke auch weggelassen werden.Fluid thus emerges from the inlet openings perpendicularly to the central longitudinal axis of the containers and also enters the outlet openings again perpendicularly to the central longitudinal axis of the containers. This is particularly advantageous when a flow movement about the central longitudinal axis is generated in the mixing containers, for example by means of an agitator. The inlet openings can, for example, also be aligned in such a way that they support a flow movement within the mixing container around the central longitudinal axis. To generate turbulence, however, it can also be useful to direct the inlet openings against the flow generated by the agitator and also to align the outlet openings against the flow generated in the container by the agitator. The inlet into the second mixing container is preferably in the direction of flow. The angled pipe sections can also be left out at the outlet openings.
In Weiterbildung der Erfindung weisen die Öffnungen der abgewinkelten Rohrstücke, die die Einlassöffnung bzw. die Auslassöffnung innerhalb der Mischbehälter bilden, parallel zu der Mittellängsachse des ersten bzw. des zweiten Mischbehälters gesehen jeweils in die gleiche tangentiale Richtung.In a further development of the invention, the openings of the angled pipe sections, which form the inlet opening or the outlet opening within the mixing container, point in the same tangential direction when viewed parallel to the central longitudinal axis of the first or second mixing container.
Dadurch kann, je nach Anwendungsfall, entweder eine Strömung um die Mittellängsachse des jeweiligen Mischbehälters durch entsprechende Anordnung der Einlassöffnung unterstützt werden. Alternativ kann die Einlassöffnung gegen die durch ein Rührwerk in dem jeweiligen Mischbehälter erzeugte Strömung gerichtet werden und auch die Auslassöffnung kann entweder in oder entgegen einer Strömungsrichtung innerhalb des jeweiligen Mischbehälters gerichtet werden.As a result, depending on the application, either a flow around the central longitudinal axis of the respective mixing container can be supported by appropriate arrangement of the inlet opening. Alternatively, the inlet opening can be directed against the flow generated by an agitator in the respective mixing container, and the outlet opening can also be directed either in or against a direction of flow within the respective mixing container.
In Weiterbildung der Erfindung ist die Einlassöffnung des ersten Mischbehälters mit einer Grundstoffzufuhr verbunden, insbesondere mit einer Zufuhr für Harnstoffschmelze, und die Auslassöffnung des zweiten Mischbehälters ist mit einer Vorrichtung zur Weiterverarbeitung der Mischung verbunden, insbesondere mit einer Pastilliervorrichtung.In a development of the invention, the inlet opening of the first mixing container is connected to a raw material feed, in particular to a feed for urea melt, and the outlet opening of the second mixing container is connected to a device for further processing the mixture, in particular to a pastillation device.
In Weiterbildung der Erfindung sind der erste Mischbehälter und der zweite Mischbehälter jeweils mit einem Rührwerk versehen.In a development of the invention, the first mixing container and the second mixing container are each provided with an agitator.
In Weiterbildung der Erfindung weisen der erste Mischbehälter, der zweite Mischbehälter, die Durchgangsleitung und/oder die Verbindungsleitung einen doppelwandigen Aufbau auf, wobei mittels des doppelwandigen Aufbaus gebildete Zwischenräume zum Durchleiten von Heiz- oder Kühlmedien ausgebildet sind. Bei der Verarbeitung von Schmelzen, insbesondere von Harnstoffschmelzen, kann dadurch die Schmelze innerhalb der Mischbehälter sowie auch innerhalb der Druckausgleichsleitung und der Verbindungsleitung im fließfähigen Zustand gehalten oder aufgeheizt werden.In a further development of the invention, the first mixing container, the second mixing container, the through-line and/or the connecting line have a double-walled structure, with gaps formed by means of the double-walled structure are designed for the passage of heating or cooling media. When processing melts, in particular urea melts, the melt can be kept in the flowable state or heated within the mixing container and also within the pressure equalization line and the connecting line.
Zusätzlich kann in Weiterbildung der Erfindung vorgesehen sein, dass der erste und/oder der zweite Mischbehälter eine außenliegende Wärmeisolation aufweisen.In addition, in a further development of the invention, it can be provided that the first and/or the second mixing container have external thermal insulation.
Zusätzlich kann in Weiterbildung der Erfindung vorgesehen sein, dass die Zwischenräume mit einer Heizvorrichtung für das Heizmedium verbunden sind. Solche Heizvorrichtungen werden auch als Begleitheizung bezeichnet.In addition, it can be provided in a further development of the invention that the intermediate spaces are connected to a heating device for the heating medium. Such heating devices are also referred to as trace heating.
Die Erfindung betrifft auch eine Anlage mit einer erfindungsgemäßen Vorrichtung, wobei die Anlage eine Grundstoffzufuhr aufweist, die Anlage eine erste Dosiervorrichtung für einen ersten, dem Grundstoff zuzumischenden Stoff, und eine zweite Dosiervorrichtung für einen zweiten, dem Grundstoff zuzumischenden Stoff aufweist, wobei die Anlage eine Leitung mit in deren Verlauf angeordneter Pumpe zum Überführen der fertigen Mischung aus dem zweiten Mischbehälter zu einer Pastilliervorrichtung zum Pastillieren der Mischung aufweist, wobei eine Rückführleitung zur teilweisen Rückführung der Mischung in den zweiten Mischbehälter vorgesehen ist, die in diesen zweiten Mischbehälter unterhalb oder oberhalb des Fluidspiegels mündet und wobei die Pastilliervorrichtung eine rotierende und gelochte Trommel sowie ein umlaufendes Kühlband aufweist.The invention also relates to a system with a device according to the invention, the system having a base material feed, the system having a first metering device for a first substance to be mixed with the base material, and a second metering device for a second substance to be mixed with the base material, the system having a line with a pump arranged in its course for transferring the finished mixture from the second mixing container to a pastillating device for pastillating the mixture, with a return line being provided for partially returning the mixture to the second mixing tank, which is fed into this second mixing tank below or above the fluid level opens out and wherein the pastillating device has a rotating and perforated drum and a rotating cooling belt.
Mittels einer solchen Anlage können insbesondere Schmelzen gemischt und dann pastilliert werden. Besonders geeignet ist die erfindungsgemäße Anlage zum Pastillieren einer Harnstoffschmelze, wobei der Harnstoffschmelze ein erster Stoff und ein zweiter Stoff zugemischt werden. Dies ist speziell bei der Herstellung von Düngern von großem Vorteil. Innerhalb der Mischbehälter kann die Schmelze in einem gut fließfähigen Zustand gehalten werden, so dass eine sehr gleichmäßige Mischung mit den beiden zugeführten Stoffen hergestellt werden kann. Im flüssigen Zustand wird die Mischung aus der Schmelze und den wenigstens zwei zugemischten Stoffen dann der Pastilliervorrichtung zugeführt. Die Rückführleitung ermöglicht es, innerhalb der Zuführleitung eine vergleichsweise große Strömungsgeschwindigkeit aufrechtzuerhalten, so dass nicht die Gefahr besteht, dass die Schmelze in der Verbindungsleitung teilweise erstarrt. Die Schmelze wird der Pastilliervorrichtung im flüssigen Zustand aber mit einer Temperatur zugeführt, die nur geringfügig oberhalb ihrer Erstarrungstemperatur liegt. Dies ermöglicht die Herstellung qualitativ hochwertiger Pastillen, die im Wesentlichen sofort nach dem Ablegen in Form flüssiger Schmelzetropfen auf dem Kühlband erstarren und somit ihre annähernd kugelförmige Tropfenform auch auf dem Kühlband im Wesentlichen beibehalten.Using such a system, melts in particular can be mixed and then pelletized. The system according to the invention is particularly suitable for pastillating a urea melt, a first substance and a second substance being admixed to the urea melt. This is of great advantage, especially in the production of fertilizers. Inside the mixing container, the melt can be kept in a good flowable state, so that a very even mixture can be produced with the two substances supplied. In the liquid state, the mixture of the melt and the at least two admixed substances is then fed to the pastillation device. The return line makes it possible to maintain a comparatively high flow rate within the feed line, so that there is no risk of the melt partially solidifying in the connecting line. The melt is fed to the pelletizing device in the liquid state but at a temperature which is only slightly above its solidification temperature. This makes it possible to produce qualitatively high-quality pastilles, which solidify essentially immediately after being deposited in the form of liquid melt droplets on the cooling belt and thus essentially retain their almost spherical droplet shape on the cooling belt.
Das der Erfindung zugrunde liegende Problem wird auch durch ein Verfahren zum Zumischen eines ersten Stoffs und eines zweiten Stoffs zu einem Grundstoff zur Bildung einer Mischung gelöst, wobei das Verfahren zum Zumischen folgende Merkmale aufweist: Einem ersten Mischbehälter wird ein Grundstoff, insbesondere eine Harnstoffschmelze, zugeführt, zu dem Grundstoff wird im ersten Mischbehälter zur Bildung einer Mischungszwischenstufe der erste zuzumischende Stoff zugeführt, die Mischungszwischenstufe aus dem ersten Mischbehälter wird dem zweiten Mischbehälter zugeführt, zu der Mischungszwischenstufe wird im zweiten Mischbehälter zur Bildung der Mischung der zweite zuzumischende Stoff zugeführt, wobei die Zufuhr der Mischungszwischenstufe aus dem ersten Mischbehälter in den zweiten Mischbehälter unter Nutzung der Schwerkraft mittels einer unterhalb der Fluidspiegel in den Mischbehältern liegenden Verbindungsleitung zwischen den Mischbehältern erfolgt.The problem on which the invention is based is also solved by a method for admixing a first substance and a second substance to a basic substance to form a mixture, the method for admixing having the following features: A basic substance, in particular a urea melt, is supplied to a first mixing container , the first substance to be mixed is fed to the base material in the first mixing tank to form an intermediate mixture, the intermediate mixture from the first mixing tank is fed to the second mixing tank, the second substance to be mixed is fed to the intermediate mixture in the second mixing tank to form the mixture, with the supply the intermediate mixing stage from the first mixing tank into the second mixing tank using gravity by means of a connecting line between the mixing tanks located below the fluid level in the mixing tanks.
Durch die Nutzung der Schwerkraft zum Weitertransportieren der Mischungszwischenstufe aus dem ersten Mischbehälter in den zweiten Mischbehälter kann eine ausreichende Mischzeit und damit das Herstellen einer sehr gleichmäßigen Mischung sowohl im ersten als auch im zweiten Mischbehälter gewährleistet werden.By using gravity to transport the intermediate mixing stage from the first mixing container to the second mixing container, a sufficient mixing time and thus the production of a very uniform mixture can be ensured both in the first and in the second mixing container.
Vorteilhafterweise ist der Grundstoff eine Schmelze, insbesondere eine Harnstoffschmelze.The base material is advantageously a melt, in particular a urea melt.
Weitere Vorteile und Merkmale der Erfindung ergeben sich aus den Ansprüchen und der nachfolgenden Beschreibung bevorzugter Ausführungsbeispiele der Erfindung, die nachfolgend anhand der Figuren erläutert sind. Einzelmerkmale der unterschiedlichen Ausführungsbeispiele lassen sich dabei in beliebiger Weise miteinander kombinieren, ohne den Rahmen der Erfindung zu überschreiten. In den Zeichnungen zeigen:
- Fig. 1
- eine teilweise geschnittene Seitenansicht einer erfindungsgemäßen Vorrichtung,
- Fig. 2
- eine schematische Ansicht des ersten Mischbehälters der Vorrichtung der
Fig. 1 von oben, - Fig. 3
- eine abschnittsweise Schnittansicht des Behälters der
Fig. 2 und - Fig. 4
- eine schematische Darstellung einer erfindungsgemäßen Anlage zum Herstellen eines Harnstoffdüngers aus einer Harnstoffschmelze.
- 1
- a partially sectioned side view of a device according to the invention,
- 2
- a schematic view of the first mixing container of the device
1 from above, - 3
- a partial sectional view of the container of FIG
2 and - 4
- a schematic representation of a system according to the invention for producing a urea fertilizer from a urea melt.
Eine in
Der erste Mischbehälter 12 weist darüber hinaus eine Druckausgleichsöffnung 30 auf, die oberhalb der Auslassöffnung 28 angeordnet ist und die im Betrieb oberhalb eines Fluidspiegels innerhalb des ersten Mischbehälters 12 liegen muss.The
Der zweite Mischbehälter 14 ist identisch zum ersten Mischbehälter 12 aufgebaut und weist eine Einlassöffnung 32 zum Einlassen einer Mischungszwischenstufe aus dem ersten Mischbehälter 12 und eine Auslassöffnung 34 zum Auslassen der fertigen Mischung auf. Die Auslassöffnung 34 ist gegenüber der Einlassöffnung 32 und auf gleicher Höhe wie die Einlassöffnung 32 angeordnet, wobei dies, wie bereits anhand des ersten Mischbehälters 12 ausgeführt wurde, nicht zwingend ist.The
Der zweite Mischbehälter 14 weist auch eine Druckausgleichsöffnung 36 auf, die oberhalb der Einlassöffnung 32 und der Auslassöffnung 34 angeordnet ist. Im Betrieb soll die Druckausgleichsöffnung 36 oberhalb eines Fluidspiegels im zweiten Mischbehälter 14 liegen und die Auslassöffnung 34 soll unterhalb eines Fluidspiegels im zweiten Mischbehälter 14 liegen.The
Die Druckausgleichsöffnungen 30, 36 liegen auf gleicher Höhe und sind mit einer Druckausgleichsleitung 38 verbunden.The
Die Auslassöffnung 28 des ersten Mischbehälters 12 und die Einlassöffnung 32 des zweiten Mischbehälters 14 liegen auf gleicher Höhe und sind mit einer Verbindungsleitung 40 verbunden. Es ist im Rahmen der Erfindung nicht unbedingt erforderlich, dass die Auslassöffnung 28 des ersten Mischbehälters 12 und die Einlassöffnung 32 des zweiten Mischbehälters 14 auf gleicher Höhe liegen. Wesentlich ist aber, dass die Verbindungsleitung 40 über ihre gesamte Länge unterhalb eines Fluidspiegels im ersten Mischbehälter 12 und unterhalb eines Fluidspiegels im zweiten Mischbehälter 14 liegt. Infolgedessen muss auch die Einlassöffnung 32 des zweiten Mischbehälters 14 unterhalb eines Fluidspiegels im zweiten Mischbehälter 14 liegen. Ein Transport von Fluid aus dem ersten Mischbehälter 12 in den zweiten Mischbehälter 14 und gegebenenfalls aus dem zweiten Mischbehälter 14 in den ersten Mischbehälter 12 kann dadurch mittels Schwerkraft erfolgen.The
Im ersten Mischbehälter 12 ist ein im Betrieb vorgesehener Fluidspiegel mit der Bezugsziffer 42 angedeutet. Im zweiten Mischbehälter 14 ist ein im Betrieb vorliegender Fluidspiegel mit der Bezugsziffer 44 angedeutet. Die beiden Fluidspiegel 42, 44 liegen praktisch auf gleicher oder zumindest ähnlicher Höhe, da ja die beiden Mischbehälter 12, 14 über die Verbindungsleitung 40 miteinander kommunizieren.In the
Wird im Betrieb der erfindungsgemäßen Vorrichtung nun über die Einlassöffnung 26 des ersten Mischbehälters 12 ein Grundstoff zugeführt, beispielsweise eine Harnstoffschmelze, so wird der Fluidspiegel 42 im ersten Mischbehälter 12 geringfügig ansteigen. Der geringfügig erhöhten Flüssigkeitsdruck an der Auslassöffnung 28 des ersten Mischbehälters 12 verursacht, dass das im ersten Mischbehälter 12 befindliche Fluid, das eine Mischungszwischenstufe bildet, über die Verbindungsleitung 40 in den zweiten Mischbehälter 14 befördert wird, so dass sich die Fluidspiegel 42, 44 wieder angleichen.If, during operation of the device according to the invention, a base material is fed in via the inlet opening 26 of the
Der erste Mischbehälter 12 weist einen Deckel auf, in dem eine Einführöffnung 46 zum Zumischen eines ersten Stoffs vorgesehen ist. Über die Einführöffnung 46 kann beispielsweise ein Additiv oder ein sonstiger Stoff in den Grundstoff, speziell die Harnstoffschmelze, im ersten Mischbehälter 14 eingebracht werden. Feststoffe sind gegebenenfalls vorzuwärmen. Der erste Stoff wird über die Einführöffnung 46 vorzugsweise kontinuierlich eingebracht. Innerhalb des ersten Mischbehälters wird dadurch eine Mischungszwischenstufe aus dem Grundstoff und dem ersten Stoff hergestellt.The
Der zweite Mischbehälter 14 weist ebenfalls einen Deckel mit einer Einführöffnung 48 auf, durch die ein zweiter Stoff zugemischt werden kann. Der zweite Stoff gelangt durch die Einführöffnung 48 in den zweiten Mischbehälter und wird dort mit der Mischungszwischenstufe, die aus dem Grundstoff und dem ersten Stoff besteht und über die Verbindungsleitung 40 in den zweiten Mischbehälter 48 gelangt ist, vermischt. Nach Zumischen des zweiten Stoffs liegt innerhalb des zweiten Mischbehälters 14 die fertiggestellte Mischung vor, die dann über die Auslassöffnung 34 entnommen werden kann. Die erfindungsgemäße Vorrichtung arbeitet kontinuierlich. Im Betrieb wird somit Grundstoff über die Einführöffnung 26 kontinuierlich zugeführt, der erste Stoff wird über die Einlassöffnung 46 und der zweite Stoff wird über die Einlassöffnung 48 kontinuierlich zugeführt und über die Auslassöffnung 34 kann die fertiggestellte Mischung kontinuierlich entnommen werden.The
Indem ein Fluidtransport von dem ersten Mischbehälter 12 in den zweiten Mischbehälter 14 durch Schwerkrafteinfluss über die Verbindungsleitung 40 erfolgt, kann sowohl innerhalb des ersten Mischbehälters 12 als auch innerhalb des zweiten Mischbehälters 14 eine ausreichende Mischzeit sichergestellt werden. Dadurch wird eine besonders gleichmäßige Mischung aus dem ersten Stoff mit dem Grundstoff zur Herstellung einer Mischungszwischenstufe und dann aus dem zweiten Stoff und der Mischungszwischenstufe im zweiten Mischbehälter sichergestellt werden. Die in jedem Mischbehälter 12, 14 vorgesehenen Rührwerke 18 unterstützen das Herstellen einer besonders gleichmäßigen Mischung.Sufficient mixing time can be ensured both within the
Jeder der Mischbehälter 12, 14 weist an seinem Boden eine weitere Auslassöffnung 50 auf. Diese weitere Auslassöffnung 50 ist beispielsweise zum vollständigen Entleeren der Mischbehälter 12, 14 im Rahmen einer Inspektion oder im Rahmen einer Stilllegung der Vorrichtung vorgesehen. Die Verbindungsleitung 40 ist mit Abzweigen versehen und kann auch, wie die Druckausgleichsleitung 38, mit einem Absperrventil versehen sein. Im Betrieb der Vorrichtung sollen aber sowohl die Druckausgleichsleitung 38 als auch die Verbindungsleitung 40 offen sein, um einen Druckausgleich zwischen den Mischbehältern 12, 14 bzw. einen Fluidtransport zwischen den beiden Mischbehältern 12, 14 zu ermöglichen.Each of the mixing
Die beiden Mischbehälter 12, 14 sind jeweils doppelwandig ausgebildet, so dass jeweils ein Zwischenraum 52 gebildet ist, in dem ein Heizmedium oder Kühlmedium transportiert werden kann. Wird mittels der erfindungsgemäßen Vorrichtung eine Mischung aus einer Harnstoffschmelze und zwei weiteren Stoffen hergestellt, so wird der Zwischenraum 52 jeweils mit einem Heizmedium beaufschlagt, um sicherzustellen, dass die Schmelze nicht bereits teilweise innerhalb der Mischbehälter 12, 14 erstarrt. Auch die Druckausgleichsleitung 38 und die Verbindungsleitung 40 sind jeweils doppelwandig ausgebildet, so dass das Heizmedium auch die Druckausgleichsleitung 38 und die Verbindungsleitung 40 beheizen kann. Auch die Anschlussstutzen der Einlassöffnung 26, der Auslassöffnung 28, der Einlassöffnung 32 und der Auslassöffnung 34 sind jeweils doppelwandig ausgeführt, um diese beheizen zu können und um zu verhindern, dass die Schmelze in diesen Bereichen erstarrt, wodurch sich Ablagerungen bilden könnten. Feststoffe sind gegebenenfalls vorzuwärmen.The two mixing
Ein Heizmedium wird in den Zwischenraum 52 beispielsweise über eine Heizleitung 54 zugeführt.A heating medium is fed into the
Die Darstellung der
Lediglich schematisch angedeutet ist in
Die Einlassöffnung 26 ist mit einem abgewinkelten Rohrstück 56 versehen, das die durch die Einlassöffnung 26 eintretende Schmelze um 90° umlenkt und dadurch etwa tangential zur Mittellängsachse 24 in den Innenraum des ersten Mischbehälters 12 einleitet.The
Das Rohrstück 56 weist, in der Darstellung der
Die Darstellung der
Die Darstellung der
Eine Harnstoffschmelze wird, wie bereits erläutert wurde, über die Einführöffnung 26 dem ersten Mischbehälter 12 zugeführt und dort mit einem ersten Stoff, der über die Einführöffnung 46 zugeführt wird, vermischt. Ausgehend vom ersten Mischbehälter 12 gelangt die Mischungszwischenstufe aus der Harnstoffschmelze und dem ersten Stoff in den zweiten Mischbehälter 14 und wird dort mit einem zweiten Stoff, der über die Einführöffnung 48 zugeführt wird, vermischt. An der Auslassöffnung 34 wird die fertiggestellte Mischung dem zweiten Mischbehälter 14 entnommen und mittels einer Pumpe 72 einer Mahleinheit 74 zugeführt. In der Mahleinheit 74 kann eine Partikelgröße der Mischung, die eine Dispersion aus der Harnstoffschmelze und dem ersten Stoff sowie dem zweiten Stoff bildet, verkleinert werden. Die Mahleinheit 74 kann alternativ auch entfallen.As has already been explained, a urea melt is supplied to the
Ausgehend von der Mahleinheit 74 wird die Mischung dann über eine weitere Verbindungsleitung einer Pastilliervorrichtung 76 zugeführt. Die Pastilliervorrichtung 76 weist eine rotierende gelochte Trommel 78 und eine Düsenleiste auf, die die Mischung von innen her gegen die gelochte Trommel 78 fördert. Mittels der gelochten Trommel werden Schmelzetropfen erzeugt, die dann auf einem umlaufenden Kühlband 80 abgelegt werden. Nach dem Ablegen erstarren die abgelegten Produkttropfen auf dem Kühlband 80 zu Pastillen und können dann als feste Pastillen vom Kühlband 80 abgenommen werden.Starting from the grinding
Eine Rückführleitung 82 führt von einem Abzweig 84 wieder zum zweiten Mischbehälter 14 zurück. Durch diese Rückführleitung 82 kann die fertiggestellte Mischung vom Abzweig 84 nicht nur zu der Pastilliervorrichtung 76, sondern wieder zurück in den zweiten Mischbehälter 14 gelangen. Zum einen ist es dadurch möglich, eine größere Menge an der Mischung in der Verbindungsleitung und der Rückführleitung 82 zirkulieren zu lassen. Dadurch kann beispielsweise sichergestellt werden, dass die Mischung, die ja aus einer Dispersion aus einer Schmelze und weiteren Stoffen besteht, nicht innerhalb der Verbindungsleitung wieder entmischt oder teilweise erstarrt. Darüber hinaus kann die Mischvorrichtung 10 weiter betrieben werden, auch wenn die Pastilliervorrichtung 76 beispielsweise vorübergehend angehalten wird.A
Claims (14)
- Device for admixing at least one first substance and one second substance to a flowable base substance for forming a mixture by means of a continuous mixing operation, in particular for admixing a first substance and a second substance to a urea melt for forming a dispersion, wherein the device for admixing has the following features:a the device (10) for mixing has at least one first mixing vessel (12) and one second mixing vessel (14),b the first and second mixing vessels (12, 14) have in each case one inlet opening (26, 32), in each case one introduction opening (46, 48) for admixture of the first substance and second substance, respectively, in each case one outlet opening (28, 34) and in each case one pressure-equalization opening (30, 36), each of the mixing vessels (12, 14) having at its base a further outlet opening (50), which is intended for complete emptying of the mixing vessels (12, 14),whereinc the first mixing vessel and the second mixing vessel are each provided with a stirrer,d the pressure-equalization openings (30, 36) of the first and second mixing vessels (12, 14) are connected to one another by means of a pressure-equalization line (38) or are open to the surroundings, wherein, during the operation of the device, the pressure-equalization openings (30, 36) are situated above fluid surfaces (42, 44) present in the mixing vessels, ande the outlet opening (28) of the first mixing vessel (12) and the inlet opening (32) of the second mixing vessel (14) are connected to one another by means of a connecting line (40), wherein, during the mixing operation of the device (10), the connecting line (49) is open and the outlet opening (28) of the first mixing vessel (12) and the inlet opening (32) of the second mixing vessel (14) and also the connecting line (40) are situated below the fluid surfaces (42, 44) in the mixing vessels (12, 14), so that fluid can pass from the first mixing vessel (12) into the second mixing vessel (14) under the effect of gravitational force.
- Device for admixing according to Claim 1, characterized in that
the first mixing vessel (12) and the second mixing vessel (14) in each case have a substantially identical basic shape with substantially the same volume and are arranged at substantially the same height. - Device for admixing according to Claim 1 or 2, characterized in that
the outlet opening (28) of the first mixing vessel (12) and the inlet opening (32) of the second mixing vessel (14) are arranged at substantially the same height. - Device for admixing according to one of the preceding claims, characterized in thata the inlet openings (26, 32) and/or the outlet openings (28, 34) of the first and second mixing vessels (12, 14), within the mixing vessels (12, 14), in each case transition into an angled tube piece (56, 58), preferably into a tube piece which is angled away by an angle of 90°, andb the central planes of the angled tube pieces (56, 58) are in each case oriented substantially perpendicularly to a central longitudinal axis (24) of the first or second mixing container (12, 14) .
- Device for admixing according to Claim 4, characterized in thata openings of the angled tube pieces (56, 58) that form the inlet opening or the outlet opening within the mixing vessels (12, 14) in each case face in the same tangential direction as seen parallel to the central longitudinal axis (24) of the first and of the second mixing vessel (12, 14), respectively.
- Device for admixing according to one of the preceding claims, characterized in thata the inlet opening (26) of the first mixing vessel (12) is connected to a base-substance feed, in particular to a feed for urea melt, andb the outlet opening (34) of the second mixing vessel (14) is connected to a device for further processing of the mixture, in particular to a pastillation device (76), to a granulating device or to a device for producing flakes.
- Device for admixing according to one of the preceding claims, characterized in thata the first mixing vessel (12), the second mixing vessel (14), the pressure-equalization line (38) and/or the connecting line (40) have/has a double-walled construction,b intermediate spaces formed by means of the double-walled construction are configured for passing-through of heating or cooling media.
- Device for admixing according to Claim 7, characterized in thata the first and/or second mixing vessel (12, 14) have/has external heat insulation.
- Device for admixing according to either of Claims 7 and 8, characterized in thata the intermediate spaces are connected to a heating device for the heating medium.
- Installation having a device for mixing according to one of the preceding claims, characterized in thata the installation has a base-substance feed,b the installation has at least one first dosing device for a first substance to be admixed to the base substance and has at least one second dosing device for a second substance to be admixed to the base substance,c the installation has a line with a pump (72) arranged in the course thereof for transferring the finished mixture from the second mixing vessel (14) to a pastillation device (76) for pastillation of the mixture, to a granulating device or to a device for producing flakes.
- Installation according to Claim 10, characterized in that
provision is made of a return line (82) for returning the mixture into the second mixing vessel (14), which return line opens out into said second mixing vessel (14) preferably above the fluid surface. - Installation according to Claim 10 or 11, characterized in that
the pastillation device (76) has a rotating and perforated drum (78) and a circulating cooling belt (80) . - Method for admixing at least one first substance and at least one second substance to a base substance for forming a mixture by means of a continuous mixing operation using a device according to one of Claims 1 to 9, wherein the method for admixing has the following features:a a base substance is fed to a first mixing vessel (12),b the first substance for admixture is fed to the base material in the first mixing vessel (12) for forming an intermediate mixture stage,c the intermediate mixture stage from the first mixing vessel (12) is fed to the second mixing vessel (14),d the second substance for admixture is fed to the intermediate mixture stage in the second mixing vessel (14) for forming the mixture,characterized in that
e the feeding of the intermediate mixture stage from the first mixing vessel (12) into the second mixing vessel (14) is realized, utilizing gravitational force, by means of a connecting line (40) between the mixing vessels (12, 14), which connecting line is open during mixing operation and is situated below the fluid surfaces (42, 44) in the mixing vessels (12, 14). - Method according to Claim 13, wherein the method has the following feature:
a the base substance is a melt, in particular a urea melt.
Applications Claiming Priority (2)
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DE102016203293.3A DE102016203293A1 (en) | 2016-03-01 | 2016-03-01 | Apparatus, plant and method for admixing at least a first substance and a second substance to a base material to form a mixture |
PCT/EP2017/054014 WO2017148758A1 (en) | 2016-03-01 | 2017-02-22 | Device, system, and method for mixing at least one first material and a second material so as to form a base material for forming a mixture |
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EP3423179A1 EP3423179A1 (en) | 2019-01-09 |
EP3423179B1 true EP3423179B1 (en) | 2023-08-09 |
EP3423179C0 EP3423179C0 (en) | 2023-08-09 |
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EP17706750.1A Active EP3423179B1 (en) | 2016-03-01 | 2017-02-22 | Device, system, and method for mixing at least one first material and a second material so as to form a base material for forming a mixture |
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EP (1) | EP3423179B1 (en) |
CN (1) | CN109152996B (en) |
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WO (1) | WO2017148758A1 (en) |
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CN109225056A (en) * | 2018-09-17 | 2019-01-18 | 淮北惠源环保科技有限公司 | A kind of urea for vehicle solution heating device |
FR3090401B1 (en) * | 2018-12-21 | 2023-04-28 | Seb Sa | Manufacturing apparatus, mixing machine and/or receiving device for manufacturing a composition from a mixture of formulations |
CN110238966B (en) * | 2019-06-27 | 2023-08-15 | 四川宏华石油设备有限公司 | Mixing device |
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GB125426A (en) * | 1916-07-14 | 1919-04-24 | Chance And Hunt Ltd | An Improved Apparatus for the Treatment of One Liquid with Another. |
GB1310725A (en) * | 1970-09-28 | 1973-03-21 | Cluett Peabody & Co Inc | Method and apparatus for mixing volatile liquid with non-volatile material |
DE3032384A1 (en) * | 1980-08-28 | 1982-07-08 | Sociedad Minera y Metalúrgica de Penarroya España S.A., Madrid | Emulsion plant for heavy oil - esp. for mfg. homogeneous and stable emulsion of fuel oil and water which is fed to fuel burners |
DE4130413C2 (en) * | 1991-09-10 | 1995-05-04 | Mette Manfred | Plant for mixing and / or homogenizing liquid components |
DE10322998B4 (en) * | 2003-02-28 | 2006-06-29 | Dürr Systems GmbH | Twin component paint preparation for a robot vehicle paint spraying assembly and especially a polyurethane paint emulsion pumps the two components under a low pressure to a mixer followed by a homogenizer |
DE10361307A1 (en) * | 2003-11-24 | 2005-06-30 | Romaco Ag Frymakoruma | Apparatus for mixing and dispersing powder in liquid comprises tank containing rotor, into which pumps continuously feed liquid into tank through inlets and dosing unit dispenses fixed amounts of powder from above |
FI122939B (en) * | 2009-06-11 | 2012-09-14 | Outotec Oyj | Method and apparatus for regenerating leach solution in metal leaching processes |
DE102010028774A1 (en) * | 2010-05-07 | 2011-11-10 | Otc Gmbh | Emulsifying device for the continuous production of emulsions and / or dispersions |
CN104555975B (en) * | 2015-01-28 | 2017-01-18 | 江苏华东锂电技术研究院有限公司 | Continuous lithium iron phosphate preparation device and continuous lithium iron phosphate preparation method |
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CN109152996A (en) | 2019-01-04 |
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EP3423179C0 (en) | 2023-08-09 |
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