EP3171110A1 - Appareil d'échange de chaleur à pétrole-gaz aérien à colonne de distillation atmosphérique et procédé d'échange de chaleur - Google Patents
Appareil d'échange de chaleur à pétrole-gaz aérien à colonne de distillation atmosphérique et procédé d'échange de chaleur Download PDFInfo
- Publication number
- EP3171110A1 EP3171110A1 EP16829559.0A EP16829559A EP3171110A1 EP 3171110 A1 EP3171110 A1 EP 3171110A1 EP 16829559 A EP16829559 A EP 16829559A EP 3171110 A1 EP3171110 A1 EP 3171110A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- shell
- water injection
- heat exchange
- stream
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 12
- 238000004821 distillation Methods 0.000 title description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 123
- 238000002347 injection Methods 0.000 claims abstract description 70
- 239000007924 injection Substances 0.000 claims abstract description 70
- 239000011148 porous material Substances 0.000 claims abstract description 7
- 239000010779 crude oil Substances 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 7
- 238000012423 maintenance Methods 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 3
- 229910052719 titanium Inorganic materials 0.000 claims description 3
- 239000010936 titanium Substances 0.000 claims description 3
- 238000005260 corrosion Methods 0.000 abstract description 16
- 230000007797 corrosion Effects 0.000 abstract description 14
- 239000000463 material Substances 0.000 description 3
- 238000005292 vacuum distillation Methods 0.000 description 3
- MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 description 2
- 150000003863 ammonium salts Chemical class 0.000 description 2
- 230000003373 anti-fouling effect Effects 0.000 description 2
- 239000003350 kerosene Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- -1 diesel Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid group Chemical group C(CCCCCCC\C=C/CCCCCCCC)(=O)O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000009991 scouring Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/0066—Multi-circuit heat-exchangers, e.g. integrating different heat exchange sections in the same unit or heat-exchangers for more than two fluids
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F19/00—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F21/00—Constructions of heat-exchange apparatus characterised by the selection of particular materials
- F28F21/08—Constructions of heat-exchange apparatus characterised by the selection of particular materials of metal
- F28F21/081—Heat exchange elements made from metals or metal alloys
- F28F21/086—Heat exchange elements made from metals or metal alloys from titanium or titanium alloys
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F27/00—Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus
- F28F27/02—Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus for controlling the distribution of heat-exchange media between different channels
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F9/00—Casings; Header boxes; Auxiliary supports for elements; Auxiliary members within casings
- F28F9/02—Header boxes; End plates
- F28F9/0246—Arrangements for connecting header boxes with flow lines
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D21/00—Heat-exchange apparatus not covered by any of the groups F28D1/00 - F28D20/00
- F28D2021/0019—Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for
- F28D2021/0059—Other heat exchangers for particular applications; Heat exchange systems not otherwise provided for for petrochemical plants
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/02—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled
- F28D7/024—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being helically coiled the conduits of only one medium being helically coiled tubes, the coils having a cylindrical configuration
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
- F28D7/16—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged in parallel spaced relation
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28G—CLEANING OF INTERNAL OR EXTERNAL SURFACES OF HEAT-EXCHANGE OR HEAT-TRANSFER CONDUITS, e.g. WATER TUBES OR BOILERS
- F28G9/00—Cleaning by flushing or washing, e.g. with chemical solvents
Definitions
- the present invention relates to a field of a chemical industry equipment and a chemical industry method, and in particular to a heat exchange device for atmospheric tower oil-gas and a heat exchange method thereof.
- an atmospheric and vacuum distillation unit divides the crude oil into naphtha, aviation kerosene, diesel, kerosene, vacuum residues and other fractions by distillation.
- the technical distillation level and the stable and efficient operation of this unit are directly relevant to the yield and economical benefits of the subsequent units.
- the overall quality of the crude oil around the world declines, including declined global yield of light crude oil, rising sulfur content, aggregated oleic performance, and increased exploration difficulty, there is thus a large amount of Cl-containing auxiliaries in the processed crude oil.
- the units are generally constructed in such a manner that the corrosion is relieved by upgrading materials and enhancing corrosion-resistant measurements "one removal and three injections". Nevertheless, the corrosion and leakage of the atmospheric tower top heat exchanger are still very serious.
- Most atmospheric tower top heat exchangers are common heat exchangers. Although the grade of materials has been improved because of the anti-corrosion requirements, majority of such atmospheric tower top heat exchangers are still unable to operate for a long period, and tube bundles are likely to be corroded to result in leakage.
- Some of the atmospheric tower top heat exchangers are welded-plate heat exchangers. Although the materials of such heat exchanges are upgraded, it is likely to result in channel occlusion and leakage due to their poor fluctuation resistance and small circulation channel.
- a first technical problem to be solved by the present invention is, in view of the prior art, to provide an heat exchange device for atmospheric tower oil-gas which can effectively avoid the occlusion of the heat exchanger so as to achieve the purpose of preventing the equipment from corrosion, prolonging the operating period and reducing the operating cost.
- a second technical problem to be solved by the present invention is to provide an atmospheric tower oil-gas heat exchange method which can effectively avoid the occlusion of the heat exchanger.
- the heat exchange device for atmospheric tower oil-gas comprises, a heat exchanger, the heat exchanger comprising a shell having a top, a bottom, a tube pass entrance and a tube pass exit; an upper tube plate and a lower tube plate which both are located within the shell; and supported between the upper tube plate and a lower tube plate; an inlet of each heat exchange tube connecting to a tube pass entrance arranged on the bottom of the shell, while an outlet of each heat exchange tube connecting to a tube pass exit arranged on the top of the shell, the tube pass exit and the tube pass entrance used for connecting crude oil flow; a shell pass entrance for connecting to an atmospheric tower oil-gas pipeline arranged on an upper portion of the shell; and a shell pass exit arranged on a lower portion of the shell; characterized in that:
- annular water injection pipe connected to an external water injection pipeline is arranged within the upper portion of the shell, the annular water injection pipe has multiple water pores communicated to the interior of the shell;
- the atmospheric tower oil-gas pipeline is connected to the external water injection pipeline via a first water injection pipeline and a third water injection pipeline;
- a first solenoid valve and a second solenoid valve are respectively arranged on the first water injection pipeline and the third water injection pipeline; and, the annular water injection pipe is communicated to the external water injection pipeline via a second water injection pipeline.
- the shell has a water inlet, and the external water injection pipeline is communicated to the annular water injection pipe via the water inlet.
- the annular water injection pipe is located below the upper tube plate and close to the upper tube plate.
- each heat exchange tube between the upper tube plate and the lower tube plate is coiled around a central axis of the shell.
- a gas outlet which is communicated to the interior of the shell and used for exhausting gas on the top of the shell during maintenance, is further arranged on the top of the shell, and a liquid outlet for discharging liquid on the bottom of the shell during maintenance is further arranged on the bottom of the shell.
- each of the heat exchange tubes is a pure-titanium heat exchange tube.
- the heat exchange method using the heat exchange device for atmospheric tower oil-gas provided in the above solutions comprises the following steps:
- the heat exchange device for atmospheric tower oil-gas and heat exchange method of the present invention under feeding water to the oil-gas pipeline and washing the shell by the annular water injection pipe, the heat exchange efficiency is effectively improved, the anti-fouling performance is excellent and the resistance against HCl-H 2 S-H 2 O corrosion and under-deposit corrosion is great. Moreover, the stubborn phenomena such as corrosion resulted from ammonium salt crystalline deposit and occlusion resulted from ferrous sulfide are avoided, and the problems of frequent occlusion and leakage or even replacement of the atmospheric tower oil-gas/crude oil head exchanger due to its easy corrosion, leakage, channel occlusion or other factors are solved. Meanwhile, the device has a small pressure drop and a stable operation, so that the safe operating period of the device is greatly increased.
- the heat exchange device for atmospheric tower oil-gas comprises:
- An upper tube plate 16 and a lower tube plate 17 are further provided inside the shell 11.
- each heat exchange tube 5 is a pure-titanium heat exchange tube for ensuring the anti-corrosion performance of the heat exchange tubes.
- Upper and lower ends of each of the heat exchange tubes are fixed on the upper tube plate and the lower tube plate respectively.
- a portion of each heat exchange tubes between the upper tube plate 16 and the lower tube plate 17 is coiled around a central axis of the shell 11 in order to improve the heat exchange efficiency.
- An annular water injection pipe 6 is provided inside the shell 11 and located close to the upper tube plate 16 and below the upper tube plate 16. Multiple water pores 61 communicated to the interior of the shell are uniformly distributed on the wall of the annular water injection pipe 6. An inlet of the annular water injection pipe 6 is connected to a second water injection pipeline 32 via the water inlet 15.
- a shell pass entrance 12 is connected to an atmospheric tower oil-gas pipeline 2, a first water injection pipeline 31 and a third water injection pipeline 33 are connected onto the atmospheric tower oil-gas pipeline 2, and both the first water injection pipeline 31 and the third water injection pipeline 33 are connected to an external water injection pipeline 3; and a first solenoid valve 34 and a second solenoid valve 35 are respectively arranged on the first water injection pipeline 31 and the third water injection pipeline 33.
- Water is fed into the atmospheric tower oil-gas pipeline 2 via the first water injection pipeline 31.
- the solenoid valves are used for adjusting the water flow.
- the third water injection pipeline is used for intermittently injecting water into the atmospheric tower oil-gas pipeline 2 for purpose of washing the shell pass at a large water flow.
- Both the first water injection pipeline 31 and the third water injection pipeline 33 are connected to the external water injection pipeline 3, and solenoid valves are respectively provided on the first water injection pipeline 31 and the third water injection pipeline 33.
- the two solenoid valves are connected to a control system (not shown in the Figs). The ON, OFF and degree of opening of the two solenoid valves are controlled by the control system, so that the water injection by each water injection pipeline is controlled.
- a heat exchange method using the atmospheric tower oil-gas head exchange device described above comprising the following steps:
- the atmospheric tower oil-gas has a flow of 43860 kg/h, a temperature of 125°C, a pressure of 0.11 MPaG, and a temperature of 82°C at the outlet after the heat exchange;
- the first stream of injected water has a flow of 1000 kg/h and a temperature of 40°C;
- the crude oil has a flow of 192400 kg/h, a temperature of 32°C at the inlet, a pressure of 2.1 MPaG, and a temperature of 72°C at the outlet after the heat exchange;
- the gas outlet 10 is opened to exhaust atmospheric tower oil-gas gathered in the upper portion of the shell.
- the equipment is disassembled and then washed. Cleaning liquid is injected from the gas outlet 10 and drained from the liquid outlet 19.
- the service life of an existing common atmospheric tower top heat exhauster is about 1 to 2 years, and the whole existing common atmospheric tower top heat exhauster or the whole tube bundle needs to be replaced when corrosion and leakage occur.
- the existing common atmospheric tower top heat exchanger needs to be frequently cleaned due to channel occlusion.
- the equipment body has excellent corrosion resistance and anti-fouling performance, and within two operating periods (i.e., 8 years), no fouling (thus occlusion) and corrosion (thus leakage) occurs. Therefore, a large amount of cost for equipment replacement and maintenance is saved.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510460303.6A CN104964583B (zh) | 2015-07-30 | 2015-07-30 | 常压塔顶油气换热装置及换热方法 |
PCT/CN2016/000416 WO2017016187A1 (fr) | 2015-07-30 | 2016-07-26 | Appareil d'échange de chaleur à pétrole-gaz aérien à colonne de distillation atmosphérique et procédé d'échange de chaleur |
Publications (3)
Publication Number | Publication Date |
---|---|
EP3171110A1 true EP3171110A1 (fr) | 2017-05-24 |
EP3171110A4 EP3171110A4 (fr) | 2018-04-18 |
EP3171110B1 EP3171110B1 (fr) | 2019-03-27 |
Family
ID=54218637
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP16829559.0A Active EP3171110B1 (fr) | 2015-07-30 | 2016-07-26 | Appareil d'échange de chaleur à pétrole-gaz aérien à colonne de distillation atmosphérique et procédé d'échange de chaleur |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP3171110B1 (fr) |
JP (1) | JP6315869B2 (fr) |
KR (1) | KR101848697B1 (fr) |
CN (1) | CN104964583B (fr) |
WO (1) | WO2017016187A1 (fr) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106840905B (zh) * | 2017-04-20 | 2023-04-07 | 重庆科技学院 | 油气管道压力综合教学实验装置 |
JP6933238B2 (ja) * | 2018-12-27 | 2021-09-08 | 栗田工業株式会社 | 蒸留塔の差圧解消方法 |
JP6648814B1 (ja) * | 2018-12-27 | 2020-02-14 | 栗田工業株式会社 | 蒸留塔の差圧解消方法 |
CN110373222A (zh) * | 2019-07-29 | 2019-10-25 | 镇海石化建安工程有限公司 | 一种具有缠绕管式换热器的常减压换热系统及换热工艺 |
CN114440698A (zh) * | 2020-11-05 | 2022-05-06 | 南京科技职业学院 | 一种脱脂碱洗换热器减少管式炉烧穿炉门的方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE566112A (fr) * | 1957-05-21 | |||
JPS5849482Y2 (ja) * | 1977-06-20 | 1983-11-11 | 川崎重工業株式会社 | 煙管式給水ヒ−タ |
JPS5849482A (ja) * | 1981-09-19 | 1983-03-23 | 株式会社 サタケ | 穀粒選別装置 |
JPH09159393A (ja) * | 1995-12-08 | 1997-06-20 | Tokyo Gesuido Energ Kk | 熱交換器のチューブ内壁付着物の剥離促進方法 |
US6283133B1 (en) * | 1997-08-18 | 2001-09-04 | Jgc Corporation | Method for cleaning heavy hydrocarbon scale adhered to heat exchanger and piping structure for cleaning |
CN202902937U (zh) * | 2012-11-02 | 2013-04-24 | 镇海石化建安工程有限公司 | 一种换热器结构 |
CN103453782B (zh) * | 2013-09-18 | 2015-01-28 | 南京都乐制冷设备有限公司 | 三位一体壳管式油气换热器 |
CN103673693A (zh) * | 2013-12-10 | 2014-03-26 | 山东蓝星清洗防腐公司 | 新型原油常压塔顶油气换热器 |
CN104697293A (zh) | 2015-03-03 | 2015-06-10 | 李丽芬 | 米兰花烘干方法 |
CN104697393A (zh) * | 2015-03-16 | 2015-06-10 | 北京中科华誉热泵设备制造有限公司 | 一种配备喷淋式清洗结构的壳管干式蒸发器 |
CN204478881U (zh) * | 2015-03-17 | 2015-07-15 | 江苏国信淮安燃气发电有限责任公司 | 水浴炉加热系统的二次热交换水箱 |
CN204987954U (zh) * | 2015-07-30 | 2016-01-20 | 镇海石化建安工程有限公司 | 常压塔顶油气换热装置 |
-
2015
- 2015-07-30 CN CN201510460303.6A patent/CN104964583B/zh active Active
-
2016
- 2016-07-26 EP EP16829559.0A patent/EP3171110B1/fr active Active
- 2016-07-26 KR KR1020177001699A patent/KR101848697B1/ko active IP Right Grant
- 2016-07-26 WO PCT/CN2016/000416 patent/WO2017016187A1/fr active Application Filing
- 2016-07-26 JP JP2017506929A patent/JP6315869B2/ja active Active
Also Published As
Publication number | Publication date |
---|---|
EP3171110A4 (fr) | 2018-04-18 |
JP2017532388A (ja) | 2017-11-02 |
JP6315869B2 (ja) | 2018-04-25 |
CN104964583B (zh) | 2017-01-11 |
WO2017016187A1 (fr) | 2017-02-02 |
KR20170023989A (ko) | 2017-03-06 |
KR101848697B1 (ko) | 2018-05-28 |
EP3171110B1 (fr) | 2019-03-27 |
CN104964583A (zh) | 2015-10-07 |
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