EP2537804A4 - Verfahren zur herstellung anorganischer oxidpartikel - Google Patents

Verfahren zur herstellung anorganischer oxidpartikel

Info

Publication number
EP2537804A4
EP2537804A4 EP11744831.6A EP11744831A EP2537804A4 EP 2537804 A4 EP2537804 A4 EP 2537804A4 EP 11744831 A EP11744831 A EP 11744831A EP 2537804 A4 EP2537804 A4 EP 2537804A4
Authority
EP
European Patent Office
Prior art keywords
oxide particles
inorganic oxide
producing inorganic
producing
particles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP11744831.6A
Other languages
English (en)
French (fr)
Other versions
EP2537804B1 (de
EP2537804A1 (de
Inventor
Takayuki Maehara
Tadaharu Komatsubara
Yuuya Yamano
Kenichi Ishizu
Makoto Satou
Hiroaki Taira
Hiroshi Kato
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tokuyama Dental Corp
Original Assignee
Tokuyama Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tokuyama Corp filed Critical Tokuyama Corp
Publication of EP2537804A1 publication Critical patent/EP2537804A1/de
Publication of EP2537804A4 publication Critical patent/EP2537804A4/de
Application granted granted Critical
Publication of EP2537804B1 publication Critical patent/EP2537804B1/de
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/32—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of elements or compounds in the liquid or solid state or in non-aqueous solution, e.g. sol-gel process
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C01B13/363—Mixtures of oxides or hydroxides by precipitation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/141—Preparation of hydrosols or aqueous dispersions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/146—After-treatment of sols
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/146—After-treatment of sols
    • C01B33/148—Concentration; Drying; Dehydration; Stabilisation; Purification
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/152—Preparation of hydrogels
    • C01B33/154—Preparation of hydrogels by acidic treatment of aqueous silicate solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/10—Compounds having one or more C—Si linkages containing nitrogen having a Si-N linkage
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3081—Treatment with organo-silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Silicon Compounds (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
EP11744831.6A 2010-02-19 2011-02-18 Verfahren zur herstellung anorganischer oxidpartikel Active EP2537804B1 (de)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2010035111 2010-02-19
JP2010122277 2010-05-28
JP2010149306 2010-06-30
PCT/JP2011/054216 WO2011102548A1 (ja) 2010-02-19 2011-02-18 無機酸化物粒子の製造方法

Publications (3)

Publication Number Publication Date
EP2537804A1 EP2537804A1 (de) 2012-12-26
EP2537804A4 true EP2537804A4 (de) 2015-10-21
EP2537804B1 EP2537804B1 (de) 2017-03-22

Family

ID=44483128

Family Applications (1)

Application Number Title Priority Date Filing Date
EP11744831.6A Active EP2537804B1 (de) 2010-02-19 2011-02-18 Verfahren zur herstellung anorganischer oxidpartikel

Country Status (6)

Country Link
US (2) US9000202B2 (de)
EP (1) EP2537804B1 (de)
KR (1) KR101757015B1 (de)
CN (1) CN102762498B (de)
TW (1) TW201144226A (de)
WO (1) WO2011102548A1 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6152103B2 (ja) * 2012-07-10 2017-06-21 日本板硝子株式会社 金属酸化物を含む粒体の製造方法
JP6147554B2 (ja) * 2013-04-26 2017-06-14 株式会社トクヤマ 疎水性無機酸化物粉末及びその製造方法
CN107552031B (zh) * 2016-07-01 2020-12-11 东联化学股份有限公司 含钛氧化硅材料的制备方法及应用
KR102142386B1 (ko) * 2017-08-31 2020-08-07 가부시키가이샤 도쿠야마 표면 처리 졸겔 실리카 및 그 제조 방법
JP6968632B2 (ja) * 2017-09-07 2021-11-17 扶桑化学工業株式会社 疎水性シリカ粉末
CN107601558A (zh) * 2017-10-25 2018-01-19 广西科技大学 一种微波加热制备纳米二氧化钛的方法
TWI761649B (zh) * 2017-12-27 2022-04-21 日商日揮觸媒化成股份有限公司 多孔二氧化矽粒子及其製造方法
WO2019177004A1 (ja) 2018-03-15 2019-09-19 株式会社トクヤマ 複合酸化物粉末、及びその製造方法
EP3708617A1 (de) * 2019-03-14 2020-09-16 Tata Consultancy Services Limited Zusammensetzung und verfahren zur herstellung einer hydrophoben beschichtung
CN116283041B (zh) * 2023-05-24 2023-08-25 中国电子工程设计院有限公司 一种建筑复合材料及其制备方法和用途

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6090811A (ja) * 1983-10-22 1985-05-22 Nippon Chem Ind Co Ltd:The 高純度シリカの製造法
EP0959102A2 (de) * 1998-05-18 1999-11-24 Shin-Etsu Chemical Co., Ltd. Mit Silan oberflächenbehandelte Kieselsäureteilchen, Verfahren zu ihrer Herstellung und ihre Verwendung
US20020061457A1 (en) * 2000-09-27 2002-05-23 Fuji Xerox Co., Ltd. Toner for developing electrostatic latent image, image forming method and image forming apparatus using the same

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06115925A (ja) 1992-09-30 1994-04-26 Nippon Steel Chem Co Ltd 単分散シリカ微粒子の製造方法
DE19630451C1 (de) * 1996-07-27 1998-01-08 Solvay Deutschland Verfahren zur Herstellung von porösen Polymerkugeln und deren Verwendung
JP3756339B2 (ja) 1998-05-18 2006-03-15 信越化学工業株式会社 シラン表面処理シリカ系微粒子、その製造方法およびそれを含有する有機樹脂組成物
JP4184683B2 (ja) 2002-03-19 2008-11-19 宇部日東化成株式会社 金属酸化物球状粒子およびその製造方法
CN1233556C (zh) * 2003-09-17 2005-12-28 韩志萍 二氧化硅快速沉淀法
JP4611006B2 (ja) * 2004-11-30 2011-01-12 信越化学工業株式会社 球状シリカ微粒子、静電荷像現像用トナー外添剤およびトナー
CN100463851C (zh) 2005-10-26 2009-02-25 太原理工大学 一种超细疏水性二氧化硅的制取方法
CN101495409B (zh) * 2006-07-31 2011-07-27 扶桑化学工业股份有限公司 硅溶胶及其制造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6090811A (ja) * 1983-10-22 1985-05-22 Nippon Chem Ind Co Ltd:The 高純度シリカの製造法
EP0959102A2 (de) * 1998-05-18 1999-11-24 Shin-Etsu Chemical Co., Ltd. Mit Silan oberflächenbehandelte Kieselsäureteilchen, Verfahren zu ihrer Herstellung und ihre Verwendung
US20020061457A1 (en) * 2000-09-27 2002-05-23 Fuji Xerox Co., Ltd. Toner for developing electrostatic latent image, image forming method and image forming apparatus using the same

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Week 198527, Derwent World Patents Index; AN 1985-161525, XP002744259 *
See also references of WO2011102548A1 *

Also Published As

Publication number Publication date
EP2537804B1 (de) 2017-03-22
EP2537804A1 (de) 2012-12-26
WO2011102548A1 (ja) 2011-08-25
CN102762498A (zh) 2012-10-31
US20120323030A1 (en) 2012-12-20
US9000202B2 (en) 2015-04-07
CN102762498B (zh) 2015-11-25
US9079777B2 (en) 2015-07-14
KR101757015B1 (ko) 2017-07-11
KR20130008528A (ko) 2013-01-22
TW201144226A (en) 2011-12-16
US20150056119A1 (en) 2015-02-26

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