EP2512812B1 - Installation destinée à l'impression de récipients - Google Patents

Installation destinée à l'impression de récipients Download PDF

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Publication number
EP2512812B1
EP2512812B1 EP10776542.2A EP10776542A EP2512812B1 EP 2512812 B1 EP2512812 B1 EP 2512812B1 EP 10776542 A EP10776542 A EP 10776542A EP 2512812 B1 EP2512812 B1 EP 2512812B1
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EP
European Patent Office
Prior art keywords
printing
containers
printed
ink
plant according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP10776542.2A
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German (de)
English (en)
Other versions
EP2512812A1 (fr
Inventor
Heinz Till
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dekron GmbH
Original Assignee
Dekron GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Publication of EP2512812A1 publication Critical patent/EP2512812A1/fr
Application granted granted Critical
Publication of EP2512812B1 publication Critical patent/EP2512812B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
    • B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
    • B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
    • B41J2/01—Ink jet
    • B41J2/135—Nozzles
    • B41J2/165—Prevention or detection of nozzle clogging, e.g. cleaning, capping or moistening for nozzles
    • B41J2/16579—Detection means therefor, e.g. for nozzle clogging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
    • B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
    • B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
    • B41J2/01—Ink jet
    • B41J2/17—Ink jet characterised by ink handling
    • B41J2/175—Ink supply systems ; Circuit parts therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
    • B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
    • B41J2/005—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by bringing liquid or particles selectively into contact with a printing material
    • B41J2/01—Ink jet
    • B41J2/17—Ink jet characterised by ink handling
    • B41J2/175—Ink supply systems ; Circuit parts therefor
    • B41J2/17503—Ink cartridges
    • B41J2/17556—Means for regulating the pressure in the cartridge
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
    • B41J29/00—Details of, or accessories for, typewriters or selective printing mechanisms not otherwise provided for
    • B41J29/17—Cleaning arrangements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
    • B41J3/00—Typewriters or selective printing or marking mechanisms characterised by the purpose for which they are constructed
    • B41J3/407—Typewriters or selective printing or marking mechanisms characterised by the purpose for which they are constructed for marking on special material
    • B41J3/4073—Printing on three-dimensional objects not being in sheet or web form, e.g. spherical or cubic objects
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
    • B41J3/00—Typewriters or selective printing or marking mechanisms characterised by the purpose for which they are constructed
    • B41J3/407—Typewriters or selective printing or marking mechanisms characterised by the purpose for which they are constructed for marking on special material
    • B41J3/4073—Printing on three-dimensional objects not being in sheet or web form, e.g. spherical or cubic objects
    • B41J3/40733—Printing on cylindrical or rotationally symmetrical objects, e. g. on bottles

Definitions

  • the invention relates to a system for printing on containers, such as bottles, with at least one printed image (font and / or image pattern) on at least one printing machine with at least one print head, as well as on a thus executed method.
  • containers such as bottles and other packaging are provided with labels so that consumer information can be attached. It is also known that with inkjet printers markings or other information are applied to the packaging, which allow an individualization that does not allow the label printing. Such printing systems work monochrome and are limited to a few printing dots / lines.
  • the drying / crosslinking can be done on the transfer between the carousels.
  • the container or the packaging on a belt in each case on the belt in a division, which is equal to the pitch of the machine to fix, clamp independent transport unit and thus centered successively through the various successively arranged carousels to drive ,
  • This holder would be designed as a pivot bearing, so that drive the container on the carousels and thus be passed to the individual print head of the respective color with the entire surface.
  • a device for multicolor printing of containers is described.
  • the containers are fed to the device via a conveyor in a single-lane container stream and, after passing through a corona tunnel and a sub-section screw, reach a rotor of the device.
  • offset printing stations are formed at regular angular intervals around this machine axis.
  • the containers are each transferred individually via a transport star to one of the printing stations.
  • Each printing step with drying takes place on an angular range of a rotational movement of the rotor of about 50 °, so that the printing of the container is completed before the container reach a container outlet, where they are discharged via a transport star on a conveyor.
  • a device for inspecting filled and sealed containers of the document WO 2004/053471 A1 includes a carousel in which the vessels to be tested are so rotated about their longitudinal axis in that the contents begin to rotate in the vessels sufficiently quickly to whirl up any foreign bodies from the bottom of the vessel. It also comprises a second carousel for bottom-free vessel transport following in the direction of transport, to which at least one inspection device operating in the dark field method is assigned for detecting light-scattering foreign bodies in the filling material. Both carousels are tangent with their subcircles side by side are arranged, that the vessels from the first carousel are directly convertible into the second carousel.
  • bottles which are closed at their container mouth with a closure are first fed to a labeling machine designed as a circulating machine and labeled therein.
  • the labeled bottles reach with a rotating rotor to a container outlet or in a local transport star, which has at its periphery a plurality of receptacles for each bottle and is synchronously, but driven in opposite directions to the rotor.
  • a printing station for generating an imprint on an upper side of the closures is arranged stationarily over the movement path of the bottles or the closures on the transport star.
  • a fluid system for simultaneously and independently controlling multiple printheads of a continuous ink jet printer is disclosed in documents EP 1 013 450 A2 disclosed.
  • Each printhead is controlled by its own printhead interface control box.
  • Ink pumps each providing ink to only one printhead, draw ink from a shared ink container. This is supplied by a regulated vacuum system with negative pressure.
  • Each printhead has an individual ink heater.
  • An ink temperature in the print head is expected to increase rapidly to produce the condensation needed to clean a load plate of the ink jet printer. For example, after a switch-on operation, residual ink which may still be present should be washed into a catching device.
  • An overpressure air pump supplies clean air to each drop generator via air valves to remove ink from the printheads when the printheads are turned off.
  • document DE 100 27 261 A1 shows an ink jet printer with a Drucckopf which is selectively displaceable in a printing position close to a substrate or in a retracted cleaning position.
  • a printing ink is stripped off the nozzle exit surface with a doctor blade on a cleaning head and sucked off with a vacuum generator connected to the cleaning head.
  • the post-published document WO 2010/034375 A1 which falls under Article 54 (3) EPC, discloses a device for applying multiple printing to bottles.
  • the device consists of eight adjoining modules, wherein the modules are each formed by an identical basic unit, which is equipped with the functional elements necessary for the specific task of the respective module.
  • Each basic unit includes, inter alia, a circumferentially driven about a vertical machine axis of the respective module transport element in the form of a transport or process star with a plurality of shots which are provided distributed at a circumference of the transport element at equal angular intervals and each of which recording for secure recording respectively serves a bottle.
  • the transport elements of the individual modules are immediately adjacent to each other and driven in opposite directions, but synchronously, so that the bottles within the device in a multi-deflected transport path with a container inlet at one end of the device and a container outlet at another end of the Device to be moved.
  • the individual bottles are in this case forwarded directly from the transport element of a module to the transport element of the following module.
  • the three modules which connect to a first module form the actual printing modules in which the multiple printing takes place.
  • the modules include one or more printheads.
  • Object of the present invention is to propose a system of the type mentioned, with the help of which in a simple way with reliable function and high print quality, a high printing performance can be achieved.
  • the system of the type mentioned in which the containers are positioned during printing in each case in a position in a station of the printing press Clamping device are inventively designed to the fact that the respective jig after printing the container in the last printing machine leaves this, the printed container separated from the jig and the jig on a rinse pipe.
  • the paint residues can be eliminated from the jigs or on the jigs z. B. by UV, EB or heat radiation.
  • the printing of containers is usually done with inks that are liquid, the print head is usually supplied from a cartridge with the color.
  • the respective printhead with liquid ink (ink) are supplied by several printheads or all the printheads of a printing press from one and the same reservoir with the ink in question are supplied by pumping the ink. This can be done for example via a central rotary feedthrough with a flow channel and a return channel by pumping.
  • a central container within the carousel, from which the print heads are supplied, either each with its own pump or with a central pressure supply.
  • the central container can either be filled via a rotary union or kept constant in level.
  • the ink supply not as a central container, but from individual containers for one or more printheads or as a ring-shaped container each approximately on the pitch circle of the printheads, ie substantially above or preferably below the printhead or the printheads.
  • the preferred arrangement of the reservoir (s) below the printhead (s) has the advantage that there is no static fluid pressure and therefore the individual pumps carrying the fluid are more controllable.
  • the pressure points are applied by an inkjet printer side by side on the container surface.
  • the pressure points should also be provided the possibility to apply pressure points on top of each other, for. B. in transparent or opaque material.
  • a cleaning device to the respective print head which can be designed as a suction and / or defogging device.
  • Such a cleaning device is arranged either between two successive press carousels and / or between an inlet star for the containers to be printed and the downstream printing carousel and / or between a pressure carousel and a downstream outlet star where the respective print head for the cleaning device is easily accessible.
  • the cleaning device can also be designed as a transport star with the same pitch as the inlet star or the outlet star.
  • the respectively to be cleaned printhead is z. B. driven in cleaning intervals each in a cleaning position and brought to a standstill.
  • liquid printing ink (ink) which can be dried with heat and / or crosslinked.
  • Another idea of the invention is to make the printing on the container before it is filled, in particular in a system or a method of the type discussed above.
  • a liquid printing ink (ink) can be used, which can be dried with heat and / or crosslinked.
  • a plasma or IR rays can be applied.
  • the pressure points of the inkjet printer instead of side by side and / or, if necessary, several times, be applied to the color cover one above the other on the container surface, which is advantageous for example in transparent or opaque container wall material.
  • Fig. 1 shown plant for printing on containers has a plurality of successively designed as carousels printing presses 1 for the successive recording of containers to be printed, which be passed from a carousel directly to a subsequent carousel or recorded.
  • the containers to be printed are z. B. passed over a transport device 2 and an infeed starter 3 a first carousel 1 and passed successively directly to other carousels, in each carousel each a printing ink and / or a print pattern is applied to the surface of the respective container.
  • the containers are each received in a jig.
  • the printed containers are each separated from clamping devices and the former is fed via a transport device 4 for further use.
  • the clamping devices freed from the printed containers are led out of the last carousel via a further outlet star 5 and via a return conveyor belt 6 through a paint drying and / or washing unit 7, 8, optionally with a drying / aftertreatment unit 9 to the entrance of the first carousel 1 cleaned and dried again returned.
  • the jigs are abandoned via an inlet star 3 the first carousel, where they are each available for receiving a new container to be printed available, which is supplied via the transport device 2.
  • transition stars between the individual carousels are dispensable in a compact system and clamping devices for the containers to be printed constantly reusable.
  • Fig. 2 schematically illustrates a system for printing on containers with a designed as a carousel printing press 1.
  • a central reservoir 10 for receiving liquid ink (ink) F is associated with the printheads 11 instead of previously known each individual printhead associated cartridges.
  • the ink F is supplied to the printheads 11 from the reservoir 10 via a pump 12 and superfluous ink F returned from the printheads 11 back into the reservoir 10.
  • the storage tank 10 can be refilled when it is empty, but also easily replaced.
  • Fig. 3 illustrates a printing machine in which liquid ink F is received in an external reservoir 10 and fed by means of pumps 12 via a central rotary feedthrough 15 by means of flow channels 13 the individual printheads 11, which are arranged in the carousel of a printing press 1.
  • Fig. 4 refers to a system for printing on containers, in which the printheads 11 are accommodated in the carousel of a printing machine 1 and are supplied with liquid ink F from an internal storage container 10.
  • the level of the ink F in the reservoir 10 is kept constant by supplying ink through a central rotary union 15.
  • the reservoir 10 for ink F immediately below the associated printhead 11 in the form of a carousel printing machine 1, so on the pitch circle of the printheads 11.
  • the arrangement of the reservoir 10 below the printheads 11 has the advantage that no static fluid pressure is present and the pump 12 for supplying the ink F to the printheads 11 is easier to control.
  • the reservoir 10 may be formed as a single container below the respective print head 11 but also as all printheads 11 common ring container.
  • Fig. 6 1 schematically illustrates how the discharge openings 16 of a pressure pot 11 can be supplied with printing ink F at constant pressure by regulating the pump pressure P1 as a function of the rotational speed.
  • a storage container 10 above the respective print head 11 and a return container 17 below the respective print head 11 are provided.
  • the supplied for example via a rotary feedthrough 15 in the return tank 17 ink F is pumped via a pump 12 initially via a flow channel 13 in the reservoir 10 above the respective printhead 11, from where a pressure gradient between reservoir 10 and printhead 11 for the ink supply of the printheads 11 is exploited.
  • This allows a high constancy of the pressures, since a pump vibration does not affect the pressure at the outlet openings 16 of the print head 11.
  • the air cushion within the reservoir 10 acts as a balance, as it does not allow rapid pressure changes. Possibly. If not enough static height, a superposition pressure can be given up.
  • Fig. 8a to 8c illustrate various ways in which a cleaning device relative to the designed as a carousel printing presses 1 a system for printing containers can be assigned to the printheads.
  • a static cleaning device 18 is moved at cleaning intervals in a cleaning position in which a printhead 11 has been brought to a standstill on the carousel of the printing press 1.
  • the cleaning device 18 is located here between the inlet star 3 and the outlet star 5 of the carousel, so that neither to be printed nor printed containers affect the cleaning process.
  • the cleaning of the print heads 11 takes place here discontinuously.
  • the cleaning device 18 is the cleaning device 18 as a transport star with the same Division formed as the inlet star 3 and the outlet star 5.
  • Fig. 8c is a combination of cleaning devices 18 indicated, which is working on the one hand with a stationary cleaning device discontinuously or with a designed as a transport star cleaning device continuously at a plant in which the carousels consecutively connected printing presses 1 directly to the container to be printed without interposition of a transport star on the subsequent carousel hand over or take over.
  • the cleaning devices 18 are located in the vicinity of a carousel in each case in the space between the previous carousel and the subsequent carousel.
  • the cleaning process can be controlled by the respective printed containers, z. B. with a camera, in terms of printed image deviations and cleaned inadmissible deviation of the printhead in question.

Landscapes

  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Ink Jet (AREA)
  • Accessory Devices And Overall Control Thereof (AREA)

Claims (15)

  1. Installation, destinée à imprimer des récipients (B), tels que des bouteilles, avec au moins une image d'impression sur au moins deux imprimantes (1) montées l'une derrière l'autre, pourvue d'au moins une tête d'impression (11) chacune,
    les au moins deux imprimantes (1) montées l'une derrière l'autre étant conçues sous la forme de carrousels destinés à recevoir successivement les récipients (B) à imprimer et les récipients (B) étant transférés ou repris d'un carrousel directement sur un carrousel suivant,
    lors de l'impression, les récipients (B) étant enserrés chacun dans un dispositif de serrage positionné dans un poste de l'imprimante (1)
    après l'impression du récipient (B) dans la dernière imprimante (1), le dispositif de serrage respectif quittant celle-ci, le récipient (B) imprimé étant désolidarisé du dispositif de serrage et le dispositif de serrage étant ramené sur un brin de transport en retour (6) vers l'entrée de la première imprimante (1), pour recevoir un nouveau récipient (B) à imprimer et
    au moins un système de nettoyage (18) susceptible d'être affecté à la tête d'impression (11) respective étant prévu.
  2. Installation selon la revendication 1, caractérisée en ce que les carrousels comportent un nombre identique de postes pour recevoir successivement les récipients (B) à imprimer.
  3. Installation selon l'une quelconque des revendications 1 ou 2, caractérisée en ce que de l'encre d'impression (F) liquide est alimentée par transvasement vers la tête d'impression (11) respective à partir d'un réservoir de réserve (10) pour l'encre d'impression (F) concernée, par l'intermédiaire d'un passage tournant (15) central, pourvu d'un canal aller (13) et d'un canal retour (14) ou évacuée de celle-ci, pour alimenter une ou plusieurs têtes d'impression (11), le réservoir de réserve (10) pour l'encre d'impression (F) concernée étant placé sur le cercle partiel sur lequel se trouve ou se trouvent la tête d'impression (11) ou les têtes d'impression (11)
  4. Installation selon la revendication 3, caractérisée en ce que le réservoir de réserve (10) est placé quasiment directement au-dessus ou en-dessous de la tête d'impression (11) associée.
  5. Installation selon la revendication 3 ou 4, caractérisée en ce que le réservoir de réserve est conçu sous la forme de réservoir annulaire.
  6. Installation selon l'une quelconque des revendications 3 à 5, caractérisée en ce qu'une chute de pression vers un réservoir de retour (17) est exploitée pour l'alimentation de la tête d'impression (11) respective avec de l'encre d'impression (F) liquide à partir d'un réservoir de réserve (10) pour l'encre d'impression (F) concernée.
  7. Installation selon l'une quelconque des revendications précédentes, caractérisée en ce que le système de nettoyage (18) est conçu sous la forme d'un dispositif d'aspiration et/ou d'un dispositif de tamponnage.
  8. Installation selon l'une quelconque des revendications précédentes, caractérisée en ce que le système de nettoyage (18) est placé soit entre deux carrousels imprimante successifs et/ou entre un dispositif d'alimentation en étoile (3) pour les récipients (B) à imprimer et le carrousel d'imprimante (1) placé en aval et/ou entre un carrousel d'imprimante (1) et un dispositif d'évacuation en étoile (5) placé en aval.
  9. Installation selon la revendication 8, caractérisée en ce que le système de nettoyage (18) est conçu sous la forme d'un dispositif de transport en étoile pourvu de la même répartition que le dispositif d'alimentation en étoile (3) ou que le dispositif d'évacuation en étoile (5).
  10. Installation selon l'une quelconque des revendications précédentes, caractérisée en ce qu'à des intervalles de nettoyage, la tête d'impression (11) qui doit être respectivement nettoyée est amenée dans une position de nettoyage et y est mise à l'arrêt.
  11. Installation selon l'une quelconque des revendications précédentes, caractérisée en ce que sur le récipient (B) imprimé, des anomalies de l'image d'impression sont contrôlés et lorsque les anomalies sont inacceptables, la tête d'impression (11) concernée est nettoyée.
  12. Installation selon la revendication 11, caractérisée par une caméra, destiné à contrôler les anomalies de l'image d'impression.
  13. Procédé, servant à faire fonctionner une installation destinée à imprimer des récipients (B), tels que des bouteilles, selon l'une quelconque des revendications précédentes, lors duquel, lors de l'impression des récipients (B), on fait fonctionner tous les carrousels présentant la même vitesse périphérique adaptée au débit respectif.
  14. Procédé selon la revendication 13, caractérisé en ce que lors d'un embouteillage de récipients (b) en aval de l'imprimante (1) l'arrivée de récipients (B) à imprimer vers l'imprimante (1) est bloquée et l'imprimante (1) à puissance nominale prédéfinie identique continue de fonctionner jusqu'à ce que le dernier récipient (B) ait quitté l'imprimante (1).
  15. Procédé selon la revendication 14, caractérisé en ce qu'une fois qu'il a été remédié à l'embouteillage, l'imprimante (1) est d'abord réglée une nouvelle fois à la puissance nominale prédéfinie et ce n'est qu'après que l'arrivée des récipients (B) à imprimer est de nouveau libérée.
EP10776542.2A 2009-12-15 2010-09-25 Installation destinée à l'impression de récipients Active EP2512812B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009058219A DE102009058219A1 (de) 2009-12-15 2009-12-15 Anlage zum Bedrucken von Behältern
PCT/EP2010/005869 WO2011082721A1 (fr) 2009-12-15 2010-09-25 Installation destinée à l'impression de récipients

Publications (2)

Publication Number Publication Date
EP2512812A1 EP2512812A1 (fr) 2012-10-24
EP2512812B1 true EP2512812B1 (fr) 2019-09-18

Family

ID=43500251

Family Applications (1)

Application Number Title Priority Date Filing Date
EP10776542.2A Active EP2512812B1 (fr) 2009-12-15 2010-09-25 Installation destinée à l'impression de récipients

Country Status (6)

Country Link
US (2) US20120255450A1 (fr)
EP (1) EP2512812B1 (fr)
CN (1) CN102753352B (fr)
BR (1) BR112012014766B1 (fr)
DE (1) DE102009058219A1 (fr)
WO (1) WO2011082721A1 (fr)

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DE102013110108A1 (de) * 2013-09-13 2015-03-19 Khs Gmbh Drucksystem zum Bedrucken von Flaschen oder dergleichen Behältern sowie Druckvorrichtung oder –maschine mit einem solchen Drucksystem
EP2942195B1 (fr) * 2014-05-02 2018-04-18 PackSys Global (Thailand) Ltd. Machine d'impression d'articles creux
DE102014110520A1 (de) * 2014-07-25 2016-01-28 Krones Ag Direktdruckmaschine mit Tintenversorgungssystem
DE102014225405A1 (de) 2014-12-10 2016-06-16 Krones Ag Direktdruckmaschine zur Bedruckung von Behältern
DE102015114344A1 (de) 2015-08-28 2017-03-02 Khs Gmbh Behälterbehandlungsvorrichtung sowie Verfahren zum Behandeln von Behältern
CN108372715A (zh) * 2018-04-12 2018-08-07 宜春市同茂印务有限公司 一种古籍用高仿古印刷设备

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CN102753352A (zh) 2012-10-24
EP2512812A1 (fr) 2012-10-24
CN102753352B (zh) 2015-01-07
DE102009058219A1 (de) 2011-06-16
WO2011082721A1 (fr) 2011-07-14
US20120255450A1 (en) 2012-10-11
BR112012014766A2 (pt) 2016-03-29
BR112012014766B1 (pt) 2020-05-05
US20170197446A1 (en) 2017-07-13

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