EP2313319B1 - Verfahren zum verpacken eines fluidprodukts in einem spender - Google Patents

Verfahren zum verpacken eines fluidprodukts in einem spender Download PDF

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Publication number
EP2313319B1
EP2313319B1 EP09772731A EP09772731A EP2313319B1 EP 2313319 B1 EP2313319 B1 EP 2313319B1 EP 09772731 A EP09772731 A EP 09772731A EP 09772731 A EP09772731 A EP 09772731A EP 2313319 B1 EP2313319 B1 EP 2313319B1
Authority
EP
European Patent Office
Prior art keywords
reservoir
fluid
inert gas
air
vacuum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Not-in-force
Application number
EP09772731A
Other languages
English (en)
French (fr)
Other versions
EP2313319A2 (de
Inventor
Stéphane DESRUES
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AirlesSystems SAS
Original Assignee
AirlesSystems SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by AirlesSystems SAS filed Critical AirlesSystems SAS
Publication of EP2313319A2 publication Critical patent/EP2313319A2/de
Application granted granted Critical
Publication of EP2313319B1 publication Critical patent/EP2313319B1/de
Not-in-force legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65BMACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B31/00Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
    • B65B31/02Filling, closing, or filling and closing, containers or wrappers in chambers maintained under vacuum or superatmospheric pressure or containing a special atmosphere, e.g. of inert gas
    • B65B31/025Filling, closing, or filling and closing, containers or wrappers in chambers maintained under vacuum or superatmospheric pressure or containing a special atmosphere, e.g. of inert gas specially adapted for rigid or semi-rigid containers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B11/00Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
    • B05B11/0005Components or details
    • B05B11/0097Means for filling or refilling the sprayer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B11/00Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
    • B05B11/01Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use characterised by the means producing the flow
    • B05B11/02Membranes or pistons acting on the contents inside the container, e.g. follower pistons
    • B05B11/028Pistons separating the content remaining in the container from the atmospheric air to compensate underpressure inside the container

Definitions

  • the present invention relates to a fluid product conditioning method in a fluid dispenser comprising a reservoir filled with fluid product defining an opening and a fluid dispenser member such as a pump or a valve.
  • the dispensing member is intended to be mounted in a sealed manner on the opening of the reservoir to thereby constitute the fluid dispenser.
  • This type of dispenser is frequently used in the fields of cosmetics, perfumery or pharmacy to condition various fluid products, such as perfumes, creams, gels, lotions, or powders.
  • Some fluid products are likely to deteriorate when in contact with the air. For example, they may dry out or oxidize.
  • the documents are known EP-0 509 179 and EP-0 481 854 . These documents describe vacuum filling and sealing processes.
  • a vacuum chamber is used in which the reservoir and / or the dispensing member to be sealed to the reservoir are arranged. In the filling process, the vacuum chamber contains only the reservoir, and fluid is injected into the reservoir, while a vacuum prevails inside the enclosure. This ensures that there will be no inclusion of air inside the fluid product.
  • the object of the present invention is to remedy the aforementioned disadvantage of the prior art by defining a new packaging method which can be used in place of or in addition to the vacuum filling and sealing processes of the art. prior.
  • the present invention provides a fluid product conditioning method in a fluid dispenser comprising a fluid reservoir defining an opening and a fluid dispenser member, such as a pump or a valve, for to be mounted in a sealed manner on the opening of the reservoir, an inert gas, such as nitrogen or argon, being present in the reservoir above the fluid during the sealed assembly of the dispenser member on the opening of the reservoir, such that the fluid product is in contact with the inert gas in the reservoir, characterized in that the step of sealing assembly of the dispensing member on the opening of the reservoir is carried out under vacuum , the inert gas is at least partially removed from the reservoir during this evacuation step, so that the reservoir is subjected to a vacuum of inert gas.
  • an inert gas such as nitrogen or argon
  • the air initially contained in the reservoir is removed, for example by suction, and then the inert gas is allowed to enter the reservoir instead of air.
  • the inert gas is allowed to enter the reservoir instead of air.
  • the fluid filling and / or sealing of the dispensing member on the reservoir can be carried out at atmospheric pressure with inert gas inside the reservoir above the fluid.
  • the packaging method of the invention may comprise a step of filling the reservoir with fluid, the air being replaced by the inert gas before and / or after this filling step.
  • the filling step is carried out under vacuum of air or inert gas, the tank being returned to atmospheric pressure by letting inert gas enter the tank.
  • the purge is performed with an inert gas at a pressure at least equal to atmospheric pressure, this to ensure that the fluid does not come into contact with the air.
  • a gas heavier than air such as argon, the inert gas can remain inside the tank above the fluid even at atmospheric pressure.
  • the tank thus filled with fluid and inert gas can pass to the next station where the dispensing member is sealingly mounted on the tank, this operation can be performed at atmospheric pressure.
  • a gas evacuation before assembly is preferable, especially when it is an "airless" tank, which should contain only fluid.
  • the spirit of the invention lies in the fact of performing at least some fluid product conditioning operations in an inert gas atmosphere at least at the reservoir, so that after conditioning, the fluid product is not in contact with air, but in contact with an inert gas that does not interact with the fluid and thus guarantees its perfect preservation.
  • the present invention consists of a packaging process which is carried out by means of a suitable packaging device for the purpose of producing a fluid dispenser which incorporates the results of the packaging process.
  • the two conditioning devices represented on the Figures 1 and 2 are very similar in that they each comprise a vacuum chamber 4, an inlet of inert gas 43 connected to a source of inert gas G, an outlet 44 connected to a vacuum pump V to evacuate the enclosure 4, and a filling station 5 or a waterproof mounting station 6.
  • the enclosure 4 comprises a lower bucket 41 and an upper bell 42 or 42 ', tightly attached to one another to create an interior space in which we can make a vacuum prevail.
  • the inlet of inert gas 43 and the outlet 44 are located at the bell 42, 42 '.
  • bell 42 is equipped with a filling station 5 through which fluid product P can be injected into the interior of the bell.
  • the bell 42 ' is equipped with a sealed mounting station 6, which may for example be a crimping station or snap.
  • the packaging method and the packaging devices of the invention are intended to condition fluid product P inside a fluid dispenser comprising, inter alia, a fluid reservoir and a dispenser member, such as a pump or a valve, intended to be mounted sealingly on the reservoir.
  • the dispensing member can be of any kind as mentioned above, and is therefore not limited only to a pump or a valve.
  • the tank it can also be of any kind, of constant or variable capacity, rigid or deformable nature, or further comprising a movable element to vary its capabilities. Given the purpose of the present invention, namely a perfect preservation of the fluid within the tank, it is of course preferable that the amount of fluid extracted from the tank is not replaced by an equivalent volume of outside air .
  • the tank 1 is of the piston-follower type. More specifically, the reservoir 1 comprises a cylindrical sliding shaft 11 which is extended by forming a neck 12 defining internally an opening 13 communicating the interior of the barrel 11 with the outside.
  • the reservoir 1 also comprises a follower piston 14 which is slidably engaged inside the barrel 11.
  • the follower piston 14 is intended to move inside the barrel 11 as fluid is extracted therefrom. .
  • the displacement of the follower piston 14 is generated by a depression created inside the reservoir. All this is quite conventional for this type of piston-follower tank.
  • the dispensing member 2 is only shown on the figure 2 .
  • a fixing ring 3 is used which is only very schematically. It may be a crimping ring or a snap ring. It is even possible to use a screw ring. The essential thing is that the ring 3 carries a tight assembly of the pump 2 on the neck 12 of the tank.
  • the tank 1 is introduced inside the cup 41 of the chamber 4, and the bell 42 completes the chamber 4 to isolate the interior of the chamber 4 from the outside.
  • the interior of the tank 1, as well as the outside of the tank, are subjected to the same pressure prevailing inside the chamber 4.
  • the filling station 5 extends inside the bell 42 so as to penetrate at least partially inside the neck 12 to inject fluid into the tank.
  • the air that is present inside the chamber 4 is evacuated through the outlet 44 connected to the vacuum pump V.
  • the vacuum pump V there is a void of air inside the enclosure 4.
  • air inside the chamber 4 there is more or less air inside the chamber 4: we can make a vacuum that tends to 100%.
  • an inert gas is introduced inside the chamber 4 through the inlet 43 connected to the source of inert gas G. Since there is an air gap inside the enclosure 4, it is sufficient to let the inert gas enter the enclosure G through the inlet 43.
  • the filling operation can be performed under vacuum, but this is not an air vacuum, but a vacuum of inert gas.
  • the enclosure 4 filled with inert gas it can evacuate the enclosure by means of the vacuum pump V through the outlet 44.
  • the enclosure is then partially or completely emptied of its contents, which is the inert gas.
  • the filling operation can then begin under this vacuum of inert gas.
  • the vacuum of inert gas can be broken and the chamber 4 can then be opened by moving the cup 41 relative to the bell 42.
  • the tank is then at atmospheric pressure and / or ambient air, depending on which a vacuum or not was made in the enclosure.
  • the opening of the chamber 4 causes a dispersion in the atmosphere of the inert gas.
  • a substantially heavy inert gas as is the case with argon
  • the empty space of fluid inside the tank above the fluid can remain filled with inert gas. It then suffices during a subsequent sealed mounting step to mount the dispensing member 2 in the opening of the reservoir 12 sealingly.
  • the empty space of fluid inside the tank is then mainly filled with inert gas. It is thus possible to implement the present invention without producing a vacuum.
  • the opening of the enclosure 4 when the filling operation has been carried out under vacuum, the opening of the enclosure 4 generates an introduction of air inside the tank 1 above the fluid product. It is in this case preferable to perform a sealed mounting operation of the dispenser member on the reservoir under vacuum conditions.
  • inert gas may be introduced into the tank after the filling operation, which has been carried out at atmospheric pressure. It will be necessary to purge with an inert gas, which will ensure complete protection of the fluid filled.
  • a complete fluid product dispenser is introduced inside the enclosure 4.
  • the dispenser comprises a reservoir 1, such as that of the figure 1 as well as a dispensing member 2 arranged in an unsealed manner in the opening 12 of the reservoir.
  • the distributor also comprises a fixing ring 3 which is non-definitively mounted and therefore not sealed on the dispensing member 2.
  • the reservoir 1 is filled with fluid product P to a level close to the opening 12.
  • there remains a space E which is empty of fluid and which is therefore initially filled with air.
  • the enclosure is closed: however the space E is subjected to the same pressure as that prevailing in the rest of the enclosure outside the tank, since there is no sealing between the dispensing member 2 and the reservoir.
  • the air initially contained inside the chamber 4 is replaced by an inert gas.
  • This operation can be carried out in the same way as in the first implementation of the figure 1 .
  • the air of the enclosure can be evacuated through the outlet 44 using the vacuum pump V, then inert gas can be introduced inside the chamber 4 emptied of its air through the 43 to the gas source G.
  • the air contained inside the chamber 4 can be removed by the injection pressure of inert gas inside the chamber.
  • the air is flushed or vented through exit 44 directly open to the atmosphere. In both cases, we end up with an enclosure 4 filled with inert gas. Therefore, the space E is filled with inert gas.
  • the implementations of the packaging method according to the invention Figures 1 and 2 can be performed successively or independently of one another.
  • the filling operation and / or the sealed mounting operation can be carried out under vacuum or not. If inert gas remains above the fluid within the tank 1 after the filling operation, the mounting operation can be carried out at atmospheric pressure. However, this will rarely be used, because the operation of the dispenser will not be optimal, especially for "airless" distributors without outside air intake.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Vacuum Packaging (AREA)
  • Nozzles (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Claims (6)

  1. Verfahren zum Konditionieren eines Fluidproduktes (P) in einen Spender für ein Fluidprodukt, aufweisend einen Fluidproduktbehälter (1), der eine Öffnung (13) begrenzt, und ein Spenderelement (2) für ein Fluidprodukt, wie eine Pumpe oder ein Ventil, das dazu gedacht ist, dichtend auf der Öffnung (13) des Behälters montiert zu werden, wobei sich bei der dichtenden Montage des Spenderelements (2) auf der Öffnung (13) des Behälters in dem Behälter ein Inertgas, wie Stickstoff oder Argon, über dem Fluidprodukt (P) befindet, so dass das Fluidprodukt (P) in dem Behälter (1) mit Inertgas in Kontakt steht,
    dadurch gekennzeichnet, dass der Schritt des dichtenden Montierens des Spenderelements (2) auf der Öffnung (13) des Behälters (1) in Vakuum erfolgt und das Inertgas bei diesem Schritt des Vakuumierens zumindest teilweise derart aus dem Behälter abgezogen wird, dass der Behälter frei von Inertgas ist.
  2. Verfahren zum Konditionieren nach Anspruch 1, aufweisend das Austreiben von Luft aus dem Behälter (1) und das anschließende Zulassen des Eindringens des Inertgases in den Behälter.
  3. Verfahren zum Konditionieren nach Anspruch 1, aufweisend das Austreiben von Luft aus dem Behälter (1) mit dem Inertgas.
  4. Verfahren zum Konditionieren nach einem der vorhergehenden Ansprüche, aufweisend einen Schritt des Befüllens des Behälters (1) mit Fluidprodukt, wobei die Luft vor diesem Schritt des Befüllens durch das Inertgas ersetzt wird.
  5. Verfahren zum Konditionieren nach einem der vorhergehenden Ansprüche, aufweisend einen Schritt des Befüllens des Behälters (1) mit Fluidprodukt, wobei die Luft nach diesem Schritt des Befüllens durch das Inertgas ersetzt wird.
  6. Verfahren zum Konditionieren nach Anspruch 5, wobei der Schritt des Befüllens in einem Luftvakuum oder Inertgas-Vakuum vorgenommen wird, wobei der Behälter (1) wieder unter atmosphärischen Druck gesetzt wird, indem das Eindringen von Inertgas in den Behälter zugelassen wird.
EP09772731A 2008-07-01 2009-06-30 Verfahren zum verpacken eines fluidprodukts in einem spender Not-in-force EP2313319B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0854438A FR2933380B1 (fr) 2008-07-01 2008-07-01 Procede de conditionnement de produit fluide dans un distributeur
PCT/FR2009/051262 WO2010001049A2 (fr) 2008-07-01 2009-06-30 Procede de conditionnement de produit fluide dans un distributeur

Publications (2)

Publication Number Publication Date
EP2313319A2 EP2313319A2 (de) 2011-04-27
EP2313319B1 true EP2313319B1 (de) 2011-12-07

Family

ID=40297652

Family Applications (1)

Application Number Title Priority Date Filing Date
EP09772731A Not-in-force EP2313319B1 (de) 2008-07-01 2009-06-30 Verfahren zum verpacken eines fluidprodukts in einem spender

Country Status (8)

Country Link
US (1) US8726615B2 (de)
EP (1) EP2313319B1 (de)
CN (1) CN102076566B (de)
AT (1) ATE536309T1 (de)
BR (1) BRPI0913917A2 (de)
ES (1) ES2378336T3 (de)
FR (1) FR2933380B1 (de)
WO (1) WO2010001049A2 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
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FR3019531B1 (fr) * 2014-04-04 2019-08-09 Techniplast Procede d'extraction de liquide d'un appareil de distribution de liquide par injection de gaz
FR3036389B1 (fr) * 2015-05-18 2019-08-23 Aptar France Sas Procede et dispositif de remplissage de reservoir.
EP3472052A4 (de) * 2016-06-16 2020-01-22 Muffin Incorporated Phiolenfüllsystem mit lokalisierter reinzone
ES2883723T3 (es) * 2017-07-11 2021-12-09 Becton Dickinson France Dispositivo de taponamiento por vacío y tubo de purga de un recipiente médico
FR3083721B1 (fr) 2018-07-12 2020-12-18 Aptar France Sas Dispositif de distribution de produit fluide et son procede de remplissage et de bouchage.
FR3087360B1 (fr) * 2018-10-19 2021-06-04 Promens Sa Procede de remplissage d'un reservoir d'un dispositif de distribution du type sans reprise d'air
CN110282168A (zh) * 2019-05-20 2019-09-27 珠海市维启自动化设备有限公司 粉末充进机
WO2020234842A1 (en) * 2019-05-23 2020-11-26 G.D Societa' Per Azioni Filling unit to fill a container, in particular a cartridge, with a liquid product of the pharmaceutical industry
EP4139213A1 (de) 2020-02-28 2023-03-01 Taramar Seeds Ehf. Kosmetische formulierungen mit einer argondecke und einem internen argonreservoir sowie herstellungsverfahren dafür
CA3173770A1 (en) * 2021-06-25 2022-12-25 Jon Austin LUBOW Systems and methods of preserving customized cosmetic products

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Also Published As

Publication number Publication date
US20110146207A1 (en) 2011-06-23
US8726615B2 (en) 2014-05-20
CN102076566A (zh) 2011-05-25
WO2010001049A3 (fr) 2010-02-25
BRPI0913917A2 (pt) 2015-10-20
ES2378336T3 (es) 2012-04-11
FR2933380B1 (fr) 2013-01-18
EP2313319A2 (de) 2011-04-27
ATE536309T1 (de) 2011-12-15
FR2933380A1 (fr) 2010-01-08
CN102076566B (zh) 2012-12-05
WO2010001049A2 (fr) 2010-01-07

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