EP1901849A1 - Drei-phasen-vollmantel-schneckenzentrifuge und verfahren zur regelung des trennprozesses - Google Patents
Drei-phasen-vollmantel-schneckenzentrifuge und verfahren zur regelung des trennprozessesInfo
- Publication number
- EP1901849A1 EP1901849A1 EP06754000A EP06754000A EP1901849A1 EP 1901849 A1 EP1901849 A1 EP 1901849A1 EP 06754000 A EP06754000 A EP 06754000A EP 06754000 A EP06754000 A EP 06754000A EP 1901849 A1 EP1901849 A1 EP 1901849A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- drum
- phase
- screw centrifuge
- disc
- solid bowl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007787 solid Substances 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims description 19
- 230000008569 process Effects 0.000 title description 11
- 239000012071 phase Substances 0.000 claims abstract description 52
- 239000007791 liquid phase Substances 0.000 claims abstract description 40
- 239000007788 liquid Substances 0.000 claims abstract description 15
- 238000000926 separation method Methods 0.000 claims description 32
- 230000008859 change Effects 0.000 claims description 15
- 239000012530 fluid Substances 0.000 claims description 9
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 8
- 239000000839 emulsion Substances 0.000 claims description 6
- 238000011144 upstream manufacturing Methods 0.000 claims description 6
- 230000033228 biological regulation Effects 0.000 claims description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
- 229910017052 cobalt Inorganic materials 0.000 claims description 4
- 239000010941 cobalt Substances 0.000 claims description 4
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- 239000010949 copper Substances 0.000 claims description 4
- 229910052759 nickel Inorganic materials 0.000 claims description 4
- 238000005191 phase separation Methods 0.000 claims description 3
- 238000011084 recovery Methods 0.000 claims description 3
- 241000237858 Gastropoda Species 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract 1
- 239000011343 solid material Substances 0.000 abstract 1
- 238000005352 clarification Methods 0.000 description 8
- 239000007790 solid phase Substances 0.000 description 6
- 238000010586 diagram Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 230000001276 controlling effect Effects 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 240000007817 Olea europaea Species 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 230000012447 hatching Effects 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 230000010363 phase shift Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B1/00—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
- B04B1/20—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B11/00—Feeding, charging, or discharging bowls
- B04B11/02—Continuous feeding or discharging; Control arrangements therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B11/00—Feeding, charging, or discharging bowls
- B04B11/08—Skimmers or scrapers for discharging ; Regulating thereof
- B04B11/082—Skimmers for discharging liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B13/00—Control arrangements specially designed for centrifuges; Programme control of centrifuges
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B1/00—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
- B04B1/20—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl
- B04B2001/2083—Configuration of liquid outlets
Definitions
- the invention relates to a three-phase solid bowl screw centrifuge (three-phase decanter) according to the preamble of claim 1 and a method for controlling the separation process with such a centrifuge.
- US Pat. No. 3,623,656 shows a three-phase decanter with which two liquid phases and one solid phase can be discharged from the drum.
- the liquid outlets can be adjusted by a conversion of the machine when the machine stops.
- WO 03/074 185Al shows a three-phase decanter, with which also two liquid phases and one solid phase can be derived from the drum. With a weir, the flow rate of the heavier liquid phase can be adjusted.
- DE 38 22 983 A1 shows a three-phase decanter, with which also two liquid phases and one solid phase can be derived from the drum, one liquid phase being diverted through a weir and the other through a paring disc.
- DE 195 00 600 C1 and DE 102 23 802 A1 show two-phase decanters in which the liquid is discharged from a chamber by means of a paring disc.
- WO 02/062483 A1 shows a method for operating a solid-bowl slug centrifuge.
- DE 26 17 692 A1 discloses a solid bowl screw centrifuge with a plurality of disk packs from separating discs and a plurality of screw portions.
- Conversion parts are generally available for adapting to the respective product properties or for adapting the process to the respective conditions in the case of three-phase separating decanters.
- the invention has the object of reducing the design effort to create a slightly changed in itself product properties adaptable three-phase decanter and specify an advantageous method for its operation.
- the invention initially provides a three-phase solid bowl screw centrifuge comprising: a rotatable drum and a screw disposed in the drum, at least one solids discharge at one axial end of the drum and at least two or more liquid outlets at the other axial end thereof various dense liquid phases - a lighter liquid phase and a heavier liquid phase - the one liquid outlet being one in ner peeling chamber arranged peeling disk and wherein the other liquid outlet is formed like an overflow, wherein the peeling disk two Regulierusionn preferably the same inner diameter are connected upstream, extending radially from outside to inside and between which a siphon dives in the peeling chamber of the inner circumference extends to the outside, so that between the siphon disc and the paring disc as axial boundaries, the inner radius of the lighter liquid phase in this axial region and the inner shell in the peeling chamber in operation, an annular chamber is formed in the at least one fluid line to change the pressure in the Ring chamber opens, via or through which the pressure in the annular chamber is variable to change the separation zone
- the annular chamber as means for changing the pressure in the annular chamber on a fluid line for supplying a fluid, in particular a gas in the annular chamber.
- the overflow for the other phase can be realized by radial discharge pipes, which pass through the drum shell or lid.
- This basic structure can be realized in particular in two variants: in one, the heavier liquid phase is diverted through the discharge tube and the lighter one through the paring disc and the other the lighter liquid phase through the discharge tube and the heavier one through the paring disc. Both variants allow a good control of the process, but lead to different rule characteristics.
- the invention also provides a method of operating a three-phase solid bowl screw centrifuge according to any one of the preceding claims, wherein the control of the separation process in the drum in the simplest way by changing the pressure in the annular chamber as a control variable. This variant is preferred because a simple and good control of the separation process is possible.
- the regulation of the separation process in the drum takes place as a controlled variable as a function of the concentration in the solid phase or in one or both of the liquid phases derived.
- the invention is also particularly suitable for phase separation in the recovery of hydrometals such as e.g. Cobalt, nickel, copper.
- the formation of emulsions during the extraction can not be avoided.
- the extraction and the emulsion consist of three phases, an organic phase, an aqueous phase and solids.
- the open settling tanks of the extraction are susceptible to contamination from the air. These different dust concentrations lead to a density difference of the individual phases in the emulsion.
- the decanter according to the invention provides a remedy.
- the separation diameter within the decanter can be adjusted online by applying pressure to the annulus. This separates the emulsion cleanly into the three phases.
- hydrometals such as e.g. Cobalt, nickel, copper thus offers considerable advantages.
- FIG. 2 is a schematic sectional view of a portion of the Vollmantel
- 3 is a schematic sectional view of a portion of the solid shell
- Fig. 4 is a diagram for illustrating the performance
- FIG. 1 Controllability of separation and clarification processes with the solid bowl centrifuge according to the invention from FIG. 1; 5 is a sectional view of a second three-phase
- FIG. 6 is a schematic sectional view of a portion of the solid shell
- FIG. 7 shows a schematic sectional view of a partial region of the solid bowl centrifuge from FIG. 5 in a second operating state
- Fig. 8 is a diagram for illustrating the performance and the
- Fig. 1 and 5 show parts of three-phase solid bowl screw centrifuges, which has a rotatably mounted (bearing 17) drum 1 - here with a horizontal axis of rotation - and arranged in the drum 1 rotatable screw 2 with a screw body 3, on which a circumferential Schneckenblatt 4 is arranged.
- the drum 1 and the screw 2 rotate at different speeds n, m about the same axis of rotation (at the diameter D 0 ).
- a bearing 16 is arranged between drum 1 and screw body 3.
- the second bearing of the screw is located on the solid side (not shown here).
- both the drum 1 and the screw 2 for example conical, taper at one end.
- a solids discharge 24 is arranged for the solid phase S transported by the screw to this end of the drum 1, whereas two liquid phases LL and FIL separable from each other in the centrifugal field - a lighter and a heavier liquid phase - Area of the opposite cylindrical end of the drum 1, which is closed by a drum cover 5, are derived from the drum 1.
- a baffle plate 18 may for example be arranged on the worm body 3 in the transition region to the tapering section.
- An inlet pipe 19 here extends, for example, from the cylindrical end of the drum 1 into the drum 1. It opens into a distributor 20, via which the product is passed into the drum 1.
- the drum cover 5 has several openings or openings 21, 22 which pass axially through the drum cover. Preferably, between four and eight such openings on a circle of a predetermined diameter circumferentially distributed in the drum cover 5 are formed.
- first openings 21 - A portion of these openings - hereinafter referred to as first openings 21 - is formed in the manner of one-sided closed recesses (or in the manner of blind holes) and serves to drain the heavier liquid phase HL and a portion of these openings - hereinafter referred to as second openings 22 - serves to discharge the lighter liquid phase LL.
- FIGS. 1 and 5 are the same.
- the regions of the decanter 1 arranged downstream of the first and second openings are arranged, as it were, "reversed", or the separating rifle is located in front of the openings leading to the paring disc 9.
- the heavier-fluid phase-gathering radially further outward-via the cutting-off rifle 6 on the drum cover is guided in each case into a chute which adjoins the cutting-off rifle 6 over a part of the circumference of the cutting rifle 6.
- tion space 7 - here formed by the openings 21 itself - directed.
- discharge spaces 7 each projecting the drum shell passing discharge pipes 8, wherein the inner radius to which the respective discharge pipe 8 extends, also miter the drain radius for the heavier liquid phase HL.
- This discharge radius for the heavier phase HL is not variable during operation or during a running process, but it can be changed or set at a standstill of the drum 1 by exchanging the discharge tube 8 and the tube against one with a different length.
- the derivative of the lighter liquid phase LL takes place after passing through the second openings 22 by means of a paring disc 9, which is arranged in a peel chamber 10 upstream of the drum shell, which connects axially to the drum interior and whose inner diameter is equal to or - preferably - smaller than that Inner diameter of the drum 1 in its cylindrical portion.
- the light liquid phase LL is discharged through this peeling disk 9 and a subsequent discharge channel 23 from the drum.
- the peeling disk 9 are connected to the interior of the drum - see also Figs. 2 and 3 - in the peeling chamber 10 axially upstream two regulating disks 11, 12 of the same inner diameter, which extend radially from outside to inside and between which a siphon disk 13 dives extends in the peeling chamber 10 from the inner circumference to the outside and whose outer diameter is at a larger radius relative to the axis of rotation D of the drum 1 than the inner diameter of the two Regulierusionn 11, 12th
- the regulating blade 11 facing the cutting-edge gun provides an overflow diameter for the easy liquid phase LL.
- annular chamber 14 thus forms during operation.
- this annular chamber 14 opens a fluid supply line 15 through which a fluid, such as a gas can be passed from the outside into the annular chamber 14. It is thus possible to change the pressure in the annular chamber 14, which also causes a change in the radius of the lighter liquid phase and thus reacts on the separation diameter in the drum 1. This makes it possible in a simple way, these two sizes - pond depth (inner radius drum minus the radius at the line D mirror level, eg in Fig. 3) and separation zone between light and heavy phase - during operation only by changing the pressure in the annular chamber 14 to influence or change.
- a fluid such as a gas
- the overflow diameter of the lighter phase can be preset.
- the layer thickness of the lighter phase becomes larger and the outflow velocity smaller (longer sedimentation time).
- the degree of clarification of the lighter phase is thus increased or better.
- the crossed hatching indicates a mixed phase or separation zone region.
- the drain pressure of the lighter phase can be largely varied independently of the chamber pressure.
- the pressure in the annular chamber 14 is increased in order to move the separation zone in the interior of the drum further outwards to a larger radius. This usually causes a greater layer thickness and a better degree of clarification of the lighter phase or a better phase separation.
- the diagram of Figure 4 shows the behavior at a constant speed.
- the liquid filling in the drum 1 is not constant due to the change in pressure.
- D in each case the diameter in the drum on both sides of the axis of rotation is designated.
- the diameter D pipes (diameter drain pipes) and D cutting gun are kept constant during operation, although they are per se changeable (by replacement). Constant are also the inner diameter of the drum and the inner diameter of the solids discharge, which are usually not changeable by conversion.
- the diameter on which the separation zone lies increases with the pressure.
- the liquid level D level of the mirror in contrast, decreases in inverse proportion to the pressure.
- FIGS 2 and 3 show schematically the conditions in the drum at two different pressures.
- control range is smaller in this type of control and can only be used if a change in the drum speed during operation is permitted at all.
- the diameter of the separation zone then increases with the speed (not shown here).
- FIG. 5 A further exemplary embodiment is shown in FIG. 5.
- the heavier liquid phase is discharged via the regulating disk arrangement and the peeling disk 9, and the lighter liquid phase via the discharge pipe 8, which is achieved in that here the dividing disk-like separating gun in each case before the continuous, second openings open on both sides 26 is arranged.
- the Scheidewehr 6 thus directs the heavy liquid phase HL to the peeling disc, whereas the light phase in about the discharge pipes 8 is discharged into the blind hole-like or first openings 25 closed at one end.
- control variable for example - preferably - the concentration distribution of any of the derived phases is used.
- the pressure of the heavy liquid phase in the light increases, the pressure is reduced to further shift the separation zone in the interior of the drum to a larger radiance. This usually causes a greater layer thickness and a better degree of clarification of the lighter phase.
- FIG. 8 The corresponding control behavior is illustrated in FIG. 8 by means of an example analogous to FIG. 4.
- the various diameters are impressed as a function of the pressure in the annular chamber 14.
Landscapes
- Centrifugal Separators (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102005027553A DE102005027553A1 (de) | 2005-06-14 | 2005-06-14 | Drei-Phasen-Vollmantel-Schneckenzentrifuge und Verfahren zur Regelung des Trennprozesses |
PCT/EP2006/005172 WO2006133804A1 (de) | 2005-06-14 | 2006-05-31 | Drei-phasen-vollmantel-schneckenzentrifuge und verfahren zur regelung des trennprozesses |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1901849A1 true EP1901849A1 (de) | 2008-03-26 |
EP1901849B1 EP1901849B1 (de) | 2018-08-29 |
Family
ID=36786249
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP06754000.5A Active EP1901849B1 (de) | 2005-06-14 | 2006-05-31 | Drei-phasen-vollmantel-schneckenzentrifuge und verfahren zur regelung des trennprozesses |
Country Status (8)
Country | Link |
---|---|
US (1) | US8523749B2 (de) |
EP (1) | EP1901849B1 (de) |
CN (1) | CN101203318B (de) |
AU (1) | AU2006257485B2 (de) |
CA (1) | CA2612022C (de) |
DE (1) | DE102005027553A1 (de) |
DK (1) | DK1901849T3 (de) |
WO (1) | WO2006133804A1 (de) |
Families Citing this family (14)
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DE10336350B4 (de) * | 2003-08-08 | 2007-10-31 | Westfalia Separator Ag | Vollmantel-Schneckenzentrifuge, mit Schälscheibe |
DE102005027553A1 (de) * | 2005-06-14 | 2006-12-28 | Westfalia Separator Ag | Drei-Phasen-Vollmantel-Schneckenzentrifuge und Verfahren zur Regelung des Trennprozesses |
DE102006006178A1 (de) * | 2006-02-10 | 2007-08-16 | Westfalia Separator Ag | Vollmantel-Schneckenzentrifuge und Verfahren zu deren Betrieb |
DK178253B1 (en) | 2010-11-12 | 2015-10-12 | Alfa Laval Corp Ab | A centrifugal separator and an outlet element for a centrifugal separator |
CN102041038B (zh) * | 2010-12-30 | 2013-10-16 | 中国石油天然气股份有限公司 | 一种稠油老化油处理方法 |
DE102012102478A1 (de) * | 2012-03-22 | 2013-09-26 | Hiller Gmbh | Vollmantel-Schneckenzentrifuge |
DE102012105828A1 (de) * | 2012-07-02 | 2014-01-02 | Gea Mechanical Equipment Gmbh | Verfahren zur Aufarbeitung einer bei der hydrometallurgischen Gewinnung eines Metalls gebildeten Emulsion |
DE102012106226A1 (de) * | 2012-07-11 | 2014-01-16 | Gea Mechanical Equipment Gmbh | Vollmantel-Schneckenzentrifuge mit Überlaufwehr |
CN103586142A (zh) * | 2013-11-15 | 2014-02-19 | 上海普锐通实业有限公司 | 一种卧式螺旋沉降三相分离离心机 |
CN104841573B (zh) * | 2015-05-20 | 2017-06-06 | 中国重型机械研究院股份公司 | 一种新型轻重液相堰口高度均可调装置 |
CN106540819A (zh) * | 2015-09-23 | 2017-03-29 | 济南瀚瑞糸机械设备制造有限公司 | 一种固液四相卧螺离心机 |
KR101831556B1 (ko) | 2017-05-11 | 2018-02-22 | 허승우 | 폐기물의 오일추출이 가능한 원심분리기 |
CN110142149B (zh) * | 2019-05-29 | 2024-05-03 | 浙江工业大学 | 一种卧螺离心机用复合型排气结构 |
DE102022100511A1 (de) | 2022-01-11 | 2023-07-13 | Gea Westfalia Separator Group Gmbh | Vollmantel-Schneckenzentrifuge und Verfahren zur Regelung des Trennprozesses der Vollmantel-Schneckenzentrifuge |
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DE102006006178A1 (de) * | 2006-02-10 | 2007-08-16 | Westfalia Separator Ag | Vollmantel-Schneckenzentrifuge und Verfahren zu deren Betrieb |
SE531141C2 (sv) * | 2007-05-10 | 2009-01-07 | Alfa Laval Corp Ab | Centrifugalseparator med transportörgänga som förhindrar avskiljda partiklar att täppa till rotorns insida |
SE534278C2 (sv) * | 2009-02-17 | 2011-06-28 | Alfa Laval Corp Ab | Ett kontinuerligt förfarande för isolering av oljor från alger eller mikroorganismer |
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2005
- 2005-06-14 DE DE102005027553A patent/DE102005027553A1/de not_active Ceased
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2006
- 2006-05-31 CN CN2006800214786A patent/CN101203318B/zh active Active
- 2006-05-31 AU AU2006257485A patent/AU2006257485B2/en not_active Ceased
- 2006-05-31 CA CA2612022A patent/CA2612022C/en active Active
- 2006-05-31 DK DK06754000.5T patent/DK1901849T3/en active
- 2006-05-31 US US11/922,144 patent/US8523749B2/en active Active
- 2006-05-31 EP EP06754000.5A patent/EP1901849B1/de active Active
- 2006-05-31 WO PCT/EP2006/005172 patent/WO2006133804A1/de active Application Filing
Non-Patent Citations (1)
Title |
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See references of WO2006133804A1 * |
Also Published As
Publication number | Publication date |
---|---|
WO2006133804A1 (de) | 2006-12-21 |
AU2006257485A1 (en) | 2006-12-21 |
DE102005027553A1 (de) | 2006-12-28 |
CN101203318B (zh) | 2012-01-11 |
US20100105536A1 (en) | 2010-04-29 |
AU2006257485B2 (en) | 2011-06-02 |
EP1901849B1 (de) | 2018-08-29 |
CN101203318A (zh) | 2008-06-18 |
US8523749B2 (en) | 2013-09-03 |
DK1901849T3 (en) | 2018-12-17 |
CA2612022A1 (en) | 2006-12-21 |
CA2612022C (en) | 2014-08-19 |
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