EP1813687B1 - Procédé de fabrication de tube en acier inoxydable martensitique - Google Patents

Procédé de fabrication de tube en acier inoxydable martensitique Download PDF

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Publication number
EP1813687B1
EP1813687B1 EP05787771.4A EP05787771A EP1813687B1 EP 1813687 B1 EP1813687 B1 EP 1813687B1 EP 05787771 A EP05787771 A EP 05787771A EP 1813687 B1 EP1813687 B1 EP 1813687B1
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EP
European Patent Office
Prior art keywords
pipe
steel
temperature
stainless steel
martensitic stainless
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Ceased
Application number
EP05787771.4A
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German (de)
English (en)
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EP1813687A1 (fr
EP1813687A4 (fr
Inventor
Nobuyuki Mori
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Nippon Steel Corp
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Nippon Steel and Sumitomo Metal Corp
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Publication of EP1813687A4 publication Critical patent/EP1813687A4/fr
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    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D6/00—Heat treatment of ferrous alloys
    • C21D6/002—Heat treatment of ferrous alloys containing Cr
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/10—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of tubular bodies
    • C21D8/105—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of tubular bodies of ferrous alloys
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/08—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for tubular bodies or pipes
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/001—Ferrous alloys, e.g. steel alloys containing N
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/06—Ferrous alloys, e.g. steel alloys containing aluminium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/22—Ferrous alloys, e.g. steel alloys containing chromium with molybdenum or tungsten
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/24—Ferrous alloys, e.g. steel alloys containing chromium with vanadium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/26—Ferrous alloys, e.g. steel alloys containing chromium with niobium or tantalum
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00—Microstructure comprising significant phases
    • C21D2211/008—Martensite

Definitions

  • This invention relates to a method of manufacturing a martensitic stainless steel pipe and particularly a method of manufacturing a seamless martensitic stainless steel pipe having a high yield ratio.
  • a 13Cr steel containing approximately 0.2% of C and approximately 13% of Cr (this steel is referred to below simply as a "13Cr steel”) has excellent resistance to corrosion by infiltrating carbon dioxide gas, and it is less expensive compared to a super 13Cr steel having a decreased C content or a duplex stainless steel, so it is much used for oil country tubular goods (oil well tubing, casing, and drill pipes).
  • a seamless steel pipe made of this 13Cr steel is manufactured by hot working a billet to form a mother pipe followed by quenching and annealing.
  • Patent Document 1 discloses a method for increasing toughness by the direct quenching technique (DQT) in which quenching is carried out immediately after a 13Cr steel has been hot worked to form a mother pipe. This method does not involve reheating of a mother pipe which has been cooled prior to performing quenching, and thus it is advantageous from the standpoints of productivity and costs.
  • DQT direct quenching technique
  • Patent Document 1 JP H02-277720 A1
  • EP1288316 describes a method of producing a seamless pipe which includes heating a martensitic stainless steel raw material to an austenitic range and subjecting the raw material to piercing and elongating to form an original pipe.
  • the original pipe is cooled to form a structure substantially composed of martensite in the original pipe.
  • the original pipe is reheated to a temperature in the dual-phase range between the Ac1 transformation point and the Ac3 transformation point, and is subjected to finishing rolling at an initial rolling temperature T between the Ac1 transformation point and the Ac3 transformation point.
  • the original pipe is then cooled to form a processed pipe.
  • the processed pipe is tempered at a temperature below the Ac1 transformation point.
  • GB2230024 describes a pipe which after leaving the last hot rolling stage is cooled from the rolling heat of a temperature in the range of 960 - 990 DEG C to room temperature at a cooling rate of 0.5 - 5 K/s and tempered without a transformation by separate hardening.
  • JP63293111 describes a martensitic stainless steel billet which is subjected to piercing rolling in a temp. region of about 1,050-1,250 deg.C and then worked at a temperature region about 950 deg.C. After the conclusion of working, cooling is applied, without delay, down to 500 deg.C to 50 deg.C/min cooling rate to carry out hardening. Subsequently, tempering is applied at a temperature at the Ac1 point or below so as to manufacture a seamless pipe.
  • JP2003105441 describes a method for manufacturing a seamless tube in which a base stock of 13 Cr martensitic stainless steel is hearted to the austenitic region and a tube stock is produced by applying piecing and drawing as the hot finish rolling. Then hot finish rolling is applied, and the structure is made into martensitic structure by cooling the tube stock to room temperature, and also temper treatment is performed.
  • Patent Document 1 focuses only on toughness which is a mechanical property, and there is no mention therein of corrosion resistance.
  • HRC Rockwell Hardness scale C
  • API American Petroleum Institute
  • the object of the present invention is to provide an inexpensive method of manufacturing a corrosion resistant seamless martensitic steel pipe having a high strength and a high yield ratio with good productivity.
  • a method of manufacturing a seamless martensitic stainless steel pipe which can satisfy, for example, a yield point (YP) of 552 - 656 MPa, a tensile strength (TS) of at least 657 MPa, a yield ratio of at least 75%, a toughness such that the fracture appearance transition temperature in a Charpy impact test is 0° C or lower (shape of test piece: 10 x 10 mm with a 2 mm V-shaped notch in the L direction), and a HRC hardness of at most 22.
  • YP yield point
  • TS tensile strength
  • the present inventors conjectured that it should be possible to manufacture a steel pipe of 13Cr steel having a high strength, a high yield ratio, and good corrosion resistance at a low cost and with high productivity by the direct quenching technique, and they investigated the direct quenching technique under various conditions to solve the above-described problem.
  • the present invention is defined in claim 1.
  • Figure 1 is a graph showing the results of examples.
  • composition of the steel according to the present invention is as follows.
  • the C content is 0.15 - 0.21%.
  • Si is added as a deoxidizing agent of steel. In order to obtain this effect, at least 0.16% of Si is added. Its upper limit is made 1.0% in order to prevent a degradation in toughness. Preferably the Si content is 0.16 - 0.50%.
  • Mn is added as a deoxidizing agent. In order to obtain this effect, at least 0.35% of Mn is added. However, since addition of Mn in a too large an amount causes the toughness of steel to deteriorate, its upper limit is made at most 1.0%.
  • Cr is the key element for obtaining the necessary corrosion resistance. Addition of at least 10.5% Cr produces an improvement in corrosion resistance with respect to pitting and crevice corrosion and a significant improvement in corrosion resistance in a CO 2 environment.
  • Cr is a ferrite-forming element, a Cr content exceeding 14% makes it easy that ⁇ ferrite forms during working at high temperatures, thereby adversely affecting the hot workability of steel and decreasing the strength thereof after heat treatment, so its content is limited to at most 14.0%.
  • the upper limit of S is 0.0050% since the presence of S in a large amount causes the toughness of steel to deteriorate and worsens the quality of the inner surface of the steel pipe due to occurrence of segregation.
  • the Al content is 0.025 - 0.050%.
  • the finishing temperature of hot working is 850° C or higher, it is possible to lower the lower limit of Al content to 0.005%. This is because if the finishing temperature of final rolling is a higher temperature, it is difficult for the effects of rolling to remain in the material after rolling, resulting in an increased yield ratio of the material.
  • a lower limit of Al content is preferably 0.025%. In either mode, the upper limit is 0.050%.
  • a steel according to the present invention comprises Fe and impurities.
  • N an impurity
  • the steel may also contain at most 0.15% of Ni and at most 0.08% of Ti as impurities.
  • a portion of Fe may be replaced by at least one of the following elements.
  • Mo need not be added. If it is added, it has an effect of increasing strength and corrosion resistance. For this purpose, preferably at least 0.02% of Mo is added. However, if the Mo content exceeds 2.0%, it becomes difficult for a martensitic transformation to take place, so its upper limit is 2.0%.
  • V at most 0.50%
  • Nb need not be added. If it is added, it has the effect of increasing strength. For this purpose, it is preferably added in an amount of at least 0.002%. However, if the Nb content exceeds 0.50%, the steel has a decreased toughness, so its upper limit is 0.50%.
  • the chemical composition of the steel is limited as described above, and at the same time, the finishing temperature in final rolling during hot working is made to fall into a predetermined range.
  • Hot working at this time is hot rolling in a usual pipe forming method, so below, an explanation will be given of an example in which hot working is hot rolling.
  • finishing temperature in final rolling is less than 800° C, the effects of hot working remain in the steel, thereby adversely affecting the yield ratio and toughness of steel.
  • the finishing temperature in final rolling exceeds 960° C, crystal grains are coarsened, and the toughness and corrosion resistance are worsened in this case as well. Accordingly, the finishing temperature in final rolling is at least 800° C and at most 960° C.
  • the finishing temperature in final rolling during hot working is limited to at least 850° C and at most 960° C, even if the Al content is lower than the above-described range, it is possible to provide the steel with the desired strength, toughness, and corrosion resistance. Specifically, strength, toughness, and corrosion resistance can be satisfied when the Al content is in the range of 0.005 - 0.050%.
  • hot rolling in the present invention can be performed as follows, for example.
  • a billet is manufactured therefrom by a method such as conventional continuous casting. After the billet is heated to at least 1200° C, for example, it is pierced with a piercer or the like and then subjected to hot rolling in a mandrel mill-reducer or the like to produce a steel pipe having a predetermined outer diameter and wall thickness, i.e., a mother pipe. Hot rolling can be carried out in a different rolling mill such as a plug mill.
  • the manufacturing conditions of hot rolling or the like are adjusted so that the temperature of a mother pipe at the completion of hot rolling falls into the above-described temperature range.
  • the mother pipe is cooled to room temperature at a cooling rate greater than or equal to 2 °C per second.
  • quench-hardening takes place and a martensitic structure is obtained even with air cooling.
  • Tempering is then carried out so as to achieve desired mechanical properties.
  • tempering may be carried out by heating the pipe to 700 - 750° C followed by cooling.
  • cooling is normally carried out at least at the cooling rate of air cooling, such as at least 2° C per second.
  • a product which is obtained in this manner then undergoes inspection, threading process, and the like to obtain a finished product.
  • the dimensions of the mother pipe there are no restrictions on the dimensions of the mother pipe.
  • An example is an outer diameter of 88.1 mm and a wall thickness of 6.95 mm.
  • a molten steel having the chemical composition shown in Table 1 was prepared, and it was subjected to continuous casting and then forging to prepare a billet with dimensions of an outer diameter of 191 mm and a length of 2400 mm. This billet was heated to at least 1200° C and it was pierced in a plug mill.
  • the mother pipe which was obtained in this manner was heated to a predetermined temperature in a reheating furnace and then passed through a mandrel mill-reducer for final rolling in a hot state to manufacture a seamless steel pipe with predetermined dimensions (an outer diameter of 88.90 mm and a wall thickness of 6.45 mm).
  • the heating conditions in the reheating furnace and the rolling conditions were adjusted in order to vary the temperature of the pipe at the time of completion of final rolling, namely, the finishing temperature of hot rolling.
  • the mother pipe was then air cooled to room temperature at a rate of 2° C per second, and then it was subjected to tempering at 700 - 750° C.
  • Table 1 shows the finishing temperature and the tempering temperature for each steel sample.
  • Test pieces in accordance with API 5CT were cut from each pipe which was manufactured in this manner, and the resulting arcuate test pieces were used for measurement of tensile strength, yield point, HRC hardness, and transition temperature by a Charpy impact test (shape: 10 x 5 mm with a 2-mm V-notch).
  • Evaluation was carried out on the basis of desired properties to be satisfied which include a tensile strength satisfying API grade L80 (YP: 552 - 656 MPa, TS: at least 657 MPa), an HRC hardness of at most 22, and a fracture appearance transition temperature (vTrs) in a Charpy impact test of 0° C or lower.
  • desired properties include a tensile strength satisfying API grade L80 (YP: 552 - 656 MPa, TS: at least 657 MPa), an HRC hardness of at most 22, and a fracture appearance transition temperature (vTrs) in a Charpy impact test of 0° C or lower.
  • Figure 1 compiles the results of Table 1 in the form of a graph.
  • CIRCLE (O) and X have the following meanings.
  • a martensitic stainless steel pipe of a 13Cr steel can be manufactured with good productivity and low costs by the direct quenching technique, whereby current demands for a decrease in production costs can be satisfied.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Heat Treatment Of Steel (AREA)

Claims (1)

  1. Procédé de fabrication d'un tuyau en acier inoxydable martensitique sans soudure caractérisé par
    le perçage d'une plaque d'acier pour former une plaque percée, la plaque d'acier ayant une composition chimique consistant en, en pourcent en masse,
    C : 0,15 - 0,21 %,
    Si : 0,16 - 1,0 %,
    Mn : 0,35 - 1,0 %,
    Cr : 10,5 - 14,0 %,
    P : au plus 0,020 %,
    S : au plus 0,0050 %,
    Al : comme fixé ci-dessous,
    éventuellement au moins un de Mo : au plus 2,0 %, V : au plus 0,50 %, Nb : au plus 0,50 %, N : au plus 0,100 %, Ni : au plus 0,15 % et Ti : au plus 0,08 %,
    et un reste de Fe et d'impuretés ;
    la formation d'un tuyau mère par usinage à chaud de la plaque percée avec une température de finition de 800 - 960°C ;
    immédiatement après cela, la soumission du tuyau mère à un revenu à température ambiante à une vitesse de refroidissement supérieure ou égale à 2°C par seconde, et puis
    la réalisation d'un revenu par chauffage du tuyau, dans lequel la teneur en Al dans la composition chimique est de 0,005 - 0,050 % avec la température de finition étant de 850 - 960°C, et est de 0,025 - 0,050 % avec la température de finition étant de 800 - 960°C, et
    dans lequel le tuyau d'acier inoxydable martensitique sans soudure obtenu présente une limite élastique de 552 - 656 MPa, une résistance à la traction d'au moins 657 MPa, une dureté HRC d'au plus 22 et une température de transition d'apparence de fracture dans un test de choc Charpy de 0°C ou inférieure avec une forme d'une pièce de test étant de 10 x 5 mm avec une rainure en forme de V de 2 mm.
EP05787771.4A 2004-09-28 2005-09-27 Procédé de fabrication de tube en acier inoxydable martensitique Ceased EP1813687B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2004281711A JP4380487B2 (ja) 2004-09-28 2004-09-28 マルテンサイト系ステンレス鋼管の製造方法
PCT/JP2005/017675 WO2006035735A1 (fr) 2004-09-28 2005-09-27 Procédé de fabrication de tube en acier inoxydable martensitique

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EP1813687A1 EP1813687A1 (fr) 2007-08-01
EP1813687A4 EP1813687A4 (fr) 2010-05-05
EP1813687B1 true EP1813687B1 (fr) 2018-11-14

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US (1) US8366843B2 (fr)
EP (1) EP1813687B1 (fr)
JP (1) JP4380487B2 (fr)
CN (1) CN101031663B (fr)
WO (1) WO2006035735A1 (fr)

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CN103045835A (zh) * 2011-10-17 2013-04-17 宝山钢铁股份有限公司 一种L80-13Cr油管的制造方法
JP5907083B2 (ja) * 2013-01-31 2016-04-20 Ｊｆｅスチール株式会社 靭性に優れた継目無鋼管の製造方法及び製造設備
CN104099527B (zh) * 2013-04-08 2016-06-01 宝山钢铁股份有限公司 一种超级13Cr加厚钻杆的制造方法
JP6406075B2 (ja) * 2015-03-12 2018-10-17 Ｊｆｅスチール株式会社 マルテンサイト系高Ｃｒ鋼の継目無鋼管の製造方法
JP6686320B2 (ja) * 2015-08-05 2020-04-22 日本製鉄株式会社 ステンレス鋼管の製造方法
EP3705591B1 (fr) * 2017-11-02 2021-03-17 Nippon Steel Corporation Poinçon de dispositif de perçage et procédé de fabrication s'y rapportant
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US20070246136A1 (en) 2007-10-25
EP1813687A1 (fr) 2007-08-01
CN101031663A (zh) 2007-09-05
US8366843B2 (en) 2013-02-05
WO2006035735A1 (fr) 2006-04-06
CN101031663B (zh) 2010-09-08
EP1813687A4 (fr) 2010-05-05
JP2006097051A (ja) 2006-04-13
JP4380487B2 (ja) 2009-12-09

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