EP1549729A1 - Method for the production of a solid fragrance concentrate - Google Patents
Method for the production of a solid fragrance concentrateInfo
- Publication number
- EP1549729A1 EP1549729A1 EP03748123A EP03748123A EP1549729A1 EP 1549729 A1 EP1549729 A1 EP 1549729A1 EP 03748123 A EP03748123 A EP 03748123A EP 03748123 A EP03748123 A EP 03748123A EP 1549729 A1 EP1549729 A1 EP 1549729A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- solid
- fragrance
- mixture
- fatty alcohol
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003205 fragrance Substances 0.000 title claims abstract description 67
- 239000007787 solid Substances 0.000 title claims abstract description 44
- 239000012141 concentrate Substances 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 35
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 150000002191 fatty alcohols Chemical class 0.000 claims abstract description 19
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims abstract description 10
- 238000007711 solidification Methods 0.000 claims abstract description 10
- 230000008023 solidification Effects 0.000 claims abstract description 10
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 6
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 5
- 239000000194 fatty acid Substances 0.000 claims abstract description 5
- 229930195729 fatty acid Natural products 0.000 claims abstract description 5
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 5
- 239000008247 solid mixture Substances 0.000 claims abstract 7
- 239000004064 cosurfactant Substances 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000000465 moulding Methods 0.000 claims 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 239000000344 soap Substances 0.000 description 14
- 239000003599 detergent Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 238000004851 dishwashing Methods 0.000 description 6
- 239000002537 cosmetic Substances 0.000 description 4
- 239000003845 household chemical Substances 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000013042 solid detergent Substances 0.000 description 4
- 239000012876 carrier material Substances 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000004200 deflagration Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000003826 tablet Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
Definitions
- the invention relates to a method for producing a solid fragrance concentrate, which, for. B. for perfuming solid soaps, solid detergents and dishwashing detergents in powder, granulate, chip or tablet form and other solid household chemical or cosmetic products.
- fragrances or fragrance mixtures are liquid at normal temperature and often highly volatile substances, the introduction of which into solid household chemical or cosmetic products such as e.g. B. solid soaps or in powder, granule, chip or tablet detergent and dishwashing problems.
- the known technologies for perfuming solid soaps are based, for. B. on an intensive blending of the piliert raw soap with liquid fragrance concentrate before extrusion and cutting and re-pressing to individual bars of soap. If the liquid fragrances are introduced into the piled raw soap in larger quantities, the consistency of the soap is negatively affected.
- fragrances introduced into the solid soaps evaporate relatively quickly, because the base soap can only bind the fragrances in small amounts, so that after prolonged storage most of the solid soaps produced in this way absorb a large part of the Have lost fragrance.
- Powdery solid detergents and dishwashing agents are intensively mixed with finely sprayed liquid fragrance concentrate before packaging or before they are formed into tablets, chips, etc. When the fragrance is sprayed, evaporation causes high losses of substance during production.
- the often volatile and flammable fragrances together with air can form explosive gas-air mixtures, which can lead to deflagrations and fires in the manufacturing plants.
- the object is achieved by the characterizing features of patent claim 1.
- Advantageous embodiments of the invention form the features of subclaims 2 to 10.
- fragrances are in the liquid state at a normal temperature of 20 ° C. Fragrances ready for use by the consumer are in most cases mixtures of up to 40, in some cases even more, individual fragrance components.
- these fragrances or fragrance mixtures which are liquid at normal temperature, in relatively high concentrations and conveniently into solid soaps, powder or other solid detergents and dishwashing detergents or other solid household chemical or cosmetic products, without affecting the quality of the products is noticeably impaired or that disadvantages or dangers occur in the production process
- the liquid fragrances are dissolved according to the invention in surfactants or cosurfactants which are solid at normal temperature.
- liquid fragrances can be dissolved in the surfactants or cosurfactants or in the surfactant-cosurfactant mixtures and solidified to form a solid fragrance concentrate according to the invention.
- fragrance substances were dissolved in a liquefied mixture of 30% by weight of fatty alcohol C22 and 30% by weight of polyethylene glycol, which had a solidification point of 60 ° C., at a temperature of 80 ° C.
- the fatty alcohol-polyethylene glycol fragrance solution solidified on cooling at a temperature below 54 ° C. to give the solid fragrance concentrate according to the invention.
- the solid fragrance concentrates obtained in the above manner can be produced in known form in pelletized or granulated form, and they can be used in this form in the production of solid soaps, powder, granule or tablet detergents and dishwashing detergents or other solid ones Add household chemical or cosmetic products easily and dose precisely.
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10247583 | 2002-10-11 | ||
DE10247583A DE10247583C5 (en) | 2002-10-11 | 2002-10-11 | Process for the preparation of a solid perfume concentrate |
PCT/EP2003/011109 WO2004035721A1 (en) | 2002-10-11 | 2003-10-08 | Method for the production of a solid fragrance concentrate |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1549729A1 true EP1549729A1 (en) | 2005-07-06 |
EP1549729B1 EP1549729B1 (en) | 2007-01-03 |
EP1549729B2 EP1549729B2 (en) | 2014-06-04 |
Family
ID=32049241
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP03748123.1A Expired - Lifetime EP1549729B2 (en) | 2002-10-11 | 2003-10-08 | Method for the production of a solid fragrance concentrate |
Country Status (9)
Country | Link |
---|---|
US (1) | US7485610B2 (en) |
EP (1) | EP1549729B2 (en) |
JP (1) | JP2006516153A (en) |
CN (1) | CN1692154B (en) |
AT (1) | ATE350455T1 (en) |
DE (2) | DE10247583C5 (en) |
EA (1) | EA006727B1 (en) |
ES (1) | ES2280772T5 (en) |
WO (1) | WO2004035721A1 (en) |
Families Citing this family (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10357676A1 (en) * | 2003-12-10 | 2005-07-21 | Henkel Kgaa | Duftkomposite |
GB2417204A (en) | 2004-08-19 | 2006-02-22 | Bell Flavours & Fragrances Ltd | Air treatment apparatus |
DE102004052929A1 (en) * | 2004-10-29 | 2006-05-04 | Bell Flavors & Fragrances Duft Und Aroma Gmbh | Process and apparatus for the production of solid fragrance |
DE102005025041A1 (en) * | 2005-05-30 | 2006-12-07 | Bell Flavors & Fragrances Duft Und Aroma Gmbh | Means for use in dishwashers and apparatus for its metered introduction during the rinsing and drying phases |
DE102005036415A1 (en) * | 2005-07-29 | 2007-02-01 | Bell Flavors & Fragrances Duft Und Aroma Gmbh | Method for attaching volatile substance to carrier element, comprises dipping carrier element into melt or spraying |
DE102006029092A1 (en) * | 2006-06-24 | 2007-12-27 | Bell Flavors & Fragrances Duft Und Aroma Gmbh | Process for the aromatization of cellulosic products |
JP5465823B2 (en) * | 2006-12-13 | 2014-04-09 | ユニ・チャーム株式会社 | Functional sheet and absorbent article |
DE102007037147A1 (en) * | 2007-08-07 | 2009-02-12 | Henkel Ag & Co. Kgaa | Fragrance composites with improved fragrance release |
US20110243872A1 (en) * | 2008-12-30 | 2011-10-06 | Bell Flavors And Fragrances, Inc. | Carbohydrate treatment for fragranced articles |
GB2471303A (en) | 2009-06-24 | 2010-12-29 | Bell Flavors & Fragrances Duft Und Aroma Gmbh | Microparticles and method of making microparticles |
CA2682636C (en) * | 2009-11-05 | 2010-06-15 | The Procter & Gamble Company | Laundry scent additive |
US8476219B2 (en) | 2009-11-05 | 2013-07-02 | The Procter & Gamble Company | Laundry scent additive |
WO2012084061A1 (en) | 2010-12-23 | 2012-06-28 | Symrise Ag | Fragrance granules for detergents |
US20130065812A1 (en) * | 2011-09-14 | 2013-03-14 | Ecolab Usa Inc. | Water-dilutable solid concentrate |
US20130126634A1 (en) | 2011-11-22 | 2013-05-23 | Ecolab Usa Inc. | Solid air freshener |
JP6151374B2 (en) | 2012-12-20 | 2017-06-21 | ザ プロクター アンド ギャンブル カンパニー | Laundry fragrance additive |
CN103405346B (en) * | 2013-06-08 | 2015-04-22 | 苏州靖羽新材料有限公司 | Preparation method of solid perfume |
MX2017001220A (en) | 2014-07-30 | 2017-10-02 | Georgia Pacific Consumer Products Lp | Air freshener dispensers, cartridges therefor, systems, and methods. |
WO2017067841A1 (en) | 2015-10-23 | 2017-04-27 | Basf Se | Solid solutions of odoriferous substances and flavoring agents with vinyl lactam polymers |
JP6997171B2 (en) | 2016-08-09 | 2022-01-17 | 高砂香料工業株式会社 | Solid composition containing free fragrances and encapsulated fragrances |
WO2018055115A1 (en) * | 2016-09-26 | 2018-03-29 | Henkel Ag & Co. Kgaa | Perfume-containing melting bodies which contain highly ethoxylated non-ionic surfactants |
WO2018085021A1 (en) | 2016-11-02 | 2018-05-11 | Dow Global Technologies Llc | Solid non-aqueous gel air odorizer |
CN107260128B (en) * | 2017-06-13 | 2020-09-29 | 江苏金森海默生物技术有限公司 | Olfactory disorder detection kit and application thereof |
DE102017222992A1 (en) * | 2017-12-18 | 2019-06-19 | Henkel Ag & Co. Kgaa | Production of fragrance-containing enamel body |
CN111286414B (en) * | 2019-11-28 | 2021-04-27 | 纳爱斯浙江科技有限公司 | Clothing fragrance retaining bead and preparation method thereof |
Family Cites Families (36)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE548617C (en) * | 1930-10-08 | 1932-04-19 | Hydrierwerke Akt Ges Deutsche | Method for fixing fragrances |
US2300769A (en) * | 1940-03-28 | 1942-11-03 | Palol Perfumed Products Inc | Solid perfume |
DE1120046B (en) * | 1960-06-30 | 1961-12-21 | Spitzner Arzneimittelfabrik G | Grindable, free-flowing product made from essential oils, liquid fragrances and flavors and process for its production |
GB1169656A (en) * | 1967-12-18 | 1969-11-05 | Fumio Enomoto | Scented Composition |
FR2123824A5 (en) | 1971-02-02 | 1972-09-15 | Oreal | Solid perfumed soap - contains a soap gel with volatile solvent water and volatile perfume |
US3945950A (en) * | 1974-10-02 | 1976-03-23 | Universal Oil Products Company | Solid perfumed compositions of matter |
US4017574A (en) * | 1975-06-04 | 1977-04-12 | Colgate-Palmolive Company | Process for making variegated soap |
GB1587122A (en) * | 1976-10-29 | 1981-04-01 | Procter & Gamble Ltd | Fabric conditioning compositions |
PH17340A (en) * | 1980-03-11 | 1984-08-01 | Unilever Nv | Detergent composition |
US4741899A (en) * | 1983-06-06 | 1988-05-03 | Bristol-Myers Company | Process for arresting the proliferation of organisms that convert axillary secretions to malodorous materials |
JPS60182955A (en) * | 1984-03-01 | 1985-09-18 | 中村物産株式会社 | Production of solid perfume |
JPH0270797A (en) * | 1988-03-23 | 1990-03-09 | Union Camp Corp | Solid composition and its manufacture |
CA2004270A1 (en) * | 1988-12-29 | 1990-06-29 | William R. Michael | Perfume microcapsules for use in granular detergent compositions |
US5002681A (en) * | 1989-03-03 | 1991-03-26 | The Procter & Gamble Company | Jumbo particulate fabric softner composition |
CA2015737C (en) * | 1989-05-11 | 1995-08-15 | Diane Grob Schmidt | Coated perfume particles |
US5154842A (en) * | 1990-02-20 | 1992-10-13 | The Procter & Gamble Company | Coated perfume particles |
ATE137795T1 (en) * | 1990-07-31 | 1996-05-15 | Procter & Gamble | IMPROVED CARRIER AND RELEASE SYSTEM OF ORNAMENTS FOR LAUNDRY TREATMENT |
US5194172A (en) * | 1990-09-13 | 1993-03-16 | The Procter & Gamble Company | Aerated and freezer bar soap compositions containing sucrose as a mildness aid and a processing aid |
US5635164A (en) * | 1991-07-03 | 1997-06-03 | The Mennen Company | Stick composition with sodium chloride and stearyl alcohol |
US5378468A (en) * | 1992-09-22 | 1995-01-03 | The Mennen Company | Composition containing body activated fragrance for contacting the skin and method of use |
TR28670A (en) * | 1993-06-02 | 1996-12-17 | Procter & Gamble | Perfume release system containing zeolites. |
US5506201A (en) * | 1994-04-29 | 1996-04-09 | International Flavors & Fragrances Inc. | Formulation of a fat surfactant vehicle containing a fragrance |
BR9611424A (en) * | 1995-10-31 | 1999-02-23 | Procter & Gamble | Deodorant cosmetics |
DE19710635A1 (en) * | 1997-03-14 | 1998-09-17 | Buck Chemie Gmbh | Gel-based cleaning block for toilet hygiene with permanent room air scenting |
DE19735783A1 (en) * | 1997-08-18 | 1999-02-25 | Henkel Kgaa | High dosage perfumed moulding useful in laundry detergent or for separate addition to wash |
DE19744571A1 (en) | 1997-10-09 | 1999-04-15 | Haarmann & Reimer Gmbh | Toilet stones |
US6086644A (en) * | 1997-10-10 | 2000-07-11 | Takasago International Corporation | Scented candle and manufacturing method for same |
DE19746780A1 (en) * | 1997-10-23 | 1999-04-29 | Henkel Kgaa | Production of perfumed moldings especially beads with high bulk density useful in detergent |
DE19749760A1 (en) * | 1997-11-11 | 1999-05-12 | Henkel Kgaa | Multi-phase stick preparation |
DE19808757B4 (en) * | 1998-03-02 | 2007-09-20 | Henkel Kgaa | Fragrance beads in detergent tablets |
DE19917692A1 (en) * | 1999-04-20 | 2000-10-26 | Henkel Kgaa | Beads for use in sachets for imparting fragrance to dry laundry consist of a washing agent ingredient containing perfume oil so as to obviate need for disposal of carrier material |
DE19948667A1 (en) * | 1999-10-08 | 2001-04-12 | Henkel Kgaa | Detergent component with double-controlled fragrance release |
US6531444B1 (en) * | 2000-11-09 | 2003-03-11 | Salvona, Llc | Controlled delivery system for fabric care products |
DE10063428A1 (en) * | 2000-12-20 | 2002-07-11 | Henkel Kgaa | Dispersions of nanoparticulate fragrance-containing composite materials |
US20030126788A1 (en) * | 2001-11-07 | 2003-07-10 | Colloid Tech. Inc. | Storage stable translucent flammable article |
US7381697B2 (en) * | 2002-04-10 | 2008-06-03 | Ecolab Inc. | Fabric softener composition and methods for manufacturing and using |
-
2002
- 2002-10-11 DE DE10247583A patent/DE10247583C5/en not_active Expired - Fee Related
-
2003
- 2003-10-08 DE DE50306219T patent/DE50306219D1/en not_active Expired - Lifetime
- 2003-10-08 CN CN2003801006895A patent/CN1692154B/en not_active Expired - Lifetime
- 2003-10-08 EP EP03748123.1A patent/EP1549729B2/en not_active Expired - Lifetime
- 2003-10-08 EA EA200401487A patent/EA006727B1/en not_active IP Right Cessation
- 2003-10-08 US US10/521,033 patent/US7485610B2/en active Active
- 2003-10-08 WO PCT/EP2003/011109 patent/WO2004035721A1/en active IP Right Grant
- 2003-10-08 JP JP2004544106A patent/JP2006516153A/en active Pending
- 2003-10-08 AT AT03748123T patent/ATE350455T1/en active
- 2003-10-08 ES ES03748123.1T patent/ES2280772T5/en not_active Expired - Lifetime
Non-Patent Citations (1)
Title |
---|
See references of WO2004035721A1 * |
Also Published As
Publication number | Publication date |
---|---|
JP2006516153A (en) | 2006-06-22 |
ATE350455T1 (en) | 2007-01-15 |
ES2280772T5 (en) | 2014-09-19 |
EA006727B1 (en) | 2006-04-28 |
DE50306219D1 (en) | 2007-02-15 |
US20050227905A1 (en) | 2005-10-13 |
WO2004035721A1 (en) | 2004-04-29 |
CN1692154B (en) | 2010-04-28 |
EP1549729B1 (en) | 2007-01-03 |
DE10247583C5 (en) | 2009-04-30 |
DE10247583B4 (en) | 2007-08-23 |
EA200401487A1 (en) | 2005-10-27 |
US7485610B2 (en) | 2009-02-03 |
EP1549729B2 (en) | 2014-06-04 |
ES2280772T3 (en) | 2007-09-16 |
CN1692154A (en) | 2005-11-02 |
DE10247583A1 (en) | 2004-04-29 |
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