EP1521933B1 - Verfahren zur druckregelung eines behälters für kryogenes fluid und entsprechender behälter - Google Patents

Verfahren zur druckregelung eines behälters für kryogenes fluid und entsprechender behälter Download PDF

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Publication number
EP1521933B1
EP1521933B1 EP03762706A EP03762706A EP1521933B1 EP 1521933 B1 EP1521933 B1 EP 1521933B1 EP 03762706 A EP03762706 A EP 03762706A EP 03762706 A EP03762706 A EP 03762706A EP 1521933 B1 EP1521933 B1 EP 1521933B1
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EP
European Patent Office
Prior art keywords
tank
liquid
pressure
fluid
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP03762706A
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English (en)
French (fr)
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EP1521933A2 (de
Inventor
Alain Résidence du Moulin Saint-Martin CLOAREC
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of EP1521933A2 publication Critical patent/EP1521933A2/de
Application granted granted Critical
Publication of EP1521933B1 publication Critical patent/EP1521933B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C7/00Methods or apparatus for discharging liquefied, solidified, or compressed gases from pressure vessels, not covered by another subclass
    • F17C7/02Discharging liquefied gases
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C5/00Methods or apparatus for filling containers with liquefied, solidified, or compressed gases under pressures
    • F17C5/02Methods or apparatus for filling containers with liquefied, solidified, or compressed gases under pressures for filling with liquefied gases
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2227/00Transfer of fluids, i.e. method or means for transferring the fluid; Heat exchange with the fluid
    • F17C2227/01Propulsion of the fluid
    • F17C2227/0107Propulsion of the fluid by pressurising the ullage
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2250/00Accessories; Control means; Indicating, measuring or monitoring of parameters
    • F17C2250/04Indicating or measuring of parameters as input values
    • F17C2250/0404Parameters indicated or measured
    • F17C2250/043Pressure
    • F17C2250/0434Pressure difference
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2250/00Accessories; Control means; Indicating, measuring or monitoring of parameters
    • F17C2250/06Controlling or regulating of parameters as output values
    • F17C2250/0605Parameters
    • F17C2250/0626Pressure

Definitions

  • the present invention relates to a method of pressure regulation of a cryogenic fluid reservoir connected to an installation consuming this fluid, which reservoir contains, under a storage pressure greater than atmospheric pressure, a cryogenic fluid in the liquid phase at the bottom of the reservoir and in the gaseous phase at the top of the tank, this tank being adapted to supply the consumer facility liquid withdrawn from the bottom of the tank, and to be supplied from the outside with fluid. It also relates to such a tank.
  • a pressure control method of a tank is described in the document US 2,850,882 .
  • the invention is particularly applicable to tanks called "low storage pressure", that is to say, the maximum pressure reached at the top of the tank is generally less than about 4 bar, the pressure indicated here and the pressures indicated thereafter being in absolute bars.
  • Such reservoirs are commonly used to store a cryogenic fluid, that is to say a fluid that at atmospheric pressure is liquid at a temperature much lower than 0 ° C. They are connected to at least one consumer installation, such as a freezing tunnel of food products.
  • the storage pressure of the tank being greater than the atmospheric pressure, the opening of a valve placed on the connection line of the tank to the consuming installation causes the liquid to move from its point of drawing to its point of use, without forced drive means and despite the pressure drops.
  • the pressure of the gas at the top of the tank is conventionally regulated so that this pressure remains substantially equal to a predetermined value. fixed, generally of the order of 2 to 3 bars.
  • the pressure of the liquid at the bottom of the tank varies according to the height of the liquid inside the tank, so that as the liquid level drops, the pressure of the liquid withdrawn decreases and tends to get closer to the gas pressure at the top.
  • a liquid height of about 10 meters implies a differential of pressure of the order of 0.6 bar between the gas pressure at the top and the liquid pressure at the bottom of the tank, at the drawing.
  • the object of the present invention is to provide a control method which guarantees a drawing flow at the bottom of the substantially constant reservoir and which, more generally, improves the storage, supply and withdrawal performance of the cryogenic fluid reservoir.
  • the subject of the invention is a method for regulating the pressure of a cryogenic fluid reservoir as defined above, in which the pressure of the gas at the top of the tank is varied according to the operating state of the this tank.
  • operating state of the reservoir must be understood to mean the different phases that it traverses during its use: drawing of liquid causing a drop in level, re-supply of the reservoir causing a rise in level , or even stand-by phases of the consumer installation where the tank is at rest.
  • a nitrogen tank 1 containing liquid nitrogen at the bottom, also called “tank”, and nitrogen gas under a pressure of about 2 bars at the top, also called “head” .
  • the level of liquid inside the tank is marked by the reference N.
  • the bottom of the tank 1 is connected to a consumer installation 2, for example a freezing tunnel, via a connecting pipe 3 provided with a closing valve 4.
  • the connection point of the pipe 3 to the tank 1, which is noted P, is commonly called "point of draw”.
  • the tank 1 comprises means 5 for pressurizing the gas at the top of the tank.
  • These means 5 comprise a line 6 connecting the bottom of the tank to its top, and is provided, upstream to downstream, of a device 7 for measuring the pressure of the liquid nitrogen, for example a manometer, a closing valve 8 (preferably a solenoid valve) and a vaporizer 9.
  • the tank 1 also comprises means 10 for venting the gas at the top of the tank.
  • These means 10 comprise a line 11 for outward evacuation, provided upstream downstream of a manometer 12, a closure valve 13 and possibly an air exhaust member, not shown, commonly called "silent".
  • a unit 15, controlling the means 5 for pressurizing the top, as well as means 10 for venting the top, is connected, for example by electrical connections, on the one hand to the pressure measuring apparatus 7 and 12, and on the other hand to the valves 8 and 13.
  • the control unit 15 is in this way adapted, on the one hand, to know, continuously or at regular intervals, the liquid nitrogen pressure at bottom of the tank 1 and nitrogen gas at the top of the tank and, secondly, to compare the value of the bottom pressure to a predetermined value selected, modifiable by the user.
  • the unit 15 is also able to control the opening, total or partial, and the closing of the valves 8 and 13 so as to regulate the pressures of the bottom and the top of the tank 1, as will be explained in detail later .
  • Means 16 for supplying nitrogen are also provided, so as to regularly, possibly continuously, supply liquid nitrogen to the tank 1.
  • these means 16 comprise a feed pipe 17 through the bottom of the tank 1 allowing a filling said "source”, and possibly a feed pipe 18 by the top of the tank for filling said "rain”.
  • the tank 1 also comprises an overflow member 19 known per se, for limiting the height of the liquid inside the tank.
  • the level of the liquid N is represented at its maximum.
  • This figure illustrates the example of a tank of 50000 liters, giving rise to a height N of about 10 meters, which creates in such a case a pressure differential between the top and the bottom of the tank. about 0.6 bar.
  • control unit 15 substantially maintains the liquid pressure at the point of drawdown P during the entire nitrogen withdrawal period.
  • the flow rate of the connection line 3 to the consumer installation 2 thus remains substantially constant, limiting the operating disturbances of this installation 2.
  • the level of liquid inside the tank 1 increases, causing a corresponding increase in the gas pressure at the top of the tank.
  • the unit 15 detects, by means of the measurements of the manometer 7, a pressure increase, and then controls the opening of the venting valve 13, which which decreases the gas pressure at the top and, consequently, that of liquid at the bottom of the tank.
  • the unit 15 maintains the opening of the valve 13 as the liquid pressure at the bottom of the tank remains greater than the aforementioned predetermined value.
  • the regulation of the tank 1 is substantially similar when the supply of liquid nitrogen is made by the top.
  • Source filling is, however, preferred over filling with rain, the latter tending on the one hand to decrease more significantly the gas pressure, and on the other hand to heat the liquid.
  • control unit 15 is adapted to improve the storage capacities of the frigories of the stored liquid. To do this, when the container 1 is not biased in racking and will not be biased a priori for a period of several hours (for example at night), the unit 15 controls the total opening of the valve of setting. 13. The gas pressure at the top of the tank then changes from a storage value of about 2 bars to substantially atmospheric pressure (residual pressure of a few hundred grams). In this state, the tank 1 is no longer able to supply the installation 2, the displacement of the fluid inside the pipe 3 is no longer ensured. However, by lowering the nitrogen storage pressure in this way, the enthalpy of the latter tends to increase, which amounts to having a lower temperature fluid than when it was under pressure. The fluid thus stored during these periods of non-use of the tank 1 therefore has a lower temperature than usual, guaranteeing a better "cryogenic quality" (in terms of available frigories).
  • the unit 15 controls the pressurization of the top of the tank, via the means 5, until the liquid pressure at the bottom of the tank reaches the predetermined value mentioned above.
  • the regulation method according to the invention makes it possible thus improve storage, supply and withdrawal performance.
  • the measurement of the liquid pressure is not carried out, as above, substantially at the point of drawing of the liquid, but is carried out at the highest point of altitude. along the connection line 3 between the tank 1 and the consumer installation 2.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Claims (9)

  1. Verfahren zur Steuerung des Drucks eines Tiefsttemperaturfluid-Vorratsbehälters (1), der mit einer dieses Fluid verbrauchenden Anlage (2) verbunden ist, wobei der Vorratsbehälter ein Tiefsttemperaturfluid in flüssiger Phase am Boden des Vorratsbehälters und in gasförmiger Phase an der Oberseite des Vorratsbehälters unter einem Aufbewahrungsdruck, der höher als der Atmosphärendruck ist, enthält, wobei der Vorratsbehälter (1) dazu ausgelegt ist, die Verbraucheranlage (2) mit vom Boden des Vorratsbehälters entnommener Flüssigkeit zu versorgen und von außerhalb mit Fluid versorgt zu werden, dadurch gekennzeichnet, dass der Gasdruck an der Oberseite des Vorratsbehälters (1) entsprechend dem Betriebszustand dieses Vorratsbehälters, nämlich:
    - der Phase der Entnahme von Flüssigkeit durch die Verbraucheranlage,
    - der Phase der Wiederversorgung des Vorratsbehälters mit Tiefsttemperaturfluid und
    - den Wartephasen der Verbraucheranlage, in denen der Vorratsbehälter im Ruhezustand ist,
    verändert wird.
  2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass dann, wenn sich der Pegel (N) der Flüssigkeit innerhalb des Vorratsbehälters (1) verändert, der Druck der Flüssigkeit am Boden des Vorratsbehälters auf einem konstanten vorgegebenen Wert gehalten wird, indem der Gasdruck an der Oberseite des Vorratsbehälters verändert wird.
  3. Verfahren nach Anspruch 2, dadurch gekennzeichnet, dass der auf dem vorgegebenen Wert gehaltene Flüssigkeitsdruck am Punkt der Abzapfung (P) der Flüssigkeit zu der Verbraucheranlage (2) gemessen wird.
  4. Verfahren nach Anspruch 2, dadurch gekennzeichnet, dass der auf dem vorgegebenen Wert gehaltene Flüssigkeitsdruck am Punkt der größten Höhe längs einer Verbindungsleitung (3) zwischen dem Vorratsbehälter (1) und der Verbraucheranlage (2) gemessen wird.
  5. Verfahren nach einem der Ansprüche 2 bis 4,
    dadurch gekennzeichnet, dass dann, wenn Flüssigkeit vom Vorratsbehälter (1) entnommen wird und wenn der Flüssigkeitspegel (N) sinkt, vom Boden des Vorratsbehälters entnommene Flüssigkeit verdampft wird, um ein Gas zu bilden, das zur Oberseite des Vorratsbehälters geschickt wird.
  6. Verfahren nach einem der Ansprüche 2 bis 5,
    dadurch gekennzeichnet, dass dann, wenn der Vorratsbehälter (1) wieder mit Fluid versorgt wird und wenn der Flüssigkeitspegel (N) ansteigt, wenigstens ein Teil des Gases an der Oberseite des Vorratsbehälters in die äußere Umgebung des Vorratsbehälters abgeführt wird.
  7. Verfahren nach Anspruch 6, dadurch gekennzeichnet, dass das Wiederversorgungsfluid am Boden des Vorratsbehälters (1) im flüssigen Zustand eingeleitet wird.
  8. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass dann, wenn der Vorratsbehälter (1) die Verbraucheranlage (2) nicht versorgt, der Gasdruck an der Oberseite des Vorratsbehälters im Wesentlichen bis auf den Atmosphärendruck abgesenkt wird.
  9. Verfahren nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der Aufbewahrungsdruck des Vorratsbehälters (1) niedriger als 4 Bar ist.
EP03762706A 2002-07-05 2003-06-24 Verfahren zur druckregelung eines behälters für kryogenes fluid und entsprechender behälter Expired - Lifetime EP1521933B1 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0208449 2002-07-05
FR0208449A FR2841963B1 (fr) 2002-07-05 2002-07-05 Procede de regulation en pression d'un reservoir de fluide cryogenique, et reservoir correspondant
PCT/FR2003/001938 WO2004005791A2 (fr) 2002-07-05 2003-06-24 Procede de regulation en pression d'un reservoir de fluide cryogenique, et reservoir correspondant

Publications (2)

Publication Number Publication Date
EP1521933A2 EP1521933A2 (de) 2005-04-13
EP1521933B1 true EP1521933B1 (de) 2009-12-30

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ID=29725193

Family Applications (1)

Application Number Title Priority Date Filing Date
EP03762706A Expired - Lifetime EP1521933B1 (de) 2002-07-05 2003-06-24 Verfahren zur druckregelung eines behälters für kryogenes fluid und entsprechender behälter

Country Status (7)

Country Link
EP (1) EP1521933B1 (de)
AT (1) ATE453829T1 (de)
AU (1) AU2003260622B2 (de)
CA (1) CA2491022C (de)
DE (1) DE60330777D1 (de)
FR (1) FR2841963B1 (de)
WO (1) WO2004005791A2 (de)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3121732A1 (fr) * 2021-04-13 2022-10-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Dispositif de stockage et de fourniture de fluide et véhicule, véhicule et procédé comportant un tel dispositif
FR3121731A1 (fr) * 2021-04-13 2022-10-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Dispositif de stockage et de fourniture de fluide et véhicule, véhicule et procédé comportant un tel dispositif

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1813855A1 (de) * 2006-01-27 2007-08-01 L'AIR LIQUIDE, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Verfahren und Vorrichtung zur Befüllung eines Behälters unter Hochdruck mit flüssigem Gas anhand hydrostatischem Duck
FR2922991B1 (fr) 2007-10-26 2015-06-26 Air Liquide Procede d'estimation de parametres caracteristiques d'un reservoir cryogenique et notamment de parametres geometriques du reservoir
FR2922992B1 (fr) 2007-10-26 2010-04-30 Air Liquide Procede de determination en temps reel du niveau de remplissage d'un reservoir cryogenique
FR2924788B1 (fr) * 2007-12-11 2015-04-03 Air Liquide Procede de determination de la masse de fluide dans un reservoir cryogenique ainsi que du debit massique de fluide consomme.
FR2953370B1 (fr) 2009-12-08 2012-08-03 Air Liquide Procede et installation de refroidissement et/ou surgelation de produits, notamment alimentaires, mettant en oeuvre l'injection de deux liquides cryogeniques
FR2959295B1 (fr) * 2010-04-27 2013-05-03 Air Liquide Procede et installation de remplissage rapide d'un reservoir aval en liquide cryogenique a partir d'un stockage amont
US9869429B2 (en) 2010-08-25 2018-01-16 Chart Industries, Inc. Bulk cryogenic liquid pressurized dispensing system and method
US9939109B2 (en) 2010-08-25 2018-04-10 Chart Inc. Bulk liquid cooling and pressurized dispensing system and method
JP6434762B2 (ja) * 2014-09-26 2018-12-05 川崎重工業株式会社 水素燃料供給システム
GB2537913B (en) * 2015-04-30 2019-12-18 Spirax Sarco Ltd Apparatus and method for determining an amount of non-condensable gas
FR3060708B1 (fr) * 2016-12-21 2019-10-25 Engie Dispositif, systeme et procede de regulation de la pression pour un reservoir de stockage de gaz naturel liquefie
AT520862B1 (de) * 2018-01-16 2019-12-15 Sasu Energiesysteme Gmbh Verfahren und Vorrichtung zum Befüllen eines Behälters mit einer kryogenen Flüssigkeit
DE102018108214A1 (de) * 2018-04-06 2019-10-10 Samson Ag Tankanordnung und Verfahren zur Füllstandsregelung
FR3089599B1 (fr) * 2018-12-06 2020-11-13 Air Liquide Réservoir de stockage de fluide cryogénique
FR3089600B1 (fr) * 2018-12-06 2021-03-19 Air Liquide Réservoir de stockage de fluide cryogénique
FR3114765B1 (fr) 2020-10-05 2022-08-19 Air Liquide « Procédé d'alimentation en fluide cryogénique d’un poste utilisateur, notamment d'une machine d'usinage »

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BE553071A (de) * 1955-12-02 1900-01-01
JP2536744B2 (ja) * 1986-12-17 1996-09-18 大成ロテック株式会社 路面加熱車並びに路面加熱車のガス供給装置
US5121609A (en) * 1991-05-17 1992-06-16 Minnesota Valley Engineering No loss fueling station for liquid natural gas vehicles
DE10040679A1 (de) * 2000-08-19 2002-02-28 Messer Griesheim Gmbh Vorrichtung und Verfahren zur druckgeregelten Versorgung aus einem Flüssiggastank

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3121732A1 (fr) * 2021-04-13 2022-10-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Dispositif de stockage et de fourniture de fluide et véhicule, véhicule et procédé comportant un tel dispositif
FR3121731A1 (fr) * 2021-04-13 2022-10-14 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Dispositif de stockage et de fourniture de fluide et véhicule, véhicule et procédé comportant un tel dispositif
EP4075048A1 (de) * 2021-04-13 2022-10-19 L'Air Liquide - Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Vorrichtung zum speichern und zuführen von fluiden, fahrzeug und verfahren mit einer solchen vorrichtung
WO2022218704A1 (fr) * 2021-04-13 2022-10-20 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Dispositif de stockage et de fourniture de fluide et véhicule, véhicule et procédé comportant un tel dispositif

Also Published As

Publication number Publication date
EP1521933A2 (de) 2005-04-13
WO2004005791A3 (fr) 2004-04-08
CA2491022C (fr) 2011-08-09
DE60330777D1 (de) 2010-02-11
AU2003260622A1 (en) 2004-01-23
ATE453829T1 (de) 2010-01-15
FR2841963A1 (fr) 2004-01-09
AU2003260622B2 (en) 2008-08-14
FR2841963B1 (fr) 2005-07-01
CA2491022A1 (fr) 2004-01-15
WO2004005791A2 (fr) 2004-01-15

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