EP1444495A1 - Detecteur de fuite de gaz traceur - Google Patents
Detecteur de fuite de gaz traceurInfo
- Publication number
- EP1444495A1 EP1444495A1 EP02787638A EP02787638A EP1444495A1 EP 1444495 A1 EP1444495 A1 EP 1444495A1 EP 02787638 A EP02787638 A EP 02787638A EP 02787638 A EP02787638 A EP 02787638A EP 1444495 A1 EP1444495 A1 EP 1444495A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- inlet
- vacuum pump
- test gas
- valve
- detector
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M3/00—Investigating fluid-tightness of structures
- G01M3/02—Investigating fluid-tightness of structures by using fluid or vacuum
- G01M3/04—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point
- G01M3/20—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material
- G01M3/202—Investigating fluid-tightness of structures by using fluid or vacuum by detecting the presence of fluid at the leakage point using special tracer materials, e.g. dye, fluorescent material, radioactive material using mass spectrometer detection systems
Definitions
- the invention relates to a test gas leak detector with the features of the preamble of claim 1.
- Leak detectors of this type are also referred to as countercurrent leak detectors, since the test gas which reaches the test gas detector via the intermediate entry into the high vacuum pump system (one or more high vacuum pump stage (s), preferably friction pump stages), flows against the conveying direction of the pump system.
- the leak detection is carried out in such a way that the inlet of the device is connected, for example, to a test object which is sprayed with test gas from the outside. In the event of a leak, test gas penetrates the test object and is detected using the test gas detector.
- a test chamber can also be connected to the inlet of the leak detector in which there are one or more test specimens containing test gas.
- test gas enters the test chamber and is detected with the help of the test gas detector.
- the vacuum leak detection described can be qualitative or quantitative be carried out. Helium has proven itself as a test gas.
- a leak detector of the type concerned here is known from US 4,472,962.
- a test chamber is connected to its inlet.
- the test chamber is evacuated via the norvacuum pump, which is required for the operation of the high vacuum pump system designed as a turbomolecular vacuum pump.
- gas to be examined for the presence of a test gas is fed to an intermediate inlet on the turbomolecular pump.
- the present invention has for its object to improve the leak detection device according to the prior art in terms of speed and sensitivity of the leak detection.
- this object is achieved by the characterizing features of the claims.
- boost pump high-vacuum pump
- the detection sensitivity remains high, since it is only determined by the high vacuum pump system and the design of its counterflow stages.
- the evacuation time becomes short, which lent through a rel. high switching pressure on the booster pump is reached.
- the figure shows schematically the components of the leak detector 1, the inlet of which is designated 2.
- Two line sections 3 and 4 connect to the inlet.
- Line section 3 is equipped with a valve 5 and is connected via the line section 6 to the inlet 7 of the fore-vacuum pump 8.
- the line 4 there are a valve 9 and a high vacuum pump 11 (booster pump), the outlet 12 of which is connected to an intermediate inlet 14 on a second high vacuum pump 15 via a continuously open line section 13.
- the outlet 12 of the high vacuum pump 11 is also connected via the line sections 16 - with valve 17 - and 6 to the inlet 7 of the fore vacuum pump 8.
- the high-vacuum pump 15 is the leak detection pump through which the test gas flows, at least in sections, against its conveying direction.
- the test gas detector 22 is connected to its inlet 21 — preferably a mass spectrometer when helium is used as the test gas. Its outlet 23 is connected via the line section 24 to the inlet 7 of the forevacuum pump 8. In the line section 24 there is a throttle 25 and a valve 26, in the direction of flow, which can also be designed as a component (eg valve with a small nominal width).
- Two pressure measuring devices 27 and 28 provide information about the inlet pressure (device 27) and the pressure at the intermediate inlet 14 (device 28).
- the leak detection mode is controlled using the pressure signals supplied.
- a controller and associated lines are not shown.
- valve 26 can be opened after a short time (inlet pressure a few mbar, depending on the properties of the pump 15). If the test specimen has a gross leak, test gas passes through valve 26, throttle 25 and high vacuum pump 15 (in countercurrent) to detector 22 and is registered.
- valve 5 is closed and valves 9 and 17 are closed. be opened.
- This step can be done at the point in time when the inlet pressure has approximately the value that is necessary at the intermediate inlet (14) in order to just maintain the working pressure in the test gas detector (mass spectrometer).
- the pumping speed of the booster pump 11 is small, so it does not cause a harmful pressure increase at the intermediate inlet.
- the pumping speed of the fore-vacuum pump 8 is even greater than the pumping speed of the booster pump 11. If the test object has minor leaks, these are recognized (fine leak detection).
- the test object With increasing pressure decrease at the inlet 2, the pumping speed of the booster pump 11 increases, the test object is evacuated relatively quickly to low pressures. If, for example, the inlet pressure has reached a value of 10 "2 mbar, the highly sensitive leak detection begins by closing the valve 17. A test gas escaping from a test gas that may still be present and very small leaks completely into the intermediate inlet 14 and is measured by the mass spectrometer 22 registered.
- Oil-sealed or dry (oil-free) pumps can be used as the backing pump 8, expediently with a pumping speed> 16 m 3 h (ie, relatively "large” pumps) because of the relatively large volumes of the test specimen or test chamber.
- the throttle 25 causes the sensitivity for the leak detection, determined by K ⁇ .
- the booster turbomolecular pump 11 should be selected such that it already has a significant pumping speed even at high inlet pressure. It applies to the leak detection pump 15 that it has a relatively high compression in the lower region in order to isolate the unstable forevacuum pump.
- An embodiment according to the figure can be implemented particularly advantageously with a speed-controlled turbopump 11 at the inlet 2 of the leak detector 1. While in the solution with an unregulated pump speed the line 16 with the valve 17 is required in order to first discharge the increased gas flow in the so-called “cross-over" (transition to fine leak detection, opening of the valve 9) into the backing pump 8, line 16 and valve 17 can also be saved if the speed of the booster TMP 11 each. is regulated so that the maximum permissible gas flow is not exceeded. This means that the condition that the pumping speed of the pump 11 is not exceeded at the beginning of the "cross-over" is achieved by speed control.
- the booster pump 11 runs at a low "standby" speed as long as the inlet valve 9 is closed. As soon as the inlet pressure has fallen below the casual value for the valve-less intermediate inlet 14 of the counterflow pump, valve 5 is closed and valve 9 is opened. At this moment, the effective pumping speed of the booster pump 11 must be approximately equal to the previous pumping speed. be pump 8 so that there is no pressure increase in the fore vacuum.
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Examining Or Testing Airtightness (AREA)
Abstract
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10156205A DE10156205A1 (de) | 2001-11-15 | 2001-11-15 | Testgaslecksuchgerät |
DE10156205 | 2001-11-15 | ||
PCT/EP2002/012601 WO2003042651A1 (fr) | 2001-11-15 | 2002-11-12 | Detecteur de fuite de gaz traceur |
Publications (1)
Publication Number | Publication Date |
---|---|
EP1444495A1 true EP1444495A1 (fr) | 2004-08-11 |
Family
ID=7705902
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP02787638A Withdrawn EP1444495A1 (fr) | 2001-11-15 | 2002-11-12 | Detecteur de fuite de gaz traceur |
Country Status (5)
Country | Link |
---|---|
US (1) | US7082813B2 (fr) |
EP (1) | EP1444495A1 (fr) |
JP (1) | JP4164030B2 (fr) |
DE (1) | DE10156205A1 (fr) |
WO (1) | WO2003042651A1 (fr) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10156205A1 (de) * | 2001-11-15 | 2003-06-05 | Inficon Gmbh | Testgaslecksuchgerät |
DE10302987A1 (de) * | 2003-01-25 | 2004-08-05 | Inficon Gmbh | Lecksuchgerät mit einem Einlass |
WO2005031169A1 (fr) * | 2003-09-26 | 2005-04-07 | The Boc Group Plc | Detection de contaminants dans un fluide pompe par une pompe a vide |
US20070240493A1 (en) * | 2006-04-18 | 2007-10-18 | Shane Conlan | Sprayer-sniffer probe |
DE102006034735A1 (de) * | 2006-07-27 | 2008-01-31 | Inficon Gmbh | Lecksuchgerät |
US7500381B2 (en) * | 2006-08-31 | 2009-03-10 | Varian, Inc. | Systems and methods for trace gas leak detection of large leaks at relatively high test pressures |
DE102007057944A1 (de) * | 2007-12-01 | 2009-06-04 | Inficon Gmbh | Verfahren und Vorrichtung zur Dichtheitsprüfung |
US8230722B1 (en) | 2010-03-16 | 2012-07-31 | Sandia Corporation | Residual gas analysis device |
DE102011107334B4 (de) * | 2011-07-14 | 2023-03-16 | Leybold Gmbh | Lecksucheinrichtung sowie Verfahren zum Überprüfen von Gegenständen auf Dichtigkeit mittels einer Lecksucheinrichtung |
DE102013218506A1 (de) * | 2013-09-16 | 2015-03-19 | Inficon Gmbh | Schnüffellecksucher mit mehrstufiger Membranpumpe |
DE102014223841A1 (de) * | 2014-11-21 | 2016-05-25 | Inficon Gmbh | Vorrichtung und Verfahren zur Gegenstrom-Leckdetektion |
DE102016210701A1 (de) * | 2016-06-15 | 2017-12-21 | Inficon Gmbh | Massenspektrometrischer Lecksucher mit Turbomolekularpumpe und Boosterpumpe auf gemeinsamer Welle |
CN107327324B (zh) * | 2017-07-25 | 2023-03-14 | 航天推进技术研究院 | 一种设置有泄漏检测装置的orc发电机组的泄漏检测方法 |
FR3070489B1 (fr) * | 2017-08-29 | 2020-10-23 | Pfeiffer Vacuum | Detecteur de fuites et procede de detection de fuites pour le controle de l'etancheite d'objets a tester |
FR3072774B1 (fr) * | 2017-10-19 | 2019-11-15 | Pfeiffer Vacuum | Detecteur de fuites pour le controle de l'etancheite d'un objet a tester |
KR102016944B1 (ko) * | 2018-04-24 | 2019-09-03 | 한국에너지기술연구원 | 고압반응기의 기체 누설량 측정장치 및 측정방법 |
Family Cites Families (31)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1648648C3 (de) * | 1967-04-12 | 1980-01-24 | Arthur Pfeiffer-Hochvakuumtechnik Gmbh, 6330 Wetzlar | Anordnung zur Lecksuche nach dem Massenspektrometer-Prinzip |
US3690151A (en) * | 1968-07-25 | 1972-09-12 | Norton Co | Leak detector |
US4472962A (en) * | 1981-08-03 | 1984-09-25 | Balzers Aktiengesellschaft | Low pressure leak detector |
DE3144503C2 (de) * | 1981-11-09 | 1985-03-21 | Cit-Alcatel GmbH, 6980 Wertheim | Massenspektrometer-Lecksuchgerät |
DE3247975A1 (de) * | 1982-12-24 | 1984-06-28 | Balzers Hochvakuum Gmbh, 6200 Wiesbaden | Verfahren und vorrichtung zur auffindung von lecks in waenden |
US4499752A (en) * | 1983-06-22 | 1985-02-19 | Varian Associates, Inc. | Counterflow leak detector with cold trap |
FR2604522B1 (fr) * | 1986-09-26 | 1989-06-16 | Cit Alcatel | Installation de detection de fuite a gaz traceur et procede d'utilisation |
EP0283543B1 (fr) * | 1987-03-27 | 1991-12-11 | Leybold Aktiengesellschaft | Appareil de détection de fuites et son fonctionnement |
US4845360A (en) * | 1987-12-10 | 1989-07-04 | Varian Associates, Inc. | Counterflow leak detector with high and low sensitivity operating modes |
EP0344345B1 (fr) * | 1988-06-01 | 1991-09-18 | Leybold Aktiengesellschaft | Système à pompe pour un appareil de détection de fuite |
DE3828588C1 (fr) * | 1988-08-23 | 1989-12-07 | Alcatel Hochvakuumtechnik Gmbh, 6980 Wertheim, De | |
US4893497A (en) * | 1988-09-12 | 1990-01-16 | Philip Danielson | Leak detection system |
US5049168A (en) * | 1988-09-12 | 1991-09-17 | Philip Danielson | Helium leak detection method and system |
DE3831258C1 (fr) * | 1988-09-14 | 1989-10-12 | Alcatel Hochvakuumtechnik Gmbh, 6980 Wertheim, De | |
US5010761A (en) * | 1990-03-01 | 1991-04-30 | Superior Industries International, Inc. | Automated leak detection apparatus and method therefor |
FR2666410B1 (fr) | 1990-09-05 | 1993-10-08 | Alcatel Cit | Detecteur de fuite haut flux a trois filtres moleculaires. |
FR2681688B1 (fr) * | 1991-09-24 | 1993-11-19 | Alcatel Cit | Installation de detection de fuites de gaz utilisant la technique de reniflage. |
FR2681689B1 (fr) * | 1991-09-25 | 1993-11-12 | Alcatel Cit | Detecteur de fuite a gaz traceur. |
DE4140366A1 (de) * | 1991-12-07 | 1993-06-09 | Leybold Ag, 6450 Hanau, De | Lecksucher fuer vakuumanlagen sowie verfahren zur durchfuehrung der lecksuche an vakuumanlagen |
DE4228313A1 (de) * | 1992-08-26 | 1994-03-03 | Leybold Ag | Gegenstrom-Lecksucher mit Hochvakuumpumpe |
DE4408877A1 (de) * | 1994-03-16 | 1995-09-21 | Leybold Ag | Testgaslecksucher |
JP2655315B2 (ja) * | 1994-06-29 | 1997-09-17 | 日本真空技術株式会社 | 複合分子ポンプを使用した漏洩探知装置 |
DE4442174A1 (de) * | 1994-11-26 | 1996-05-30 | Leybold Ag | Lecksuchgerät mit Vakuumpumpen und Betriebsverfahren dazu |
FR2728072B1 (fr) * | 1994-12-07 | 1997-01-10 | Cit Alcatel | Detecteur de fuite |
DE4445829A1 (de) * | 1994-12-22 | 1996-06-27 | Leybold Ag | Gegenstrom-Schnüffellecksucher |
ES2192568T3 (es) * | 1994-12-23 | 2003-10-16 | Unaxis Balzers Ag | Procedimiento para el analisis de gases y analizador de gases. |
DE19504278A1 (de) * | 1995-02-09 | 1996-08-14 | Leybold Ag | Testgas-Lecksuchgerät |
DE19522466A1 (de) * | 1995-06-21 | 1997-01-02 | Leybold Ag | Lecksuchgerät mit Vorvakuumpumpe |
DE19638506A1 (de) * | 1996-09-20 | 1998-03-26 | Leybold Vakuum Gmbh | Verfahren zur Untersuchung einer Mehrzahl ähnlicher Prüflinge auf Lecks sowie für die Durchführung dieses Verfahrens geeigneter Lecksucher |
DE19735250A1 (de) * | 1997-08-14 | 1999-02-18 | Leybold Vakuum Gmbh | Verfahren zum Betrieb eines Heliumlecksuchers und für die Durchführung dieses Verfahrens geeigneter Heliumlecksucher |
DE10156205A1 (de) * | 2001-11-15 | 2003-06-05 | Inficon Gmbh | Testgaslecksuchgerät |
-
2001
- 2001-11-15 DE DE10156205A patent/DE10156205A1/de not_active Withdrawn
-
2002
- 2002-11-12 JP JP2003544435A patent/JP4164030B2/ja not_active Expired - Fee Related
- 2002-11-12 EP EP02787638A patent/EP1444495A1/fr not_active Withdrawn
- 2002-11-12 US US10/496,718 patent/US7082813B2/en not_active Expired - Fee Related
- 2002-11-12 WO PCT/EP2002/012601 patent/WO2003042651A1/fr active Application Filing
Non-Patent Citations (1)
Title |
---|
See references of WO03042651A1 * |
Also Published As
Publication number | Publication date |
---|---|
WO2003042651A1 (fr) | 2003-05-22 |
JP4164030B2 (ja) | 2008-10-08 |
DE10156205A1 (de) | 2003-06-05 |
JP2006515666A (ja) | 2006-06-01 |
US7082813B2 (en) | 2006-08-01 |
US20050066708A1 (en) | 2005-03-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
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17P | Request for examination filed |
Effective date: 20040303 |
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AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR IE IT LI LU MC NL PT SE SK TR |
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RIN1 | Information on inventor provided before grant (corrected) |
Inventor name: GROSSE-BLEY, WERNER Inventor name: BOEHM, THOMAS Inventor name: HIRCHE, RALF |
|
17Q | First examination report despatched |
Effective date: 20100201 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
18D | Application deemed to be withdrawn |
Effective date: 20100812 |