Classifications

• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B19/00—Layered products comprising a layer of natural mineral fibres or particles, e.g. asbestos, mica
  • B32B19/06—Layered products comprising a layer of natural mineral fibres or particles, e.g. asbestos, mica next to a fibrous or filamentary layer
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
  • B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
  • B32B5/24—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
  • B32B5/26—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary
• • C—CHEMISTRY; METALLURGY
  • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
  • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
  • C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
  • C04B26/02—Macromolecular compounds
  • C04B26/04—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
  • C04B26/06—Acrylates
• • C—CHEMISTRY; METALLURGY
  • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
  • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
  • C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
  • C04B26/02—Macromolecular compounds
  • C04B26/28—Polysaccharides or derivatives thereof
• • C—CHEMISTRY; METALLURGY
  • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
  • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
  • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
  • C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
• • C—CHEMISTRY; METALLURGY
  • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
  • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
  • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
  • C04B28/28—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing organic polyacids, e.g. polycarboxylate cements, i.e. ionomeric systems
• • D—TEXTILES; PAPER
  • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
  • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
  • D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
  • D21H27/30—Multi-ply
  • D21H27/38—Multi-ply at least one of the sheets having a fibrous composition differing from that of other sheets
• • D—TEXTILES; PAPER
  • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
  • D21J—FIBREBOARD; MANUFACTURE OF ARTICLES FROM CELLULOSIC FIBROUS SUSPENSIONS OR FROM PAPIER-MACHE
  • D21J1/00—Fibreboard
  • D21J1/16—Special fibreboard
  • D21J1/20—Insulating board
• • E—FIXED CONSTRUCTIONS
  • E04—BUILDING
  • E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
  • E04B9/00—Ceilings; Construction of ceilings, e.g. false ceilings; Ceiling construction with regard to insulation
  • E04B9/001—Ceilings; Construction of ceilings, e.g. false ceilings; Ceiling construction with regard to insulation characterised by provisions for heat or sound insulation
• • E—FIXED CONSTRUCTIONS
  • E04—BUILDING
  • E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
  • E04B9/00—Ceilings; Construction of ceilings, e.g. false ceilings; Ceiling construction with regard to insulation
  • E04B9/04—Ceilings; Construction of ceilings, e.g. false ceilings; Ceiling construction with regard to insulation comprising slabs, panels, sheets or the like
  • E04B9/045—Ceilings; Construction of ceilings, e.g. false ceilings; Ceiling construction with regard to insulation comprising slabs, panels, sheets or the like being laminated
• • G—PHYSICS
  • G10—MUSICAL INSTRUMENTS; ACOUSTICS
  • G10K—SOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
  • G10K11/00—Methods or devices for transmitting, conducting or directing sound in general; Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
  • G10K11/16—Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
  • G10K11/162—Selection of materials
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2250/00—Layers arrangement
  • B32B2250/02—2 layers
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2250/00—Layers arrangement
  • B32B2250/20—All layers being fibrous or filamentary
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
  • B32B2262/06—Vegetal fibres
  • B32B2262/062—Cellulose fibres, e.g. cotton
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2307/00—Properties of the layers or laminate
  • B32B2307/50—Properties of the layers or laminate having particular mechanical properties
  • B32B2307/56—Damping, energy absorption
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2315/00—Other materials containing non-metallic inorganic compounds not provided for in groups B32B2311/00 - B32B2313/04
  • B32B2315/14—Mineral wool
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2317/00—Animal or vegetable based
  • B32B2317/12—Paper, e.g. cardboard
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B2419/00—Buildings or parts thereof
• • C—CHEMISTRY; METALLURGY
  • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
  • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
  • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
  • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
  • C04B2111/00612—Uses not provided for elsewhere in C04B2111/00 as one or more layers of a layered structure
• • C—CHEMISTRY; METALLURGY
  • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
  • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
  • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
  • C04B2111/52—Sound-insulating materials
• • D—TEXTILES; PAPER
  • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
  • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
  • D21H13/00—Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
  • D21H13/36—Inorganic fibres or flakes
  • D21H13/38—Inorganic fibres or flakes siliceous
  • D21H13/40—Inorganic fibres or flakes siliceous vitreous, e.g. mineral wool, glass fibres
• • D—TEXTILES; PAPER
  • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
  • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
  • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
  • D21H17/20—Macromolecular organic compounds
  • D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
  • D21H17/24—Polysaccharides
  • D21H17/28—Starch
• • D—TEXTILES; PAPER
  • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
  • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
  • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
  • D21H17/63—Inorganic compounds
  • D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
• • D—TEXTILES; PAPER
  • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
  • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
  • D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
  • D21H27/30—Multi-ply
  • D21H27/32—Multi-ply with materials applied between the sheets
  • D21H27/34—Continuous materials, e.g. filaments, sheets, nets
• • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
  • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
  • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
  • Y02W30/00—Technologies for solid waste management
  • Y02W30/50—Reuse, recycling or recovery technologies
  • Y02W30/91—Use of waste materials as fillers for mortars or concrete

Definitions

• This invention relates to an acoustical celling tile having an improved sound absorption value. More particularly, this invention relates to a dual layer acoustical ceiling tile having a low or no mineral wool base mat layer and a high mineral wool overlay surface layer which provides improved sound absorption values with or without perforating or fissuring the tile. The invention also relates to a dual layer acoustical tile which is manufactured using a high speed, water-felting process. A pattern can be applied before drying the tile (wet end embossing), or the pattern can be formed in the tile after the drying.
• the water-felting of dilute aqueous dispersions of mineral wool and lightweight aggregate is a commercial process for manufacturing acoustical ceiling tile.
• a dispersion of mineral wool, lightweight aggregate, binder and other ingredients as desired or necessary is flowed onto a moving foraminous support wire, such as that of a Fourdrinier or Oliver mat forming machine, for dewatering.
• the dispersion is first dewatered by gravity and then vacuum suction is applied. After vacuum dewatering, the wet mat is dried in heated convection drying ovens, and the dried mat is cut to the desired panel or tile dimensions. If desired, the panels or tiles can be top coated with- paint.
• Acoustical ceiling tiles can also be made by a wet pulp molding or cast process such as described in U.S. Patent No. 1,769,519.
• a molding composition comprising granulated mineral wool fibers, fillers, colorants and a binder (e.g. starch gel), is prepared for molding or casting the tile.
• the composition is placed upon suitable trays which have been covered with paper or a metallic foil and then the composition is screeded to a desired thickness with a screed bar or roller.
• a decorative surface, such as elongated fissures, may be provided by the screed bar or roller.
• the trays filled with the mineral wool composition are then placed in an oven to dry or cure.
• control tile samples were tested for NRC (noise reduction coefficient) using the Impedance tube method.
• the samples were not perforated, fissured or painted.
• the control tiles had an average NRC value of only 0.434.
• acoustical tiles made using a water-felting process have a hard surface that does not have good sound absorption properties.
• the sound absorption is substantially improved by fissuring and/or perforating the surface that increases the NRC value.
• many purchasers prefer a smooth, unperforated acoustical ceiling tile for its aesthetic appearance.
• acoustical ceiling tiles having an average NRC equivalent to commercially available cast ceiling tiles can be made by using an anionically stabilized latex binder and a cationic flocculant to couple the latex binder onto the mineral fiber materials.
• the mineral fibers constitute about 50% or more of the total dry solids, preferably from about 60 to about 95 weight % of the acoustical panel.
• the tiles made by this process are quite soft compared to the water-felted tiles having a starch binder.
• the tiles made with a latex binder have lower structural strength and are made in thicknesses of at least about inch and frequently have a woven scrim applied thereto to increase strength.
• These acoustical tiles do have smooth surfaces and higher NRC values resulting from the higher mineral wool content. Mineral wool acoustical tiles are porous which is necessary to provide good sound absorption.
• NRC sound absorption value
• a dual layer acoustical ceiling tile having an improved sound absorption value can be made in a water-felting process wherein a base mat layer has a relatively low mineral fiber content, and a surface layer having a high mineral fiber content is overlaid onto the base mat.
• the base mat layer is made from a low mineral fiber content or no mineral fiber material which has relatively low NRC values unless its surface is perforated and/or fissured.
• the mineral fiber-rich surface layer that has a thickness of about ⁇ A inch or less also has a relatively low NRC value at such thickness. It was discovered that these two low NRC value materials could be combined to provide a dual layer ceiling tile having a high NRC value.
• the acoustical ceiling tiles of this invention are based on the discovery that two acoustical materials having relatively low NRC values can be combined to form a dual layer acoustical ceiling tile having excellent sound absorption values (NRC). These ceiling tiles are made using a water-felting process to form both the base mat layer and the fiber-rich surface layer. In carrying out the process, two head boxes are used to feed the acoustical materials to the production line.
• One head box feeds the base mat material, having a relatively low mineral fiber content (less than about 50% by weight of mineral fiber) or it may contain no mineral fiber, to a moving foraminous support wire, such as that of a Fourdrinier or Oliver mat forming machine for dewatering. After water is removed through the support wire by gravity, additional water can be removed by applying a vacuum to the wet base mat, but depending upon the consistency of the base mat material in the head box, the line speed and other considerations, it may not be necessary to use vacuum for dewatering purposes prior to depositing the fiber-rich overlay material onto the base mat.
• the base mat material consists essentially of mineral wool fibers, expanded perlite, cellulose fiber, starch binder and gypsum which can be present, preferably, in the following amounts, and having at least about 30 % by weight of expanded perlite:
• the still wet base mat may be passed under a press roller to compress the mat, removing more water and establishing the thickness of the wet base mat.
• the thickness of the wet base mat just prior to depositing the fiber-rich surface layer may range from about 1 inch to about 2.5 inches. It is preferred that the completely dried base mat have a thickness ranging from about 0.25 inch to about 0.625 inch.
• a fiberglass scrim can be placed on the wet base mat prior to depositing the fiber-rich surface layer.
• the fiberglass scrim can be either woven or non-woven.
• a fiberglass scrim it is generally preferred that it be placed between the base mat material and the fiber-rich surface layer, however, if desired, the scrim can be placed on top of the fiber-rich surface layer or in contact with the back of the base mat material, in which case, the base mat slurry from the head box would be deposited on the scrim.
• the fiber-rich surface layer consists essentially of mineral wool fibers, gypsum, clay filler, latex binder, starch binder and flocculant to deposit the latex binder on the mineral wool fibers as disclosed in U.S. Patent No. 5,250,153. These ingredients may be present, preferably, in the following amounts:
• the fiber-rich surface material is prepared in accordance with the method disclosed in U.S. Patent No. 5,250,153 wherein an anionically stabilized latex binder is deposited on or coupled to the mineral fibers by adding a small amount of a flocculant such as a cationic polyacrylamide to the slurry.
• the fiber-rich slurry contains a very large amount of mineral wool fibers (at least about 75 % by weight) and little or no expanded perlite.
• the fiber-rich material is deposited on the base mat from a second headbox to form a dual layer material which is dewatered by applying a vacuum to the wet dual layer material and also by passing the wet dual layer material under a press roll. The press roll helps to remove some of the water.
• the fiber-rich surface is textured and the thickness of the dual layer material is established under the pattern/texture roll.
• the dual layer material is subsequently passed to an oven to complete the drying process and to cure the starch and latex binders.
• the dual layer material When completely dried and cut into ceiling tiles, the dual layer material has a smooth or textured surface that is rich in mineral wool fibers and unperforated.
• the dried dual layer ceiling tiles have a total thickness ranging from about 0.5 inch to about 1 inch, with the thickness of the fiber-rich surface layer ranging from about 0.125 inch to about 0.5 inch.
• the thickness of the wool-rich surface layer can be increased from about 0.5 inch to about 0.625 inch to provide higher NRC values.
• a "wet end coating" Prior to drying the dual layer material in an oven, it is preferred to apply a "wet end coating" to the mineral fiber-rich surface, which is smooth and unperforated.
• One or more coats of paint may be spray applied. It has been found that the application of paint actually increases the NRC value, because the unpainted surface tends to reflect the sound and therefore has a lower NRC (noise reduction coefficient).
• Other ingredients may also be present in either the base mat or the fiber-rich surface layer or both layers. Examples of such ingredients include dyes, pigments, inorganic fillers, antioxidants, surfactants, water repellents, fire retardants and the like.
• gypsum calcium sulfate dihydrate
• the gypsum is soluble in the aqueous slurry comprising both the base mat and the fiber-rich layer feed material.
• the solubility of the gypsum in the processing slurry enables the gypsum to function as a flocculant in the slurry formulation.
• the flocculating function provides uniform distribution of fine particles (e.g. clay, gypsum, perlite and starch) present in the formulation during mixing. This flocculating function helps to prevent the fine and high density particles from migrating to the bottom of the mat.
• the gypsum helps to disperse the mineral wool fibers in the aqueous slurry.
• a starch binder is also present in both the base mat and the fiber- rich surface layer. It is preferred to use the starch in the form of a gel which is prepared by dispersing starch particles in water and heating the slurry until the starch is fully cooked and the slurry thickens to a viscous gel. If the binder is corn starch, cooking temperatures may range from about 180°F. (82 °C.) to about 195°F. (90°O). It should be noted that starch may also be used as a binder without pre-cooking the starch to form a gel. In addition, the starch can be used in a pre-gelatinized form which is converted to a gel merely by adding it to water, without the need to cook it.
• Samples of commercially available, mineral fiber-rich, acoustical ceiling tiles were used to determine sound absorption properties (NRC values) for thin layer (approximately % inch thick) materials. Such materials do not have sufficient structural strength to be made in a water- felting process in such thin layers, and therefore, ceiling tiles were made having a thickness of about 0.7 inch and a density of about 16 pcf.
• the tiles had a back coating of 35-C clay at coverage of about 24 grams/ft. 2 (dry) which increase the tile density by about 0.85 pcf.
• the thin layer samples were cut from the back of the tile.
• Samples 1-4 had the following formulation:
• the purpose of this trial was to determine the effect of different amounts of latex binder in the fiber-rich overlay formulation, particularly its effect on the dry mat surface hardness.
• the base mat had the following formulation:
• a standard water-felting process was used to make the base mat, with the stock material having a consistency of about 5.8 % by weight of solids.
• the line speed was about 30 feet/minute.
• the dried base mat had a thickness of about 0.5 inch.
• the fiber-rich overlay material had the following formulation:
• the mineral wool, starch, latex binder, clay and gypsum combined had a total weight of 173.6 lbs. and were added to 500 gallons of water, providing a stock consistency of about 4% by weight of solids.
• the flocculant was subsequently added after thorough mixing of the stock to deposit the latex binder on the mineral fibers.
• the stock was fed through a 4 foot wide head box at a rate of about 125 gallons/miriute.
• the NRC values were determined using the Impedance tube method as follows:
• the surface of the dried tiles (both formulations) was hard.
• EXAMPLE 3 In this trial, the use of paper fiber in the fiber-rich overlay formulation was evaluated.
• the base mat used the same formulation as in Example 2 and also the same standard water-felting process.
• the fiber-rich overlay material had the following formulation:
• the NRC values were determined using the Impedance tube method as follows:
• the fiber-rich overlay material had the following formulation:
• the NRC values were determined using the Impedance tube method as follows:
• the increased use of gypsum in the overlay formulation increased the surface hardness and smoothness.
• the base mat used the same formulation as in Example 2 and also the same standard water-felting process.
• the fiber-rich overlay material had the following formulation:
• test 1 A pair of samples were evaluated in each test.
• test 2 the samples were spray painted once.
• test 3 the samples were spray painted twice, and in test 3, they were spray painted three times.
• the NRC values were determined using the Impedance tube method as follows:
• EXAMPLE 7 Two different overlay formulations were tested for their full-scale NRC values.
• the base mat formulation was the same as reported in Example 6.
• the overlay formulations were as follows:
• Dual layer ceiling tiles were made including the application of a glass fiber scrim onto the mineral wool rich surface.
• the base mat formulation was the same as the formulation used in Example 6.
• the mineral wool rich overlay was approximately 0.25 inches in thickness and contained 86% by weight of mineral wool.
• the mineral wool rich overlay surface was not ground and was not perforated.
• a standard, non-woven glass fiber scrim was applied to the mineral wool rich overlay surface using an adhesive.
• the adhesive was Super 77 multipurpose spray adhesive made by 3M Company. The adhesive coverage was approximately 1.5 gm/ftA
• the dual layer tiles were spray painted (single application) on the mineral wool rich surface with a standard acoustical tile paint.
• the paint coverage was approximately 27 gm/ft. 2 .
• the tiles were tested for estimated (Impedance Tube) NRC values.
• Dual layer ceiling tiles having a calcium carbonate surface coating were evaluated for estimated NRC value.
• the dual layer tiles were not perforated.
• the base mat formulation was the same as the formulation used in Example 6.
• the mineral wool rich overlay was approximately 0.25 inches in thickness and contained 86% by weight of mineral wool.
• the mineral wool rich surface was coated with dry calcium carbonate particles.
• the coarse calcium carbonate was spray coated at a coverage of about 38 gm./ft. 2 .
• Prior to applying the calcium carbonate the tiles were painted with standard acoustical tile paint. The paint was applied with a roll coat and then with a flow coat and dried. After applying the calcium carbonate, the tiles were spray painted with a standard acoustical tile paint and were dried.
• This dual layer ceiling tile with the calcium carbonate coating had an estimated NRC of 0.50.

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• Chemical & Material Sciences (AREA)
• Engineering & Computer Science (AREA)
• Ceramic Engineering (AREA)
• Structural Engineering (AREA)
• Organic Chemistry (AREA)
• Materials Engineering (AREA)
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