EP1307305B1 - Method and strand guide for supporting, guiding and cooling casting strands made of steel, especially preliminary sections for girders - Google Patents
Method and strand guide for supporting, guiding and cooling casting strands made of steel, especially preliminary sections for girders Download PDFInfo
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- EP1307305B1 EP1307305B1 EP01965178A EP01965178A EP1307305B1 EP 1307305 B1 EP1307305 B1 EP 1307305B1 EP 01965178 A EP01965178 A EP 01965178A EP 01965178 A EP01965178 A EP 01965178A EP 1307305 B1 EP1307305 B1 EP 1307305B1
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- 238000001816 cooling Methods 0.000 title claims abstract description 43
- 238000000034 method Methods 0.000 title claims abstract description 12
- 229910000831 Steel Inorganic materials 0.000 title claims abstract description 5
- 239000010959 steel Substances 0.000 title claims abstract description 5
- 238000005266 casting Methods 0.000 title abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000007921 spray Substances 0.000 claims description 34
- 238000009749 continuous casting Methods 0.000 claims description 10
- 230000015572 biosynthetic process Effects 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 4
- 230000003247 decreasing effect Effects 0.000 claims description 2
- 230000002250 progressing effect Effects 0.000 claims description 2
- 239000007791 liquid phase Substances 0.000 claims 6
- 238000007711 solidification Methods 0.000 abstract description 12
- 230000008023 solidification Effects 0.000 abstract description 12
- 230000002631 hypothermal effect Effects 0.000 description 5
- 230000002787 reinforcement Effects 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- IHQKEDIOMGYHEB-UHFFFAOYSA-M sodium dimethylarsinate Chemical class [Na+].C[As](C)([O-])=O IHQKEDIOMGYHEB-UHFFFAOYSA-M 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/009—Continuous casting of metals, i.e. casting in indefinite lengths of work of special cross-section, e.g. I-beams, U-profiles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/12—Accessories for subsequent treating or working cast stock in situ
- B22D11/124—Accessories for subsequent treating or working cast stock in situ for cooling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/12—Accessories for subsequent treating or working cast stock in situ
- B22D11/128—Accessories for subsequent treating or working cast stock in situ for removing
- B22D11/1282—Vertical casting and curving the cast stock to the horizontal
Definitions
- the invention relates to a method and a strand guide for supporting, guiding and cooling of cast strands of steel, in particular of BBL pre-profiles for Support in which the cast strand after leaving the continuous casting mold in a Zero segment by means of secondary cooling and in subsequent support segments further cooled by water and pulled out.
- the function of the strand guide not only the Supports the cast strand against the ferrostatic pressure includes, but also the withdrawal of solidification heat by the secondary cooling and the Maintaining the profile geometry generated in the continuous casting mold. It kick however, surface cracks still occur.
- the goal of the strand guide must be a faultless surface quality of the Casting, an interior quality without cracks and without segregation at high Be true to profile.
- the object is achieved by a method according to the preamble of claim 1 according to the invention achieved in that to avoid an undesirable solidification structure on the flange upper edges or in other cross-sectional areas the cooling and support of the beam blank format the solidification areas adapted so that only in areas where sump formation is present, cooled and supported.
- An embodiment of the method provides that the cast strand through Targeted temperature control in upper support segments with at least the length the support rollers corresponding widths of the spray water jets at Lekssund Transverse sides of the G confusestrangqueritess cooled and analogous to Strangwegbone and the cooling state in core zones of G fauxstrangqueritess supported on the transverse sides decreasing and only with on the liquid core zones directed spray water jets with the same or smaller Width of the bottom side is cooled. This will cause hypothermia Strand shell avoided, and the risk of cracks, especially surface cracks, is significantly reduced.
- the cast strand through targeted temperature control in the zero support segment at its profile ends and in the longitudinal side center region of its cross section and on the Transverse sides supported, and thereby longitudinal sides and transverse sides of the G collectstrangqueritess, except the cast strand profile corner sections, cooled and that with strand shell formation progressing along the strand path length only the center area and the two transverse sides of the G collectstrangqueritess and in the area of the swamp tips of the core zones the transverse sides are restricted in the region of the sump tip or sump tips supported and cooled and on the long sides only on the Swamp zone directed spray water jets are used.
- This can a targeted temperature control depending on the cross-sectional zones of the G cleverstrangquerites not only in rectangular G cleverstrangquerexcellent, but also be achieved in profile strands.
- the targeted temperature control can also be completed to that the cast strand in the state of substantial solidification without Spray water jets and without top and side supports, on support rollers is guided on-the-floor.
- the support and secondary cooling are designed according to further features such that in the zero support segment longitudinal sides of the G confusestrangqueritess by means of symmetrically arranged longer support roller pairs and the G fauxstrang profile corner areas supported by Tipprollenrunen shorter length are, and that the transverse sides of the G fauxstrangqueritess means of about the Side length correspondingly long support roller pairs are supported.
- Such Support is e.g. advantageous for strand shell thicknesses between 30 and 50 mm.
- the support is practically from all sides only in the sump profile to unwanted To avoid hypothermia.
- Another embodiment provides that in the following support segments to the Longitudinal sides of the G fauxstrangqueritess only the center symmetrically arranged, longer support roller pairs, and on the transverse sides about the side length corresponding support roller pairs are provided.
- the Strand shell thickness already assumed between 40 to 60 mm, so that the corner regions of the G fauxstrangqueritess are no longer supported have to.
- An improvement provides that the spray pattern of the secondary cooling analog designed for G mansumpf core zone. As a result, too high a water supply be avoided.
- Another embodiment provides that a long support role as well wider or wider spray water jet is assigned. This measure is especially applicable for relatively thin strand shells of about 30 to 60 mm.
- an embodiment may consist in that tapping rolls only still provided in a support segment following the zero support segment are.
- a cast strand 1 for a pre-profile 2 from the carrier rolled ( Figures 1 and 1A).
- the casting strand 1 is after the Leaving the continuous casting mold 3 in a zero support segment 4 with a secondary cooling and subsequently in further support segments 5, 6 and 7 Spray water jets 8 cooled and powered rollers of a Ausziehmaschine 9 pulled out.
- the length L designates the entire plant length of the Continuous casting mold 3 up to the Ausziehmaschine 9. Also put the radii R1, R2 and R3 fix the arc of the strand course.
- the form-true, cast strand 1 produced in the continuous casting mold 3 into the zero support segment 4 (Fig. 2B), in which the casting strand 1 by means of the longitudinal side 13 arranged in the longitudinal side center region 16 support rollers 17 and to the Transverse sides 14 arranged support rollers 18 is supported.
- the G hasslestrang-Profileck Schemee 19 not cooled, but supported by means of 20 Tipprollen.
- the spray water jets 8 each form opposite, still in the liquid or viscous range strand and its strand width or strand thickness an opening in the flow direction angle.
- the core zone 15 ( Figure 2F) is very small, leaving the cast strand 1 no longer needs to be cooled and only by means of Support rollers 18 is guided on the transverse sides 14.
- the smaller Kemzonen 15 continues and the casting strand 1 is only on the horizontal Support rollers 22 out.
- the cast strand 1 is solidified.
- the Thickness of the strand shell 21 is, for example (depending on the respective Casting cross-section dimensions) in each case in FIG. 2B with 38.2 mm, in FIG. 2C with 54.0 mm, in Fig. 2D with 66.1 mm, in Fig. 2E with 76.4 mm, in Fig. 2F with 85.4 mm, 93.5 mm in FIG. 2G and 101.0 mm in FIG. 2H.
- Fig. 3 one of the support segments 5,6,7 is shown. After that are essential Assemblies each have a top frame 23, a bottom frame 24, side frames 25, removal rollers 26 and battens 27.
- FIGS. 4A and 4B show the respective ones extending in the directions of the arrows 28 Outflow of spray water 29.
- the drain is in particular by a "open" design of the support segments 5,6,7, allows, wherein the G fauxstrangquerites 1a starting from an open frame in each case from the outside Ribs 30, reinforcements 31, inner ribs 32 and one nozzle 33 is surrounded on four sides.
- FIG. 4A corresponds approximately to the strand path length in FIG Figs. 2B and 2C.
- the representation of FIG. 4B corresponds to the strand path length of FIG Fig. 2D.
- Fig. 5 shows a vertical section through the drawn in operating position Support segment 5,6,7, wherein the open design of a support segment 5, 6, 7 is particularly easy to recognize.
- the nozzle sticks 33 through the Spray water jets 8 directed against the G fauxstrangquerêt 1a splashing 29 can easily drain between the reinforcements 31 all around.
- FIG. 6 a support roller stand 5, 6, 7 is described in FIG Training in operational position drawn in view.
Abstract
Description
Die Erfindung betrifft ein Verfahren und eine Strangführung zum Stützen, Führen und Kühlen von Gießsträngen aus Stahl, insbesondere von BBL-Vorprofilen für Träger, bei dem der Gießstrang nach Verlassen der Stranggießkokille in einem Null-Segment mittels Sekundärkühlung und in nachfolgenden Stützsegmenten weiter durch Spritzwasser gekühlt und ausgezogen wird.The invention relates to a method and a strand guide for supporting, guiding and cooling of cast strands of steel, in particular of BBL pre-profiles for Support in which the cast strand after leaving the continuous casting mold in a Zero segment by means of secondary cooling and in subsequent support segments further cooled by water and pulled out.
Aus der JP 42 00 844 ist es bekannt, in einer Strangführung für die Gießquerschnitts-Längsseiten einzelne Stützrollen, teils als Tipprollen, teils als im Profilgrund angeordnete Längsrollen geringer Länge, einzusetzen. An den Gießquerschnitts-Breitseiten sind dann entsprechend lange Stützrollen angeordnet. Diese Anordnung nimmt jedoch keine Rücksicht auf die an den betreffenden Gießstrang-Stellen vorhandenen Strangschalendicken und die erforderliche Kühlung.From JP 42 00 844 it is known in a strand guide for Gießquerschnitts-longitudinal sides individual support rollers, partly as Tipprollen, partly as in Profilgrund arranged longitudinal rollers of short length to use. To the Cast cross-section broadsides are then arranged correspondingly long support rollers. However, this arrangement takes no account of the on relevant cast strand bodies existing strand shell thicknesses and the required cooling.
Aus dem Bericht "Das Gießen von Beam Blanks im Elektrostahlwerk der Stahlwerk Thüringen GmbH, Unterwellenborn" ( Dengler, J-M et al, Stahl und Eisen, 1997, Nr. 5 ) ist eine geeignete Strangführung bekannt. Darin wird gelehrt, zusätzlich zur Wasserkühlung des Stranges den Steg, beide Flansche und die vier Flanschspitzen mittels ungleich langen Stützrollen zu führen. Ab der 11. Ebene bis zum Ende des betreffenden Stützsegments bei der 20. Rollen-ebene wird der Gießstrang nur noch am Steg und an beiden Flanschen mit 4 Stützrollen geführt. Die Außenkühlung ist jedoch nur in Abhängigkeit des Erstarrungszustandes geregelt.From the report "The casting of beam blanks in the electric steelworks of Stahlwerk Thüringen GmbH, Unterwellenborn "(Dengler, J-M et al, Stahl and Eisen, 1997, No. 5), a suitable strand guide is known. It teaches in addition to the water cooling of the strand the bridge, both flanges and the four flange tips to lead by means of unequal length support rollers. From the 11th Level to the end of the relevant support segment at the 20th roller level the cast strand is only on the bridge and on both flanges with 4 support rollers guided. The external cooling is only dependent on the Solidification state regulated.
Es ist zu berücksichtigen, dass die Funktion der Strangführung nicht nur das Stützen des Gießstranges gegen den ferrostatischen Druck umfasst, sondern auch den Entzug der Erstarrungswärme durch die Sekundärkühlung und die Erhaltung der Profilgeometrie, die in der Stranggießkokille erzeugt wird. Es treten jedoch immer noch Oberflächenrisse auf.It should be noted that the function of the strand guide not only the Supports the cast strand against the ferrostatic pressure includes, but also the withdrawal of solidification heat by the secondary cooling and the Maintaining the profile geometry generated in the continuous casting mold. It kick however, surface cracks still occur.
Das Ziel der Strangführung muss eine fehlerfreie Oberflächenqualität des Gießstranges, eine Innenqualität ohne Risse und ohne Seigerungen bei hoher Profiltreue sein.The goal of the strand guide must be a faultless surface quality of the Casting, an interior quality without cracks and without segregation at high Be true to profile.
Der Erfindung liegt die Aufgabe zugrunde, Risse in der Gefügestruktur, insbesondere Oberflächenkühlrisse, durch Anpassung der Abkühlbedingungen der Strangoberfläche im Bereich der Sekundärkühlung, und in dieser insbesondere eine Unterkühlung der Strangschale zu vermeiden. The invention is based on the object, cracks in the microstructure, in particular surface cooling cracks, by adaptation of the cooling conditions the strand surface in the area of secondary cooling, and in this in particular to avoid hypothermia of the strand shell.
Die Aufgabe wird mit einem Verfahren gemäß Oberbegriff von Anspruch 1 erfindungsgemäß
dadurch gelöst, dass zur Vermeidung einer unerwünschten Erstarrungsstruktur
auf den Flanschoberkanten oder in anderen Querschnittsbereichen
die Kühlung und Stützung des Beam Blank-Formates den Erstarrungsbereichen
derart angepaßt wird, dass nur in Bereichen, bei welchen Sumpfausbildung
vorliegt, gekühlt und gestützt wird.The object is achieved by a method according to the preamble of
Eine Ausgestaltung des Verfahrens sieht dabei vor, dass der Gießstrang durch gezielte Temperaturführung in oberen Stützsegmenten mit zumindest der Länge der Stützrollen entsprechenden Breiten der Spritzwasserstrahlen an Längsund Querseiten des Gießstrangquerschnitts gekühlt und analog zur Strangweglänge und dem Abkühlungszustand in Kemzonen des Gießstrangquerschnitts an dessen Querseiten abnehmend gestützt und nur noch mit auf die flüssigen Kernzonen gerichteten Spritzwasserstrahlen mit gleicher oder kleinerer Breite der Sumpfseite gekühlt wird. Dadurch wird eine Unterkühlung der Strangschale vermieden, und die Gefahr von Rissen, insbesondere von Oberflächenrissen, wird erheblich reduziert.An embodiment of the method provides that the cast strand through Targeted temperature control in upper support segments with at least the length the support rollers corresponding widths of the spray water jets at Längsund Transverse sides of the Gießstrangquerschnitts cooled and analogous to Strangweglänge and the cooling state in core zones of Gießstrangquerschnitts supported on the transverse sides decreasing and only with on the liquid core zones directed spray water jets with the same or smaller Width of the bottom side is cooled. This will cause hypothermia Strand shell avoided, and the risk of cracks, especially surface cracks, is significantly reduced.
In weiterer Ausgestaltung der Erfindung wird vorgeschlagen, dass der Gießstrang durch gezielte Temperaturführung im Null-Stützsegment an seinen Profilenden und im Längsseiten-Mittenbereich seines Querschnitts sowie an den Querseiten gestützt, und dabei Längsseiten und Querseiten des Gießstrangquerschnitts, ausgenommen die Gießstrang-Profileckbereiche, gekühlt werden, und dass bei auf der Strangweglänge fortschreitender Strangschalenbildung nur noch der Mittenbereich und die beiden Querseiten des Gießstrangquerschnitts gestützt werden, und im Bereich der Sumpfspitzen der Kemzonen die Querseiten im Bereich der Sumpfspitze bzw. der Sumpfspitzen eingeschränkt gestützt und gekühlt und an den Längsseiten nur noch auf die Sumpfzone gerichtete Spritzwasserstrahlen eingesetzt werden. Dadurch kann eine gezielte Temperaturführung abhängig von den Querschnitts-Zonen des Gießstrangquerschnitts nicht nur bei rechteckigem Gießstrangquerschnitt, sondern auch bei Profilsträngen erzielt werden. In a further embodiment of the invention, it is proposed that the cast strand through targeted temperature control in the zero support segment at its profile ends and in the longitudinal side center region of its cross section and on the Transverse sides supported, and thereby longitudinal sides and transverse sides of the Gießstrangquerschnitts, except the cast strand profile corner sections, cooled and that with strand shell formation progressing along the strand path length only the center area and the two transverse sides of the Gießstrangquerschnitts and in the area of the swamp tips of the core zones the transverse sides are restricted in the region of the sump tip or sump tips supported and cooled and on the long sides only on the Swamp zone directed spray water jets are used. This can a targeted temperature control depending on the cross-sectional zones of the Gießstrangquerschnitts not only in rectangular Gießstrangquerschnitt, but also be achieved in profile strands.
Weitere Erfindungs-Merkmale sehen vor, dass im Bereich der Sumpfzone der Gießstrangquerschnitt an seinen Querseiten ohne Spritzwasserkühlung gestützt wird. Vorteilhafterweise erfolgt dabei ein Wärmefluss von heißeren Zonen in bereits abgekühlte Zonen ohne großen Temperatursprung.Further features of the invention provide that in the area of the swamp zone of the Gießstrangquerschnitt supported on its transverse sides without spray water cooling becomes. Advantageously, a heat flow of hotter takes place Zones in already cooled zones without a large temperature jump.
Die gezielte Temperaturführung kann ferner dahingehend vollendet werden, dass der Gießstrang im Zustand weitgehender Durcherstarrung ohne Spritzwasserstrahlen und ohne oberes und seitliches Stützen, auf Stützrollen aufliegend geführt wird.The targeted temperature control can also be completed to that the cast strand in the state of substantial solidification without Spray water jets and without top and side supports, on support rollers is guided on-the-floor.
Die Aufgabe wird weiterhin durch Mittel der Führung und der Kühlung erfindungsgemäß dadurch gelöst, dass der Gießstrang in einzelnen Stützsegmenten gezielt temperaturgeführt ist, derart, dass von Stützsegment zu Stützsegment eine an den Erstarrungszustand des Strangprofils angepasste Sekundärkühlung eingesetzt ist, die aus Spritzwasserstrahlen mit einer Breite gleich oder größer als die Länge von Stützrollenpaaren besteht und an der Längsseite und jeweils an der Querseite des Gießstrangquerschnitts vorgesehen ist und dass die auf das Null-Segment folgenden Stützsegmente offen ausgebildet sind, wobei überschüssiges Spritzwasser in einer Vielzahl von Richtungen vom Gießstrangquerschnitt durch die im Rahmen offenen Stützsegmente ableitbar ist. Dadurch wird über eine prozessgerechte Sekundärkühlung durch gezielte Stützsegmentausbildung mit einer optimalen Anordnung von Strangführungsrollen die Tendenz zur Unterkühlung von Strangecken (Flanschecken) mit schlechtem Duktilitätsverhalten vermieden und damit das Entstehen von Rissen in der Gefügestruktur und an der Oberfläche vermieden. Dabei kann auch eine homogenere Temperaturverteilung im Gießstrangquerschnitt erzielt werden.The task will continue by means of guidance and cooling solved according to the invention in that the cast strand in individual Support segments targeted temperature-controlled, such that of support segment to support segment one to the solidification state of the extruded profile adapted secondary cooling is used, which consists of spray water jets a width equal to or greater than the length of support roller pairs and on the longitudinal side and in each case on the transverse side of the Gießstrangquerschnitts is provided and that following the zero segment Support segments are formed open, with excess water spray in a plurality of directions of Gießstrangquerschnitt through in the Frame open support segments can be derived. This will be over a Process-oriented secondary cooling through targeted support segment formation with an optimal arrangement of strand guide rollers the tendency to Hypothermia of strangles (flank corners) with bad Ductility behavior avoided and thus the emergence of cracks in the Microstructure and surface avoided. It can also be a homogeneous temperature distribution in Gießstrangquerschnitt be achieved.
Durch die temperaturgeführte Kühlung und Stützung in der erfindungsgemäßen Form werden folgende Effekte erzielt:
- minimierte Wasserspritzmenge nur zur Abführung der Erstarrungswärme
- Reduzierung von Laufwasser wegen Unterkühlung der Flanschoberseiten und anderer Querschnittsbereiche
- Homogenes Temperaturbild im BBL-Querschnitt
- Temperaturführung von der Kokille bis in den Richttreiberbereich
- Einstellung von Oberflächentemperaturen im günstigen Duktilitätsbereich
- Minimized water injection quantity only to dissipate the solidification heat
- Reduction of running water due to hypothermia of the flange tops and other cross-sectional areas
- Homogeneous temperature image in BBL cross section
- Temperature control from the mold to the straightener area
- Adjustment of surface temperatures in the favorable ductility range
Die Strangführungssegmente sollen in der Ausbildung den verfahrenstechnischen Anforderungen angepaßt sein. Deshalb erfolgt die Ausbildung in folgender Art:
- Stützrollen, die nur im Sumpfbereich stützen
- Segmentausbildung so, dass die Flanschoberseiten nicht überdeckt werden
- Sicherstellung optimaler Wasserablaufeigenschaften
- Wasserauffang- und Leitbleche an den Segmentoberseiten, so dass möglichst wenig Laufwasser anfällt.
- Support rollers that support only in the sump area
- Segment formation so that the flange tops are not covered
- Ensuring optimal water drainage properties
- Water collecting and baffles on the top of the segment, so that the least possible running water is obtained.
Die Stützung und Sekundärkühlung sind nach weiteren Merkmalen derart gestaltet, dass im Null-Stützsegment Längsseiten des Gießstrangquerschnitts mittels mittensymmetrisch angeordneten längeren Stützrollenpaaren und die Gießstrang-profil-Eckbereiche mittels Tipprollenpaaren kürzerer Länge gestützt sind, und dass die Querseiten des Gießstrangquerschnitts mittels etwa der Seitenlänge entsprechend langen Stützrollenpaaren gestützt sind. Eine derartige Stützung ist z.B. bei Strangschalendicken zwischen 30 und 50 mm vorteilhaft. Die Stützung erfolgt praktisch von allen Seiten nur im Sumpfprofil, um unerwünschte Unterkühlungen zu vermeiden.The support and secondary cooling are designed according to further features such that in the zero support segment longitudinal sides of the Gießstrangquerschnitts by means of symmetrically arranged longer support roller pairs and the Gießstrang profile corner areas supported by Tipprollenpaaren shorter length are, and that the transverse sides of the Gießstrangquerschnitts means of about the Side length correspondingly long support roller pairs are supported. Such Support is e.g. advantageous for strand shell thicknesses between 30 and 50 mm. The support is practically from all sides only in the sump profile to unwanted To avoid hypothermia.
Eine andere Ausgestaltung sieht vor, dass in folgenden Stützsegmenten an den Längsseiten des Gießstrangquerschnitts nur noch die mittensymmetrisch angeordneten, längeren Stützrollenpaare, und an den Querseiten die etwa der Seitenlänge entsprechenden Stützrollenpaare vorgesehen sind. Hier kann die Strangschalendicke schon zwischen 40 bis 60 mm angenommen werden, so dass die Eckbereiche des Gießstrangquerschnitts nicht mehr gestützt werden müssen.Another embodiment provides that in the following support segments to the Longitudinal sides of the Gießstrangquerschnitts only the center symmetrically arranged, longer support roller pairs, and on the transverse sides about the side length corresponding support roller pairs are provided. Here can the Strand shell thickness already assumed between 40 to 60 mm, so that the corner regions of the Gießstrangquerschnitts are no longer supported have to.
Eine weitere Verminderung der Stützkräfte erfolgt nach anderen Merkmalen, indem in einander folgenden Stützsegmenten jeweils die an den Querseiten symmetrisch angeordneten Stützrollenpaare verkürzt sind. Es wird davon ausgegangen, dass Mittenbereiche des Gießstrangs hier schon durcherstarrt sind, und die Strangschale in Außenbereichen ca. 50 bis 70 mm Dicke aufweist.A further reduction of the support forces takes place according to other characteristics, in each of the following support segments on each of the transverse sides symmetrically arranged support roller pairs are shortened. It is assumed, that central areas of the cast strand are already solidified here, and the strand shell in outdoor areas approximately 50 to 70 mm thick.
Bei weiter fortgeschrittener Erstarrung ist vorgesehen, dass in folgenden Stützsegmenten nur noch die an den Querseiten symmetrisch angeordneten, verkürzten Stützrollenpaare vorgesehen sind. Bei Vorprofil-Gießsträngen wird in den Eckbereichen des Gießstrangquerschnitts erfahrungsgemäß schon eine Strangschalendicke von 70 bis 90 mm angenommen.With more advanced solidification is provided that in the following support segments only the symmetrically arranged on the transverse sides, shortened Support roller pairs are provided. For pre-profile casting strands is in the corner regions of the Gießstrangquerschnitts experience already a Strand shell thickness of 70 to 90 mm assumed.
Dabei wird vorgeschlagen, dass der Gießstrang in Abschnitten weitgehender Kernerstarrung nur noch an der Unterseite auf Stützrollen aufliegt.It is proposed that the cast strand in sections more extensive Kernerstarrung rests only on the bottom on support rollers.
Eine Verbesserung sieht vor, dass das Spritzbild der Sekundärkühlung analog zur Gießsumpf-Kernzone ausgelegt ist. Dadurch kann eine zu hohe Wasserbeaufschlagung vermieden werden.An improvement provides that the spray pattern of the secondary cooling analog designed for Gießsumpf core zone. As a result, too high a water supply be avoided.
Dabei ist mit Vorteil vorgesehen, dass überschüssiges Spritzwasser ableitbar ist. Dadurch fallen in der Mitte des Gießstrangs, z.B. auf dem Profilsteg eines Vorprofils, nur noch minimale Wassermengen nach der Strangstützung an.It is provided with advantage that excess spray can be derived is. As a result, fall in the middle of the cast strand, e.g. on the profile web of a Preprofiles, only minimal amounts of water after the strand support on.
Eine weitere Ausgestaltung sieht vor, dass einer langen Stützrolle ein ebenso breiter oder breiterer Spritzwasserstrahl zugeordnet ist. Diese Maßnahme ist insbesondere bei relativ noch dünnen Strangschalen von ca. 30 bis 60 mm anwendbar.Another embodiment provides that a long support role as well wider or wider spray water jet is assigned. This measure is especially applicable for relatively thin strand shells of about 30 to 60 mm.
Und schließlich kann eine Ausgestaltung darin bestehen, dass Tipprollen nur noch in einem Stützsegment , das auf das Null-Stützsegment folgt, vorgesehen sind.And finally, an embodiment may consist in that tapping rolls only still provided in a support segment following the zero support segment are.
In der Zeichnung sind Ausführungsbeipiele der Erfindung dargestellt und werden nachfolgend näher erläutert. In the drawing Ausführungsbeipiele the invention are shown and will explained in more detail below.
Es zeigen:
- Fig. 1
- einen Gießstrang in Seitenansicht mit dem Gießstrangweg zugeordneten Strangschalendicken für einen Vorprofil-Gießstrang,
- Fig. 1 A
- den Gießstrangquerschnitt in der Stranggießkokille,
- Fig. 2A
- den Gießstrangquerschnitt am Ausgang der Stranggießkokille,
- Fig. 2B
- den Gießstrangquerschnitt mit Stützrollenanordnung und Sekundärkühlung im Null-Segment,
- Fig. 2C
- den Gießstrangquerschnitt mit Stützrollenanordnung und Sekundärkühlung in einem nachfolgenden Stützsegment,
- Fig. 2D
- den Gießstrangquerschnitt mit Stützrollenanordnung und Sekundärkühlung in einem weiteren Stützsegment,
- Fig. 2E
- den Gießstrangquerschnitt mit Stützrollenanordnung und Sekundärkühlung im nächsten Stützsegment,
- Fig. 2F
- den Gießstrangquerschnitt vor der Durcherstarrung, ohne Sekundärkühlung,
- Fig. 2G
- den Gießstrangquerschnitt bei nahezu vollzogener Durcherstarrung,
- Fig. 2H
- den Gießstrangquerschnitt nach vollständiger Durcherstarrung auf dem Rollgang aufliegend,
- Fig. 3
- eine perspektivische Ansicht eines Stützsegmentes,
- Fig. 4A
- ein perspektivischer Schnitt durch das Stützsegment mit Tipprollen,
- Fig. 4B
- ein perspektivischer Schnitt durch das Stützsegment ohne Tipprollen,
- Fig. 5
- eine perspektivische Seiten-Ansicht im Querschnitt eines Null-Stützsegmentes in offener Ausbildung und
- Fig. 6
- eine perspektivische Ansicht des Null-Stützsegmentes in offener Ausbildung.
- Fig. 1
- a cast strand in side view with the Gießstrangweg associated strand shell thicknesses for a pre-profile casting strand,
- Fig. 1 A
- the Gießstrangquerschnitt in the continuous casting mold,
- Fig. 2A
- the cast strand cross-section at the outlet of the continuous casting mold,
- Fig. 2B
- the cast strand cross section with support roller arrangement and secondary cooling in the zero segment,
- Fig. 2C
- the Gießstrangquerschnitt with support roller assembly and secondary cooling in a subsequent support segment,
- Fig. 2D
- the Gießstrangquerschnitt with support roller assembly and secondary cooling in another support segment,
- Fig. 2E
- the Gießstrangquerschnitt with support roller assembly and secondary cooling in the next support segment,
- Fig. 2F
- the cast strand cross-section before solidification, without secondary cooling,
- Fig. 2G
- the Gießstrangquerschnitt with almost completed Durcherstarrung,
- Fig. 2H
- the Gießstrangquerschnitt after complete solidification resting on the roller table,
- Fig. 3
- a perspective view of a support segment,
- Fig. 4A
- a perspective section through the support segment with Tipprollen,
- Fig. 4B
- a perspective section through the support segment without Tipprollen,
- Fig. 5
- a side perspective view in cross section of a zero support segment in the open and
- Fig. 6
- a perspective view of the zero support segment in open training.
Als Ausführungsbeispiel ist ein Gießstrang 1 für ein Vorprofil 2, aus dem Träger
gewalzt werden, dargestellt (Fig. 1 und 1A). Der Gießstrang 1 wird nach dem
Verlassen der Stranggießkokille 3 in einem Null-Stützsegment 4 mit einer Sekundärkühlung
und nachfolgend in weiteren Stützsegmenten 5,6 und 7 durch
Spritzwasserstrahlen 8 gekühlt und durch angetriebene Rollen einer Ausziehmaschine
9 ausgezogen.As an exemplary embodiment, a
Im Abstand von 2 m zu 2 m sind die Strangschalendicken mit Dickenangabe in mm angegeben. Die Länge L bezeichnet die gesamte Anlagenlänge von der Stranggießkokille 3 bis zur Ausziehmaschine 9. Außerdem legen die Radien R1, R2 und R3 den Bogen des Strangverlaufs fest.At a distance of 2 m to 2 m are the strand shell thicknesses with thickness information in mm indicated. The length L designates the entire plant length of the Continuous casting mold 3 up to the Ausziehmaschine 9. Also put the radii R1, R2 and R3 fix the arc of the strand course.
Der Gießstrang 1 wird durch eine gezielte Temperaturführung in dem (oberen)
Null-Stützsegment 4 mit Spritzwasserstrahlen 8 beaufschlagt, die eine Breite 10
aufweisen, die gleich oder größer ist als die Länge 11 der Stützrollenpaare 12.
Solche Spritzwasserstrahlen 8 sind an der Längsseite 13 und an der Querseite
14 des Gießstrangquerschnitts 1 a eingesetzt ( Fig. 2A- 2H). Analog zur Strangweglänge
und dem Abkühlungszustand in Kernzonen 15 , die noch zähflüssige
Schmelze in dem Gießstrangquerschnitt 1a enthalten, werden die Querseiten
14 abnehmend gestützt (Fig. 2D - 2F) und die Spritzwasserstrahlen 8 werden
nur noch auf die Kemzonen 15 gerichtet (Fig. 2D).The
Entsprechend einem bestmöglichen Verfahren (Fig. 2A - 2H) tritt der formgetreue,
in der Stranggießkokille 3 erzeugte Gießstrang 1 in das Null-Stützsegment
4 (Fig. 2B) ein, in dem der Gießstrang 1 mittels an der Längsseite
13 im Längsseiten-Mittenbereich 16 angeordnete Stützrollen 17 und an den
Querseiten 14 angeordnete Stützrollen 18 gestützt wird. Dabei werden die
Gießstrang-Profileckbereiche 19 nicht gekühlt, aber mittels Tipprollen 20 gestützt.
Die Spritzwasserstrahlen 8 bilden jeweils gegenüber dem, sich noch im
flüssigen oder zähflüssigen Bereich befindlichen Strang und dessen Strangbreite
oder Strangdicke einen sich in Strömungsrichtung öffnenden Winkel. Dadurch
wird nur dort Wärme in höherem Maße entzogen, wo sich im Inneren des
Gießstranges 1 noch flüssige oder zähflüssige Schmelze befindet, währenddem
bereits erstarrte Bereiche, im wesentlichen die übrige Strangschale 21 verschont
bleibt. Dadurch kommt ein sanfteres Abkühlen der Strangecken zustande
und deshalb entstehen weniger oder keine Oberflächenrisse. Gemäß Fig.
2C werden die Spritzwasserstrahlen 8 noch weit gefächert aufrechterhalten. In
Fig. 2D ist sofort erkennbar, dass nur noch der Mittenbereich 16 des Gießstrangquerschnitts
1a mittels Stützrollen 17 gestützt wird, aber nicht mehr gekühlt
wird. Die Spritzwasserstrahlen 8 sind nur noch auf die Kemzonen 15 gerichtet.
Die Stützrollen 18 sind erheblich kürzer gehalten. Diese gezielte Temperaturführung
setzt sich im Stranglaufweg (Fig. 2E) soweit fort, dass nur noch
Spritzwasserstrahlen 8 an der Längsseite 13 auf die Kemzone 15 gerichtet
werden. Schließlich ist die Kemzone 15 (Fig. 2F) sehr klein, so dass der Gießstrang
1 überhaupt nicht mehr gekühlt werden muss und nur noch mittels der
Stützrollen 18 an den Querseiten 14 geführt wird. In Fig. 2G verkleinern sich die
Kemzonen 15 weiter und der Gießstrang 1 wird nur noch auf den horizontalen
Stützrollen 22 geführt. Gemäß Fig. 2H ist der Gießstrang 1 durcherstarrt. Die
Dicke der Strangschale 21 ist beispielsweise (abhängig von den jeweiligen
Gießquerschnittsabmessungen) jeweils in der Fig. 2B mit 38,2 mm, in der Fig.
2C mit 54,0 mm, in Fig. 2D mit 66,1 mm, in Fig. 2E mit 76,4 mm, in Fig. 2F mit
85,4 mm, in Fig. 2G mit 93,5 mm und in Fig. 2H mit 101,0 mm angegeben.According to the best possible method (FIGS. 2A-2H), the form-true,
cast
In Fig. 3 ist eines der Stützsegmente 5,6,7 dargestellt. Danach sind wesentliche
Baugruppen jeweils ein Oberrahmen 23, ein Unterrahmen 24, Seitenrahmen
25, Ausbaurollen 26 und Spritzlatten 27.In Fig. 3 one of the
Die Fig. 4A und 4B zeigen den in den Pfeilrichtungen 28 verlaufenden jeweiligen
Abfluss des Spritzwassers 29. Der Abfluss wird insbesondere durch eine
"offene" Gestaltung der Stützsegmente 5,6,7, ermöglicht, wobei der Gießstrangquerschnitt
1a ausgehend von einem offenen Rahmen jeweils von äußeren
Rippen 30, Verstärkungen 31, inneren Rippen 32 und jeweils einem Düsenstock
33 an vier Seiten umgeben ist. FIGS. 4A and 4B show the respective ones extending in the directions of the
Dabei entspricht die Darstellung der Fig. 4A etwa der Strangweglänge in den Fig. 2B und 2C. Die Darstellung der Fig. 4B entspricht der Strangweglänge der Fig. 2D.The representation of FIG. 4A corresponds approximately to the strand path length in FIG Figs. 2B and 2C. The representation of FIG. 4B corresponds to the strand path length of FIG Fig. 2D.
Fig. 5 zeigt einen senkrechten Schnitt durch das in Betriebslage gezeichnete
Stützsegment 5,6,7, wobei die offene Ausbildung eines Stützsegmentes 5, 6, 7
besonders leicht erkennbar ist. Das aus den Düsenstöcken 33 durch die
Spritzwasserstrahlen 8 gegen den Gießstrangquerschnitt 1a gerichtete Spritzwasser
29 kann leicht zwischen den Verstärkungen 31 ringsum abfließen.Fig. 5 shows a vertical section through the drawn in operating
Gemäß Fig. 6 ist ein Stützrollengerüst 5,6,7 in der zu Fig. 3 beschriebenen
Ausbildung in Betriebsstellung in Ansicht gezeichnet. Referring to FIG. 6, a
- 11
- Gießstrangcast strand
- 1a1a
- GießstrangquerschnittGießstrangquerschnitt
- 22
- Vorprofil (Strangprofil)Preprofile (extruded profile)
- 33
- Stranggießkokillecontinuous casting
- 44
- Null-StützsegmentZero support segment
- 55
- Stützsegmentsupporting segment
- 66
- Stützsegmentsupporting segment
- 77
- Stützsegmentsupporting segment
- 88th
- Spritzwasserstrahlsplash-ray
- 99
- AusziehmaschineAusziehmaschine
- 1010
- Breite (des Spritzwasserstrahls)Width (of spray water jet)
- 1111
- Längelength
- 1212
- StützrollenpaareSupport roller pairs
- 1313
- Längsseite (des Gießstrangs)Longitudinal side (of the casting strand)
- 1414
- Querseite (des Gießstrangs)Transverse side of the casting strand
- 1515
- Kemzonecore zone
- 1616
- Längsseiten-MittenbereichLongitudinal side center region
- 1717
- Stützrollesupporting role
- 1818
- Stützrollesupporting role
- 1919
- Gießstrang-ProfileckbereichCast strand-profile corner area
- 2020
- TipprolleTip role
- 2121
- Strangschalestrand shell
- 2222
- horizontale Stützrollehorizontal support roller
- 2323
- Oberrahmentop frame
- 2424
- Unterrahmensubframe
- 2525
- Seitenrahmenside frame
- 2626
- AusbaurollenConstruction roles
- 2727
- Spritzlattespray bar
- 2828
- Pfeilrichtungarrow
- 2929
- Spritzwassersplash
- 3030
- äußere Rippenouter ribs
- 3131
- Verstärkungreinforcement
- 3232
- innere Rippeninner ribs
- 3333
- Düsenstocknozzle
Claims (15)
- Method of supporting, guiding and cooling cast strips of steel, particularly of preliminary sections for girders, in which the cast strip after leaving the continuous casting mould is cooled and drawn out in a zero segment in a secondary cooling and in subsequent support segments again by spray water, characterised in that for avoidance of an undesired hardening structure on the flange upper edges or in other cross-sectional regions the cooling and supporting of the beam blank format is adapted to the hardening regions in such a manner that there is cooling and supporting only in regions in which liquid phase formation is present.
- Method according to claim 1, characterised in that the cast strip is cooled by selective temperature guidance in upper support segments by widths, which correspond at least with the length of the support rollers, of the spray water jets at longitudinal and transverse sides of the cast strip cross-section and supported to decreasing extent analogously to the strip path length and to the state of cooling in core zones of the cast strip cross-section at transverse sides thereof and cooled only still by spray water jets, which are directed towards the liquid core zones, with the same width as or smaller width than the liquid phase side.
- Method according to claim 1 or 2, characterised in that the cast strip is supported by selective temperature guidance in the zero support segment at the section ends and in the longitudinal side centre region of its cross-section and at its transverse sides, and the longitudinal and transverse sides, excluding the section corner regions, are cooled, that in the case of strip skin formation progressing on the strip path only still the centre region and the two transverse sides of the strip cross-section are supported, and that in the region of the liquid phase ends of the core zones the transverse sides are supported and cooled to limited extent in the region thereof, and only spray water jets directed towards the liquid phase zone are still used at the longitudinal sides.
- Method according to one or more of claims 1 to 3, characterised in that the cast strip cross-section is supported in the region of the liquid phase zone at the transverse sides thereof again without spray water cooling.
- Method according to one of claims 1 to 4, characterised in that the cast strip in the state of extensive hardening through is guided without spray water jets and lying on support rollers without upper and lateral support.
- Strip guide for cast strips (1) of steel, particularly for preliminary sections (2) for girders, comprising a zero support segment (4) adjoining the continuous casting mould (3) and a secondary cooling with spray water jets (8) as well as successive further support segments (5 to 7) and a drawing-out machine (9), characterised in that the cast strip (1) is selectively guided in terms of temperature in individual support segments (4, 5, 6, 7) in such a manner that from support segment (4) to support segment (7) there is used a secondary cooling which is adapted to the state of hardening of the strip section (2) and consists of spray water jets (8) with a width (10) the same as or larger than the length (11) of support roller pairs (12) and which is provided at the longitudinal side (13) and each time at the transverse side (14) of the cast strip cross-section (1a) and that the support segments (5 to 7) following the zero segment (4) are constructed to be open, wherein excess spray water (29) can be conducted away in a plurality of directions (28) from the cast strip cross-section (1a) by the support segments (5 to 7) open in the frame.
- Strip guide according to claim 6, characterised in that, in the zero support segment (4), longitudinal sides (13) of the cast strip cross-section (1a) are supported by means of longer support roller pairs (17) arranged to be symmetrical with respect to the centre, and cast strip section comer regions (19) are supported by means of tipping roller pairs (20), and that the transverse sides (14) of the cast strip cross-section (1a) are supported by means of support rollers (18) approximately corresponding in length with the side length.
- Strip guide according to one of claims 6 and 7, characterised in that in following support segments (5, 6, 7) only longer support roller pairs (17), which are arranged centrally, are still provided at the longitudinal sides (13) of the cast strip cross-section (1a) and support roller pairs (18), which approximately correspond in length with the side length, are provided at the transverse sides (14) of the cast strip cross-section.
- Strip guide according to one of claims 6 to 8, characterised in that in following support segments (5, 6, 7) support roller pairs (18) respectively arranged at the transverse sides (14) are shortened.
- Strip guide according to one of claims 6 to 9, characterised in that in following support segments (5, 6, 7) only symmetrically shortened support roller pairs (18) are still provided at transverse sides (14).
- Strip guide according to one of claims 6 to 10, characterised in that the cast strip (1) in portions of extensive core hardening only still rests at its underside on support rollers (22).
- Strip guide according to one of claims 6 to 11, characterised in that the spray pattern of the secondary cooling is designed analogously to the cast liquid phase core zone (15).
- Strip guide according to one of claims 6 to 12, characterised in that excess spray water (29) can be conducted away.
- Strip guide according to one of claims 6 to 13, characterised in that a long support roller (17; 18) is respectively associated with a spray water jet (8) which is just as wide or is wider.
- Strip guide according to one of claims 6 to 14, characterised in that tipping rollers (20) are only still provided in a support segment (5) which follows the zero support segment (4).
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10039033 | 2000-08-10 | ||
DE10039033 | 2000-08-10 | ||
DE10133093 | 2001-07-11 | ||
DE10133093A DE10133093A1 (en) | 2000-08-10 | 2001-07-11 | Process and strand guide for supporting, guiding and cooling cast strands made of steel, in particular of pre-profiles for beams |
PCT/EP2001/009092 WO2002011923A1 (en) | 2000-08-10 | 2001-08-07 | Method and strand guide for supporting, guiding and cooling casting strands made of steel, especially preliminary sections for girders |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1307305A1 EP1307305A1 (en) | 2003-05-07 |
EP1307305B1 true EP1307305B1 (en) | 2005-02-02 |
Family
ID=26006651
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP01965178A Expired - Lifetime EP1307305B1 (en) | 2000-08-10 | 2001-08-07 | Method and strand guide for supporting, guiding and cooling casting strands made of steel, especially preliminary sections for girders |
Country Status (8)
Country | Link |
---|---|
EP (1) | EP1307305B1 (en) |
JP (1) | JP2004505775A (en) |
CN (1) | CN1241700C (en) |
AT (1) | ATE288332T1 (en) |
AU (1) | AU2001285877A1 (en) |
CA (1) | CA2419069C (en) |
ES (1) | ES2236296T3 (en) |
WO (1) | WO2002011923A1 (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1400003B1 (en) * | 2010-05-18 | 2013-05-09 | Danieli Off Mecc | CONTINUOUS CASTING DEVICE AND ITS PROCEDURE |
EP2404686A1 (en) * | 2010-07-09 | 2012-01-11 | Siemens VAI Metals Technologies GmbH | Roller holder for a line guide segment of a strand casting machine |
IT201700034742A1 (en) | 2017-03-29 | 2018-09-29 | Danieli Off Mecc | APPARATUS FOR CONTINUOUS CASTING AND ITS PROCEDURE |
IT201700067508A1 (en) * | 2017-06-16 | 2018-12-16 | Danieli Off Mecc | CONTINUOUS CASTING METHOD AND ITS APPARATUS |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5639158A (en) * | 1979-09-04 | 1981-04-14 | Kawasaki Steel Corp | Continuous casting device for beam blank |
JPS56128652A (en) * | 1980-03-12 | 1981-10-08 | Nippon Steel Corp | Holding roll for beam blank |
JPS57199555A (en) * | 1981-06-03 | 1982-12-07 | Kawasaki Steel Corp | Roll stand for continuous casting machine for beam blank |
JPH04200844A (en) * | 1990-06-25 | 1992-07-21 | Nkk Corp | Cooling method for continuously casting steel beam blank |
JP2856660B2 (en) * | 1993-12-13 | 1999-02-10 | 日立造船株式会社 | Slab support equipment for continuous casting equipment for near-net beam blanks |
JPH09174210A (en) * | 1995-12-27 | 1997-07-08 | Kawasaki Steel Corp | Method for continuously casting high mo steel |
-
2001
- 2001-08-07 AU AU2001285877A patent/AU2001285877A1/en not_active Abandoned
- 2001-08-07 AT AT01965178T patent/ATE288332T1/en active
- 2001-08-07 WO PCT/EP2001/009092 patent/WO2002011923A1/en active IP Right Grant
- 2001-08-07 EP EP01965178A patent/EP1307305B1/en not_active Expired - Lifetime
- 2001-08-07 CN CN01813959.0A patent/CN1241700C/en not_active Expired - Fee Related
- 2001-08-07 ES ES01965178T patent/ES2236296T3/en not_active Expired - Lifetime
- 2001-08-07 CA CA002419069A patent/CA2419069C/en not_active Expired - Fee Related
- 2001-08-07 JP JP2002517246A patent/JP2004505775A/en active Pending
Also Published As
Publication number | Publication date |
---|---|
CN1446132A (en) | 2003-10-01 |
ES2236296T3 (en) | 2005-07-16 |
JP2004505775A (en) | 2004-02-26 |
CN1241700C (en) | 2006-02-15 |
CA2419069C (en) | 2009-01-20 |
CA2419069A1 (en) | 2003-02-05 |
AU2001285877A1 (en) | 2002-02-18 |
WO2002011923A1 (en) | 2002-02-14 |
EP1307305A1 (en) | 2003-05-07 |
ATE288332T1 (en) | 2005-02-15 |
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