EP1277564A2 - Method of compacting powder materials - Google Patents
Method of compacting powder materials Download PDFInfo
- Publication number
- EP1277564A2 EP1277564A2 EP02015132A EP02015132A EP1277564A2 EP 1277564 A2 EP1277564 A2 EP 1277564A2 EP 02015132 A EP02015132 A EP 02015132A EP 02015132 A EP02015132 A EP 02015132A EP 1277564 A2 EP1277564 A2 EP 1277564A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- deformation
- die plate
- pressing
- forces
- punches
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B11/00—Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
- B30B11/005—Control arrangements
Definitions
- a common way to press powder material is to Form space in a so-called die plate and using a Upper and one lower stamp to produce the compact. Usually the Lower punch inserted into a predetermined position in the die hole, after which the filling with powder material takes place. Then with the help of Upper stamp of the compact shaped. With the help of such a method e.g. Pressed metal powder for the production of molded parts by the sintering process.
- the aim is to make the compact relatively precise if possible shape in terms of its geometric dimensions and density, so that the desired dimensional accuracy is achieved later after the sintering process.
- the invention has for its object a method for pressing To create powder material with which a compact is reproducibly manufactured can be while protecting the pressing device against unwanted Damage due to insufficient deformation of the die plate.
- the invention is based on the fact that the bending force acting on the die plate arises from the difference between the press forces of the upper and lower punches.
- the inventive method is a curve or a table for the dependency the deformation of the die plate from the applied pressing forces.
- the delivery routes of the press rams is also essential to know which misalignments of the die hole change with different deformations to adjust. Therefore, in the method according to the invention during the Pressing process from time to time or continuously the pressing force to the Stamps measured to determine the respective deformation.
- To a specific one Deformation value of the die plate includes a predetermined delivery path for the Ram. It is therefore possible using the method according to the invention during the pressing process the length of the delivery path according to the described Correct measurements. With the help of the invention it is therefore achieved that the upper punch is moved precisely to the edge of the die hole, but without touching them significantly.
- a pressing device 10 shown in Figure 1 has a die plate 12, with a die hole 14 with which an upper punch 16 and a lower punch 18th interact.
- the power devices that operate the punches 16, 18 are not shown. They are conventional and e.g. hydraulic acting. It is with Such pressing devices possible to position the ram in the ⁇ m range. Is between the force devices, not shown, and the punches 16, 18 one load cell 20 or 22 is arranged.
- the die plate 12 rests complaints 24, 26
- the actual shape space of the die bore 14 is in cross section conical or trapezoidal with two inclined surfaces 26. If a circular one Form space is present, there is naturally only a conical surface.
- the molding space which can be seen in Figure 1 serves e.g. for the production of a compact Metal powder material for the production of an indexable insert after the sintering process, e.g. for milling or drilling tools or the like.
- Both ram 16, 18 move into the bore 14, with the upper ram moving towards the edge 28 is and thus specifies the bearing of the top of the compact, during the Lower punch is brought up to the edge 30 in order to specify the thickness of the compact.
- the lower punch 18 first becomes one Filling position advanced. Then it is filled with powder material. Then the upper punch 16 is actuated and moved up to the edge 28, to deform the compact by pressing. At the same time we have the lower stamp 18 driven to the edge 30.
- the method of the pressing device is shown in the block diagram from FIG 10 clearly shown in Figure 1.
- the function is tabulated in a computer 30 stored between the deformation force on the die plate 12 and thereby induced deformation. More specifically, is the displacement of the die hole or the edge 28 deposited relative to the deformation force.
- the investigation this relationship can be done with the help of suitable measurements or calculations, before production starts.
- the powder material to be pressed is known and also the density required for the compact.
- the deformation can be in the case of the individual deformation forces, which is the difference between the pressing forces the stamp 16, 18 are formed, determine.
- the computer If the value of the pressing forces is too low, the computer generates 30 a shutdown signal for the press device 10. This will damage avoided by stamp and die plate.
Abstract
Description
Die Erfindung bezieht sich auf ein Verfahren zum Verpressen vom Pulvermaterial nach dem Patentanspruch 1.The invention relates to a method for pressing the powder material according to claim 1.
Eine übliche Verfahrensweise, Pulvermaterial zu verpressen besteht darin, den Formraum in einer sogenannten Matrizenplatte auszubilden und mit Hilfe eines Ober- und eines Unterstempels den Preßling herzustellen. Üblicherweise wird der Unterstempel in eine vorgegebene Position in die Matrizenbohrung eingefahren, wonach die Befüllung mit Pulvermaterial erfolgt. Anschließend wird mit Hilfe des Oberstempels der Preßling geformt. Mit Hilfe eines derartigen Verfahrens wird z.B. Metallpulver für die Herstellung von Formteilen nach dem Sinterverfahren verpresst. Dabei wird angestrebt, den Preßling nach Möglichkeit schon relativ präzise im Hinblick auf seine geometrischen Abmessungen und seine Dichte zu formen, so daß später nach dem Sinterprozeß die gewünschte Maßhaltigkeit erreicht wird.A common way to press powder material is to Form space in a so-called die plate and using a Upper and one lower stamp to produce the compact. Usually the Lower punch inserted into a predetermined position in the die hole, after which the filling with powder material takes place. Then with the help of Upper stamp of the compact shaped. With the help of such a method e.g. Pressed metal powder for the production of molded parts by the sintering process. The aim is to make the compact relatively precise if possible shape in terms of its geometric dimensions and density, so that the desired dimensional accuracy is achieved later after the sintering process.
Weist der Preßling eine geometrische Form auf, bei der eine Schrägfläche an der Außenseite vorgesehen ist, wie das z.B. bei Schneidplatten von Fräs- und Bohrwerkzeugen der Fall ist, dann wird während des Preßvorgangs eine nicht unerhebliche Verformungskraft auf die Matrizenplatte ausgeübt. Die Verformungskraft führt zur Verformung der Matrizenplatte durch Biegung und Stauchung. Die dadurch hervorgerufene Biegung der Matrizenplatte kann über eine geschickte Wahl der Auflageflächen und der Matrizenplattenquerschnitte verringert, aber nicht eliminiert werden.If the compact has a geometric shape with an inclined surface on the Outside is provided, such as for cutting inserts of milling and drilling tools is the case, then becomes a not inconsiderable during the pressing process Deformation force exerted on the die plate. The deformation force leads for deforming the die plate through bending and compression. The resulting Bending the die plate can be done by a skillful choice of the contact surfaces and the die plate cross sections reduced, but not eliminated become.
Bei dem beschriebenen Preßverfahren darf die Verformung der Matrizenplatte nicht außer acht gelassen werden. Es ist erforderlich, daß der Oberstempel die Kante am Übergang der Formflächen präzise anfährt. Wird der Oberstempel nicht an diesem Punkt angehalten, kommt es zu einer Beschädigung von Stempel und Matrize. Wird der Stempel hingegen zu früh angehalten, fehlt es an der Maßhaltigkeit.In the pressing process described, the deformation of the die plate must not be disregarded. It is necessary that the upper punch the edge on Precise transition to the mold surfaces. If the upper stamp is not on this If the point is stopped, the stamp and die will be damaged. Becomes if the stamp is stopped too early, the dimensional accuracy is missing.
Es ist bekannt, durch Versuche oder rechnerisch zu ermitteln, um welchen Betrag eine Matrizenplatte bei einem bestimmten Preßprozeß verformt wird, um den Verstellweg des Oberstempels entsprechend vorzugeben. Normalerweise erfolgt dies dadurch, daß am Preßling festgestellt wird, ob der Preßstempel die vorgegebene Strecke zurückgelegt hat oder nicht. Ein derartiges Verfahren ist relativ aufwendig und schützt die Preßvorrichtung nicht vor Beschädigungen. Kommt es aufgrund unzureichender Befüllung zu relativ kleinen Preßkräften, entfällt die Verformung der Matrizenplatte oder erreicht deutlich kleinere Werte, so daß die Positionierung des Preßstempel zwangsläufig zur Folge hat, daß der Oberstempel gegen die Kante der Matrizenbohrung anfährt.It is known to determine by experiment or by calculation what amount a die plate is deformed in a certain pressing process by the adjustment path of the upper stamp accordingly. Usually this is done in that it is determined on the compact whether the press ram is the predetermined one Traveled or not. Such a method is relatively complex and does not protect the press device from damage. It comes about insufficient filling to relatively small press forces, the deformation is eliminated the die plate or reaches significantly smaller values so that the positioning of the ram inevitably has the consequence that the upper ram against the edge the die hole starts.
Der Erfindung liegt die Aufgabe zugrunde, ein Verfahren zum Verpressen von Pulvermaterial zu schaffen, mit dem ein Preßling reproduzierbar präzise hergestellt werden kann bei gleichzeitigem Schutz der Preßvorrichtung gegen ungewollte Beschädigungen aufgrund unzureichender Verformung der Matrizenplatte.The invention has for its object a method for pressing To create powder material with which a compact is reproducibly manufactured can be while protecting the pressing device against unwanted Damage due to insufficient deformation of the die plate.
Diese Aufgabe wird durch die Merkmale des Anspruchs 1 gelöst.This object is solved by the features of claim 1.
Die Erfindung geht davon aus, daß die auf die Matrizenplatte wirkende Biegekraft sich aus der Differenz der Preßkräfte von Ober- und Unterstempel ergibt. Beim erfindungsgemäßen Verfahren wird eine Kurve oder eine Tabelle für die Abhängigkeit der Verformung der Matrizenplatte von den aufgebrachten Preßkräften. Für die Einstellung der Zustellwege der Preßstempel ist außerdem wesentlich zu wissen, welche Verlagerungen der Matrizenbohrung sich bei unterschiedlichen Verformungen einstellen. Daher wird bei dem erfindungsgemäßen Verfahren während des Preßvorgangs von Zeit zu Zeit oder auch kontinuierlich die Preßkraft an den Stempeln gemessen zur Ermittlung der jeweiligen Verformung. Zu einem bestimmten Verformungswert der Matrizenplatte gehört ein vorgegebener Zustellweg für die Preßstempel. Es ist daher möglich, mit Hilfe des erfindungsgemäßen Verfahrens während des Preßvorgangs die Länge des Zustellweges nach Maßgabe der beschriebenen Messungen zu korrigieren. Mit Hilfe der Erfindung wird daher erreicht, daß der Oberstempel präzise an die Kante der Matrizenbohrung herangefahren wird, ohne sie jedoch signifikant zu berühren.The invention is based on the fact that the bending force acting on the die plate arises from the difference between the press forces of the upper and lower punches. At the The inventive method is a curve or a table for the dependency the deformation of the die plate from the applied pressing forces. For the Setting the delivery routes of the press rams is also essential to know which misalignments of the die hole change with different deformations to adjust. Therefore, in the method according to the invention during the Pressing process from time to time or continuously the pressing force to the Stamps measured to determine the respective deformation. To a specific one Deformation value of the die plate includes a predetermined delivery path for the Ram. It is therefore possible using the method according to the invention during the pressing process the length of the delivery path according to the described Correct measurements. With the help of the invention it is therefore achieved that the upper punch is moved precisely to the edge of the die hole, but without touching them significantly.
Bei einer Verformung der Matrizenplatte kommt es naturgemäß auch zu einer Relativverlagerung von Unterstempel und Matrizenbohrung. Es ist daher erforderlich, bei der beschriebenen Korrektur des Zustellwegs des Oberstempels den Zustellwegs des Unterstempels parallel zu korrigieren.If the die plate is deformed, there is of course also a relative displacement of lower punch and die hole. It is therefore necessary to the described correction of the delivery path of the upper stamp the delivery path of the Correct lower stamp in parallel.
Mit Hilfe des erfindungsgemäßen Verfahrens kann vermieden werden, daß der Oberstempel gegen eine Kante der Matrizenbohrung anfährt, wenn es zu keiner Verformung der Matrizenplatte kommt. Da, wie erwähnt, ständig die Preßkraft gemessen wird, diese jedoch auch bestimmte Werte unterschreiten kann, kann auf diese Weise ermittelt werden, wann die gesamte Preßvorrichtung still zu setzen ist, damit eine Beschädigung von Oberstempel und Matrizenbohrung vermieden wird.With the help of the method according to the invention can be avoided that the Upper punch hits against an edge of the die hole if there is no deformation the die plate comes. Since, as mentioned, the pressing force is constantly measured is, but this can also fall below certain values, can on this Way are determined when the entire pressing device is to be shut down, so Damage to the upper punch and die hole is avoided.
Bei dem beschriebenen Preßvorgang kommt es nicht nur zu einer Verformung der Matrizenplatte, sondern auch zu einer Stauchverformung von Ober- und Unterstempel. Die Verformungswerte sind ebenso wie die Verformung der Matrizenplatte relativ klein, aber nicht vernachlässigbar. So wird z.B. bei einer Matrizenplatte eine Verformung von einigen µm pro Tonne Preßkraft erhalten. Um bei einer nicht zu vernachlässigenden Stauchung der Preßstempel ebenfalls eine Korrektur vorzunehmen, sieht eine Ausgestaltung der Erfindung vor, daß für eine Reihe von unterschiedlichen Preßkräften an den Stempeln deren Stauchverformung gemessen oder berechnet wird. Die korrelierenden Werte von Stauchverformung und Preßkräften werden tabellarisch in einem Speicher abgelegt. Die Zustellung von Ober- und Unterstempel wird dann nach Maßgabe der Stauchung korrigiert.In the pressing process described, there is not only a deformation of the Die plate, but also for upsetting the upper and lower punches. The deformation values are just like the deformation of the die plate relatively small, but not negligible. For example, for a die plate one Deformation of a few microns per ton of pressing force. In order not to one neglecting compression of the ram also to make a correction, provides an embodiment of the invention that for a number of different Pressing forces on the punches measured their compression deformation or is calculated. The correlating values of compression set and compression forces are stored in a table in a memory. The delivery of top and The lower stamp is then corrected in accordance with the compression.
Ein Ausführungsbeispiel der Erfindung wird nachfolgend anhand von Zeichnungen näher erläutert.
- Fig. 1
- zeigt schematisch eine Preßvorrichtung nach der Erfindung.
- Fig. 2
- zeigt anhand eine Blockschaltbildes den Betrieb der Preßvorrichtung nach Fig. 1.
- Fig. 1
- shows schematically a pressing device according to the invention.
- Fig. 2
- shows the operation of the pressing device according to FIG. 1 on the basis of a block diagram.
Eine in Figur 1 dargestellte Preßvorrichtung 10 weist eine Matrizenplatte 12 auf, mit
einer Matrizenbohrung 14, mit der ein Oberstempel 16 und ein Unterstempel 18
zusammenwirken. Die Kraftvorrichtungen, die die Stempel 16, 18 betätigen, sind
nicht dargestellt. Sie sind herkömmlich und z.B. hydraulisch wirkend. Es ist mit
derartigen Preßvorrichtungen möglich, die Preßtempel im µm-Bereich zu positionieren.
Zwischen den nicht gezeigten Kraftvorrichtungen und den Stempeln 16, 18 ist
jeweils eine Kraftmeßdose 20 bzw. 22 angeordnet. Die Matrizenplatte 12 ruht auf
beanstandeten Auflagern 24, 26.A
Wie zu erkennen, ist der eigentliche Formraum der Matrizenbohrung 14 im Querschnitt
konisch bzw. trapezförmig mit zwei Schrägflächen 26. Falls ein kreisrunder
Formraum vorliegt, ist naturgemäß nur eine konische Fläche vorhanden. Der Formraum,
der in Figur 1 zu erkennen ist, dient z.B. zur Herstellung eines Preßlings aus
Metallpulvermaterial zur Herstellung einer Wendeschneidplatte nach dem Sinterverfahren,
z.B. für Fräs- oder Bohrwerkzeuge oder dergleichen. Beide Preßstempel 16,
18 fahren in die Bohrung 14 ein, wobei der obere Preßstempel an die Kante 28 heranzufahren
ist und damit die Lager der Oberseite des Preßlings vorgibt, während der
Unterstempel an die Kante 30 heranzufahren ist, um die Dicke des Preßlings vorzugeben.
Während des Preßprozesses wird zunächst der Unterstempel 18 zu einer
Befüllposition vorgefahren. Dann erfolgt eine Befüllung mit Pulvermaterial.
Anschließend wird der Oberstempel 16 betätigt und bis an die Kante 28 herangefahren,
um den Preßling durch Pressen zu verformen. Zugleich wir der Unterstempel
18 bis zur Kante 30 gefahren.As can be seen, the actual shape space of the
Aufgrund der unterschiedlich zu verpressenden Querschnitte von Ober- und Unterstempel
16, 18 wird ein Differenzdruck auf die Matrizenplatte 12 aufgebracht, und
die Matrizenplatte wird zwischen den Auflagern 24, 26 durchgebogen und
gestaucht, wie deutlich und übertrieben in Figur 1 zu erkennen. Diese Verformung
der Matrizenplatte 12 bedingt nun, daß der Oberstempel 16 weiter in der Matrizenbohrung
14 hineingefahren werden muß als bei unverformter Matrizenplatte 12, um
die Kante 28 zu erreichen. Dieser Verstellweg ist abhängig von der jeweiligen Verformung
der Matrizenplatte 12, die wiederum von der Differenzkraft an der Matrizenplatte
abhängt.Due to the different cross-sections of the upper and
Aus den Blockschaltbild aus Figur 2 geht die Verfahrensweise der Preßvorrichtung
10 nach Figur 1 deutlich hervor. In einem Rechner 30 ist tabellarisch die Funktion
abgelegt zwischen der Verformungskraft an der Matrizenplatte 12 und der dadurch
hervorgerufenen Verformung. Genauer gesagt, ist die Verlagerung der Matrizenbohrung
bzw. der Kante 28 relativ zur Verformungskraft abgelegt. Die Ermittlung
dieser Beziehung kann mit Hilfe geeigneter Messungen oder Berechnungen geschehen,
bevor die Produktion beginnt. Das zu verpressende Pulvermaterial ist bekannt
und auch die Dichte, die für den Preßling gefordert ist. Mithin läßt sich die Verformung
bei den einzelnen Verformungskräften, die aus der Differenz der Preßkräfte
der Stempel 16, 18 gebildet werden, ermitteln.The method of the pressing device is shown in the block diagram from FIG
10 clearly shown in Figure 1. The function is tabulated in a
Während des Preßvorgangs werden ständig oder intermittierend mit Hilfe der
Kraftmeßdosen 20, 22 die an den Preßstempeln 16, 18 wirkenden Preßkräfte gemessen
und aus Ihnen die Verformungskraft berechnet. Im Rechner 30 wird die dazugehörige
Verformung der Matrizenplatte 12 ermittelt bzw. die Verlagerung der
Kante 28 der Matrizenplatte 12. Der Rechner 30 übermittelt daraus den Zustellweg
des Preßstempels 16 und gibt auf eine Steuervorrichtung 32 ein entsprechendes
Positioniersignal für Kraftglieder 34 bzw. 36 für die Preßstempel 16, 18. Auf diese
Weise ist es möglich, unabhängig von der Verformung der Matrizenplatte 12 mit
dem Oberstempel 16 exakt die Kante 28 und dem Unterstempel 18 die Kante 30
anzufahren. Denn bei einer Verformung der Matrizenplatte 12 findet auch eine
Relativverlagerung von Unterstempel 18 und Matrizenplatte 12 statt, und der Unterstempel
18 ist vom Kraftglied 16 entsprechend zu positionieren, damit er an der
Kante 30 verbleibt.During the pressing process, are continuously or intermittently with the help of
Falls bei der Messung der Preßkräfte ein zu geringer Wert auftritt, erzeugt der Rechner
30 ein Abschaltsignal für die Preßvorrichtung 10. Dadurch wird eine Beschädigung
von Stempel und Matrizenplatte vermieden.If the value of the pressing forces is too low, the computer generates
30 a shutdown signal for the
Claims (4)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10135283 | 2001-07-19 | ||
DE10135283A DE10135283C2 (en) | 2001-07-19 | 2001-07-19 | Process for pressing powder material |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1277564A2 true EP1277564A2 (en) | 2003-01-22 |
EP1277564A3 EP1277564A3 (en) | 2004-01-28 |
EP1277564B1 EP1277564B1 (en) | 2006-09-13 |
Family
ID=7692423
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP02015132A Expired - Lifetime EP1277564B1 (en) | 2001-07-19 | 2002-07-06 | Method of compacting powder materials |
Country Status (4)
Country | Link |
---|---|
US (1) | US6827889B2 (en) |
EP (1) | EP1277564B1 (en) |
AT (1) | ATE339298T1 (en) |
DE (2) | DE10135283C2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103718259A (en) * | 2011-07-27 | 2014-04-09 | 住友电气工业株式会社 | Compressed powder compact |
CN115093199A (en) * | 2022-06-30 | 2022-09-23 | 蒋波 | Special refractory crucible for negative electrode material carbonization and manufacturing process thereof |
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US7708702B2 (en) * | 2006-01-26 | 2010-05-04 | Roche Diagnostics Operations, Inc. | Stack magazine system |
DE102008035301B3 (en) * | 2008-07-29 | 2010-03-25 | Fette Gmbh | powder Press |
DE102013201312A1 (en) * | 2013-01-28 | 2014-07-31 | Robert Bosch Gmbh | Core for inductor, has two parallel legs which are connected by yoke, and are arranged facing bottom portion and facing away from top portion |
EP4034375A1 (en) | 2019-09-27 | 2022-08-03 | Korsch AG | Device and method for monitoring a tablet press machine, preferably during continuous operation, by means of a measuring device attached to a press punch |
CN113619177B (en) * | 2021-07-07 | 2023-06-30 | 浙江明恩新材料科技有限公司 | Production equipment of high-temperature-resistant modified material product |
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DE2951716A1 (en) * | 1979-12-19 | 1981-07-02 | Mannesmann AG, 4000 Düsseldorf | Pressing system to compensate for fluctuations - measures displacement of powder in mould simultaneously with pressure |
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EP1048450A2 (en) * | 1999-04-30 | 2000-11-02 | Wilhelm Fette GmbH | Method to determine the position of a plunger in a powder press |
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DE3520203A1 (en) * | 1985-06-05 | 1986-12-11 | Wilhelm Fette Gmbh, 2053 Schwarzenbek | ROTARY ROTARY TABLETING MACHINE AND METHOD FOR CONTROLLING YOUR PRINT ROLLERS |
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DE10010671C2 (en) * | 2000-03-04 | 2002-03-14 | Fette Wilhelm Gmbh | Process for producing pressed parts by pressing metal powder and then sintering the compact |
-
2001
- 2001-07-19 DE DE10135283A patent/DE10135283C2/en not_active Expired - Fee Related
-
2002
- 2002-07-06 AT AT02015132T patent/ATE339298T1/en active
- 2002-07-06 DE DE50208114T patent/DE50208114D1/en not_active Expired - Lifetime
- 2002-07-06 EP EP02015132A patent/EP1277564B1/en not_active Expired - Lifetime
- 2002-07-13 US US10/194,581 patent/US6827889B2/en not_active Expired - Lifetime
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103718259A (en) * | 2011-07-27 | 2014-04-09 | 住友电气工业株式会社 | Compressed powder compact |
US9251946B2 (en) | 2011-07-27 | 2016-02-02 | Sumitomo Electric Industries, Ltd. | Compact |
CN103718259B (en) * | 2011-07-27 | 2016-04-13 | 住友电气工业株式会社 | Press-powder formed body |
CN115093199A (en) * | 2022-06-30 | 2022-09-23 | 蒋波 | Special refractory crucible for negative electrode material carbonization and manufacturing process thereof |
CN115093199B (en) * | 2022-06-30 | 2023-12-22 | 青海天蓝新能源材料有限公司 | Special refractory crucible for carbonization of negative electrode material and manufacturing process thereof |
Also Published As
Publication number | Publication date |
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EP1277564B1 (en) | 2006-09-13 |
US20030024418A1 (en) | 2003-02-06 |
US6827889B2 (en) | 2004-12-07 |
ATE339298T1 (en) | 2006-10-15 |
DE50208114D1 (en) | 2006-10-26 |
DE10135283C2 (en) | 2003-09-18 |
EP1277564A3 (en) | 2004-01-28 |
DE10135283A1 (en) | 2003-02-20 |
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