EP1183454B1 - PROCEDE DE COMMANDE DE LA REGENERATION D'UN CATALYSEUR ACCUMULATEUR DE NOx - Google Patents
PROCEDE DE COMMANDE DE LA REGENERATION D'UN CATALYSEUR ACCUMULATEUR DE NOx Download PDFInfo
- Publication number
- EP1183454B1 EP1183454B1 EP00931213A EP00931213A EP1183454B1 EP 1183454 B1 EP1183454 B1 EP 1183454B1 EP 00931213 A EP00931213 A EP 00931213A EP 00931213 A EP00931213 A EP 00931213A EP 1183454 B1 EP1183454 B1 EP 1183454B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- regeneration
- measure
- comparison value
- threshold value
- concentration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
- F01N3/00—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust
- F01N3/08—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous
- F01N3/0807—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous by using absorbents or adsorbents
- F01N3/0828—Exhaust or silencing apparatus having means for purifying, rendering innocuous, or otherwise treating exhaust for rendering innocuous by using absorbents or adsorbents characterised by the absorbed or adsorbed substances
- F01N3/0842—Nitrogen oxides
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
- F01N13/00—Exhaust or silencing apparatus characterised by constructional features ; Exhaust or silencing apparatus, or parts thereof, having pertinent characteristics not provided for in, or of interest apart from, groups F01N1/00 - F01N5/00, F01N9/00, F01N11/00
- F01N13/009—Exhaust or silencing apparatus characterised by constructional features ; Exhaust or silencing apparatus, or parts thereof, having pertinent characteristics not provided for in, or of interest apart from, groups F01N1/00 - F01N5/00, F01N9/00, F01N11/00 having two or more separate purifying devices arranged in series
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/02—Circuit arrangements for generating control signals
- F02D41/021—Introducing corrections for particular conditions exterior to the engine
- F02D41/0235—Introducing corrections for particular conditions exterior to the engine in relation with the state of the exhaust gas treating apparatus
- F02D41/027—Introducing corrections for particular conditions exterior to the engine in relation with the state of the exhaust gas treating apparatus to purge or regenerate the exhaust gas treating apparatus
- F02D41/0275—Introducing corrections for particular conditions exterior to the engine in relation with the state of the exhaust gas treating apparatus to purge or regenerate the exhaust gas treating apparatus the exhaust gas treating apparatus being a NOx trap or adsorbent
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/02—Circuit arrangements for generating control signals
- F02D41/021—Introducing corrections for particular conditions exterior to the engine
- F02D41/0235—Introducing corrections for particular conditions exterior to the engine in relation with the state of the exhaust gas treating apparatus
- F02D41/027—Introducing corrections for particular conditions exterior to the engine in relation with the state of the exhaust gas treating apparatus to purge or regenerate the exhaust gas treating apparatus
- F02D41/0275—Introducing corrections for particular conditions exterior to the engine in relation with the state of the exhaust gas treating apparatus to purge or regenerate the exhaust gas treating apparatus the exhaust gas treating apparatus being a NOx trap or adsorbent
- F02D41/028—Desulfurisation of NOx traps or adsorbent
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/02—Circuit arrangements for generating control signals
- F02D41/14—Introducing closed-loop corrections
- F02D41/1438—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor
- F02D41/1444—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases
- F02D41/146—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases the characteristics being an NOx content or concentration
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/02—Circuit arrangements for generating control signals
- F02D41/14—Introducing closed-loop corrections
- F02D41/1438—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor
- F02D41/1444—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases
- F02D41/146—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases the characteristics being an NOx content or concentration
- F02D41/1463—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases the characteristics being an NOx content or concentration of the exhaust gases downstream of exhaust gas treatment apparatus
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
- F01N2550/00—Monitoring or diagnosing the deterioration of exhaust systems
- F01N2550/03—Monitoring or diagnosing the deterioration of exhaust systems of sorbing activity of adsorbents or absorbents
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F01—MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
- F01N—GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR MACHINES OR ENGINES IN GENERAL; GAS-FLOW SILENCERS OR EXHAUST APPARATUS FOR INTERNAL COMBUSTION ENGINES
- F01N2570/00—Exhaust treating apparatus eliminating, absorbing or adsorbing specific elements or compounds
- F01N2570/04—Sulfur or sulfur oxides
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/0025—Controlling engines characterised by use of non-liquid fuels, pluralities of fuels, or non-fuel substances added to the combustible mixtures
- F02D41/0047—Controlling exhaust gas recirculation [EGR]
Definitions
- the invention relates to a method for controlling a regeneration of at least one NO x storage catalytic converter arranged in an exhaust gas duct of an internal combustion engine with the features mentioned in the preamble of claim 1.
- gaseous pollutants are generated which can be divided into reducing agents such as CO, HC or H 2 or oxidizing agents such as NO X or SO X.
- reducing agents such as CO, HC or H 2
- oxidizing agents such as NO X or SO X.
- the reducing agents are oxidized on the catalyst with oxygen, while the oxidizing agents are reacted with the reducing agents.
- NO X storage which can also be combined with the catalyst for a NO x storage catalyst.
- the NO X storage catalytic converter absorbs the NO X as nitrate, until it does so a NO x desorption temperature and / or a NO x storage capacity is exceeded.
- NO x regeneration It is therefore known to regenerate the NO x storage catalytic converter in regular cycles (NO x regeneration).
- NO X regeneration there is a brief change to a working mode with ⁇ ⁇ 1.
- the stored NO X is desorbed again and reduced on the catalyst with the reducing agents.
- a need for regeneration can be made dependent on individual operating parameters that can be measured directly by suitable measuring devices. For example, it is known from DE 197 29 676 A1 to initiate the regeneration as a function of certain limit temperatures. A more complex model for such a control can be found in DE 197 16 275 C1.
- the current driving situation, a loading condition and a current lambda value can be taken into account.
- the conditions can be linked to certain parameters during the regeneration.
- Reversible damage can occur, for example, by covering the catalyst with a condensate or soot.
- SO x is formed, which, like NO x , is absorbed by the storage.
- Storage of the SO x as sulfate leads, among other things, to a reduction in the NO x storage capacity, but can also lead to damage to the catalyst in the long term, for example due to sulfite formation.
- sulfate grain formation during absorption can lead to tensions within the structure of a NO x storage catalytic converter, which can result in irreversible damage to the NO x storage catalytic converter.
- the need for desulfurization can be determined on the basis of parameters characterizing a current catalyst state, such as a degree of sulfurization, a current lambda value or a catalyst temperature.
- the degree of sulfurization can be determined, for example, as a function of a NO x concentration downstream of the NO x storage catalytic converter.
- Component-specific sensors such as NO x sensors are suitable for detecting the NO x concentration.
- a method can be found in DE 198 37 074 A1 with which a regulation of an air-fuel ratio is influenced during a desulfurization phase. An actual / target comparison of an oxygen concentration during the desulfurization is carried out and a fuel signal generated from this is used to redefine the fuel concentration supplied during the desulfurization.
- a disadvantage of the known methods is poor coordination of a sequence of individual regeneration measures. As a result, increased fuel consumption can occur and it is not possible to select the regeneration measure in accordance with a current catalytic converter condition.
- the object of the method according to the invention is to continuously monitor a functionality of the NO x storage catalytic converter with regard to the NO x storage capacity and the catalytic activity and to adapt the regeneration measure to the current catalytic converter condition.
- the comparison value is determined again during or after the regeneration measure. If the comparison value is exceeded, at least one further regeneration measure is taken.
- the catalyst system 10 comprises a NO x storage catalytic converter 16 and a pre-catalytic converter 18 as well as the temperature sensors 22.
- gas sensors 19, 20, 21 are assigned to the catalytic converter system, which can detect a gas content of a gas component in the exhaust gas. Lambda sensors or component-specific sensors are suitable, for example.
- the gas sensor 21 enables at least detection of a NO x concentration and is therefore a NO x sensor.
- a working mode of the internal combustion engine 14 can be regulated by means of an engine control unit 24. If, for example, a working mode with ⁇ ⁇ 1 (rich atmosphere) is desired, an oxygen concentration in an intake manifold 26 must be reduced before a fuel-air mixture is combusted. This simultaneously increases the content of reducing agents such as CO, HC and H 2 in the exhaust gas compared to an oxygen content.
- a working mode can be set by reducing a volume flow of intake air by means of a throttle valve 28 and by simultaneously supplying low-oxygen exhaust gas via an exhaust gas reflux valve 30.
- Gaseous pollutants such as CO, HC, NO X or SO X are formed in varying proportions during a combustion process.
- the reducing agents can be oxidized by oxygen on the pre-catalyst 18. With sufficient oxygen concentration, a complete or extensive implementation is possible under almost all working modes.
- absorbed SO X is stored in the form of sulfate in the NO X storage catalytic converter 16, although reversibility of this storage process, in contrast to the storage of NO X, requires significantly higher temperatures.
- a minimum desulfurization temperature and a lambda value ⁇ 1 must therefore be available for desulfurization (SO X regeneration parameter).
- a NO x concentration in the exhaust gas behind the NO x storage catalytic converter 16 is continuously detected. This concentration is compared with a target NO x concentration and a comparison value is formed in accordance with a deviation of the concentration from the target concentration. If the comparison value exceeds a predefinable threshold value, a regeneration measure is taken.
- the regeneration measure includes a SO x regeneration (desulfurization), NO x regeneration or an increase in the exhaust gas temperature in order to eliminate an occupation of the storage catalytic converter with condensate or soot. Important when making a selection the regeneration measure is to match this to a regeneration measure that may have been carried out beforehand. In this way, individual regeneration measures can be coordinated and control of the regeneration of the storage catalytic converter 16 can be carried out much more effectively. If the comparison value continues to exceed the threshold value after the regeneration measure has been carried out, a further regeneration measure is selected and carried out.
- FIG. 2 shows a block diagram for controlling the regeneration of the NO x storage catalytic converter 16 in a rich atmosphere.
- a NO x regeneration of the NO x storage catalytic converter 16 can already be carried out in such an atmosphere. If the comparison value in a comparison 40 is below the threshold value, no further measure (42) is taken. However, if the comparison value reaches the threshold value, an operating parameter of the internal combustion engine 14 is influenced at least temporarily in such a way that the exhaust gas temperature is increased (exhaust gas temperature increase 44). A comparison 40 of the comparison value and the threshold value is then carried out again. If the comparison value continues to exceed the threshold value, irreversible damage to the NO x storage catalytic converter 16 can be concluded.
- comparison 40 of the comparison value with the threshold value takes place and, if necessary, NO x regeneration 48 is initiated as a regeneration measure. If, in a subsequent comparison 40, the comparison value is again greater than the threshold value, a second NO X regeneration 50 is initiated. After the second NO x regeneration 50 has ended, the comparison value and threshold value are again compared. If the regeneration measure was successful, no further measures 42 are taken.
- an adaptation 52 of a content of reducing agents in the exhaust gas during the NO x regeneration can be carried out as a function of the previously detected comparison value, for example to compensate for minor irreversible damage to the NO x storage catalytic converter 16.
- the comparison value 40 continues to exceed the threshold value, the NO x storage catalytic converter 16 is subjected to an exhaust gas temperature (exhaust gas temperature increase 44) that is elevated. Perform this too Regeneration measure not to reduce the comparison value, a first SO X regeneration 54 is initiated and possibly also a second SO X regeneration 56 subsequently. A comparison 40 of the comparison value and threshold value then takes place again. If the comparison value is again below the threshold value, an adjustment of the content of reducing agents during the SO x regeneration can be carried out analogously to the method during the NO x regeneration (adaptation 58).
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Exhaust Gas After Treatment (AREA)
- Electrical Control Of Air Or Fuel Supplied To Internal-Combustion Engine (AREA)
Abstract
Claims (10)
- Procédé pour la commande d'une régénération d'au moins un catalyseur accumulateur de NOx disposé dans un canal de gaz brûlés d'un moteur à combustion interne, une concentration de NOx des gaz brûlés étant enregistrée par un capteur de NOx disposé en aval du catalyseur accumulateur de NOx,
caractérisé en ce que(a) la concentration mesurée de NOx après le catalyseur accumulateur est comparée avec une concentration prévue de NOx et une valeur de référence est déterminée en fonction d'un écart de cette concentration de NOx par rapport à la concentration prévue de NOx,(b) en cas de dépassement de la valeur de comparaison au-delà d'une valeur seuil prédéfinissable, une mesure de régénération est prise, lors de laquelle au moins un paramètre de service du moteur à combustion interne (14) est influencé au moins de façon temporaire et(c) la mesure de régénération est choisie en fonction d'une mesure de régénération appliquée auparavant. - Procédé selon la revendication 1, caractérisé en ce que, pendant ou après la mesure de régénération, la valeur de comparaison est déterminée à nouveau et au moins une autre mesure de génération est prise lorsque la valeur de comparaison dépasse la valeur seuil.
- Procédé selon la revendication 1 et la revendication 2, caractérisé en ce que, lorsque la valeur de comparaison dépasse la valeur seuil dans un mode de travail pauvre du moteur à combustion interne (14), une régénération en NOx est mise en oeuvre comme mesure de régénération.
- Procédé selon les revendications 1 et 2, caractérisé en ce que, lorsque la valeur de comparaison dépasse la valeur seuil dans un mode de travail gras du moteur à combustion interne (14), une température des gaz brûlés est augmentée comme mesure de régénération.
- Procédé selon la revendication 3, caractérisé en ce que, lorsque la valeur de comparaison dépasse à nouveau la valeur seuil, la régénération en NOx est répétée comme mesure de régénération.
- Procédé selon la revendication 5, caractérisé en ce que, lorsque la valeur de comparaison dépasse à nouveau la valeur seuil, la température des gaz brûlés est augmentée comme mesure de régénération.
- Procédé selon la revendication 6, caractérisé en ce que, lorsque la valeur de comparaison dépasse à nouveau la valeur seuil, une régénération en SOx est mise en oeuvre comme mesure de régénération.
- Procédé selon la revendication 7, caractérisé en ce que, lorsque la valeur de comparaison dépasse à nouveau la valeur seuil, la régénération en SOx est répétée comme mesure de génération.
- Procédé selon les revendications 4 et 8, caractérisé en ce qu'un préjudice irréversible pour le catalyseur accumulateur de NOx peut être déterminé avec un nouveau dépassement de la valeur de comparaison au-delà de la valeur seuil.
- Procédé selon l'une quelconque des revendications précédentes, caractérisé en ce qu'une teneur de l'agent réducteur dans les gaz brûlés est modifiée en fonction de la valeur de comparaison pendant la régénération en NOx ou SOx.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19923498A DE19923498A1 (de) | 1999-05-21 | 1999-05-21 | Verfahren zur Steuerung einer Regeneration eines NOx-Speicherkatalysators |
DE19923498 | 1999-05-21 | ||
PCT/EP2000/004335 WO2000071878A1 (fr) | 1999-05-21 | 2000-05-13 | PROCEDE DE COMMANDE DE LA REGENERATION D'UN CATALYSEUR ACCUMULATEUR DE NOx |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1183454A1 EP1183454A1 (fr) | 2002-03-06 |
EP1183454B1 true EP1183454B1 (fr) | 2004-04-28 |
Family
ID=7908846
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP00931213A Expired - Lifetime EP1183454B1 (fr) | 1999-05-21 | 2000-05-13 | PROCEDE DE COMMANDE DE LA REGENERATION D'UN CATALYSEUR ACCUMULATEUR DE NOx |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP1183454B1 (fr) |
JP (1) | JP2003500595A (fr) |
DE (2) | DE19923498A1 (fr) |
WO (1) | WO2000071878A1 (fr) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10004330A1 (de) * | 2000-02-01 | 2001-08-02 | Deutz Ag | Programmierbare Steuer- und Regelelektronik für eine Brennkraftmaschine |
DE60116278T2 (de) * | 2001-06-28 | 2006-08-03 | Isuzu Motors Ltd. | Vorrichtung zur Reinigung des Abgases mit einem Stickoxidfallekatalysator |
JP3800080B2 (ja) * | 2001-11-30 | 2006-07-19 | トヨタ自動車株式会社 | 内燃機関の排気浄化装置 |
DE10249610B4 (de) * | 2002-10-18 | 2010-10-07 | Volkswagen Ag | Verfahren und Vorrichtung zur Steuerung eines NOx-Speicherkatalysators |
DE10318210B4 (de) * | 2003-04-22 | 2006-06-14 | Siemens Ag | Betriebsverfahren für eine Brennkraftmaschine mit einem Vorkatalysator und einem Speicherkatalysator |
DE10331331B4 (de) * | 2003-07-10 | 2012-03-01 | Volkswagen Ag | Verfahren zum Betreiben einer Brennkraftmaschine |
DE102005050517A1 (de) | 2005-10-21 | 2007-04-26 | Umicore Ag & Co. Kg | Verfahren zum Betreiben eines Stickoxid-Speicherkatalysators an einem Dieselmotor |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2985638B2 (ja) * | 1993-10-18 | 1999-12-06 | トヨタ自動車株式会社 | 内燃機関の排気浄化装置 |
JP2888124B2 (ja) * | 1994-01-27 | 1999-05-10 | トヨタ自動車株式会社 | 内燃機関の排気浄化装置 |
DE19543219C1 (de) * | 1995-11-20 | 1996-12-05 | Daimler Benz Ag | Verfahren zum Betreiben eines Dieselmotors |
JPH1071325A (ja) * | 1996-06-21 | 1998-03-17 | Ngk Insulators Ltd | エンジン排ガス系の制御方法および触媒/吸着手段の劣化検出方法 |
DE19705335C1 (de) * | 1997-02-12 | 1998-09-17 | Siemens Ag | Verfahren zur Regeneration eines Speicherkatalysators |
DE19716275C1 (de) * | 1997-04-18 | 1998-09-24 | Volkswagen Ag | Verfahren zur Stickoxidreduzierung im Abgas einer Brennkraftmaschine |
DE19729676C5 (de) * | 1997-07-11 | 2004-04-15 | Ford Global Technologies, LLC (n.d.Ges.d. Staates Delaware), Dearborn | Verfahren zum Betrieb eines Verbrennungsmotors zum Schutz einer Abgasbehandlungseinrichtung |
US5983627A (en) * | 1997-09-02 | 1999-11-16 | Ford Global Technologies, Inc. | Closed loop control for desulfating a NOx trap |
DE19744409C2 (de) * | 1997-10-08 | 2001-11-08 | Ford Global Tech Inc | Verfahren zur Regeneration einer Stickoxidfalle im Abgassystem eines Verbrennungsmotors sowie Vorrichtung zur Durchführung des Verfahrens |
DE19801815A1 (de) * | 1998-01-19 | 1999-07-22 | Volkswagen Ag | Mager-Regeneration von NOx-Speichern |
DE19830829C1 (de) * | 1998-07-09 | 1999-04-08 | Siemens Ag | Verfahren zur Regeneration eines NOx-Speicherkatalysators |
-
1999
- 1999-05-21 DE DE19923498A patent/DE19923498A1/de not_active Withdrawn
-
2000
- 2000-05-13 WO PCT/EP2000/004335 patent/WO2000071878A1/fr active IP Right Grant
- 2000-05-13 DE DE50006263T patent/DE50006263D1/de not_active Expired - Lifetime
- 2000-05-13 EP EP00931213A patent/EP1183454B1/fr not_active Expired - Lifetime
- 2000-05-13 JP JP2000620236A patent/JP2003500595A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
DE50006263D1 (de) | 2004-06-03 |
DE19923498A1 (de) | 2000-11-23 |
WO2000071878A1 (fr) | 2000-11-30 |
EP1183454A1 (fr) | 2002-03-06 |
JP2003500595A (ja) | 2003-01-07 |
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