EP1140391B1 - Method and device for controlling and/or maintaining the temperature of a melt, preferably of a steel melt during continuous casting - Google Patents
Method and device for controlling and/or maintaining the temperature of a melt, preferably of a steel melt during continuous casting Download PDFInfo
- Publication number
- EP1140391B1 EP1140391B1 EP00901067A EP00901067A EP1140391B1 EP 1140391 B1 EP1140391 B1 EP 1140391B1 EP 00901067 A EP00901067 A EP 00901067A EP 00901067 A EP00901067 A EP 00901067A EP 1140391 B1 EP1140391 B1 EP 1140391B1
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- EP
- European Patent Office
- Prior art keywords
- melt
- temperature
- induction coil
- heat
- cooling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 239000000155 melt Substances 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 20
- 239000000161 steel melt Substances 0.000 title claims abstract description 5
- 238000009749 continuous casting Methods 0.000 title description 6
- 230000006698 induction Effects 0.000 claims abstract description 22
- 238000001816 cooling Methods 0.000 claims abstract description 15
- 230000008878 coupling Effects 0.000 claims abstract description 7
- 238000010168 coupling process Methods 0.000 claims abstract description 7
- 238000005859 coupling reaction Methods 0.000 claims abstract description 7
- 239000012809 cooling fluid Substances 0.000 claims description 8
- 239000004020 conductor Substances 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 4
- 238000005259 measurement Methods 0.000 claims description 3
- 230000033228 biological regulation Effects 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 claims description 2
- 238000004804 winding Methods 0.000 claims description 2
- 239000007788 liquid Substances 0.000 abstract description 3
- 230000005672 electromagnetic field Effects 0.000 abstract description 2
- 230000005540 biological transmission Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 25
- 229910000831 Steel Inorganic materials 0.000 description 15
- 239000010959 steel Substances 0.000 description 15
- 238000005266 casting Methods 0.000 description 10
- 238000009826 distribution Methods 0.000 description 7
- 239000002893 slag Substances 0.000 description 7
- 239000002184 metal Substances 0.000 description 6
- 230000001939 inductive effect Effects 0.000 description 5
- 238000000465 moulding Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 230000001276 controlling effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 238000009420 retrofitting Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/10—Supplying or treating molten metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D41/00—Casting melt-holding vessels, e.g. ladles, tundishes, cups or the like
- B22D41/005—Casting melt-holding vessels, e.g. ladles, tundishes, cups or the like with heating or cooling means
- B22D41/01—Heating means
- B22D41/015—Heating means with external heating, i.e. the heat source not being a part of the ladle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/10—Supplying or treating molten metal
- B22D11/11—Treating the molten metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/16—Controlling or regulating processes or operations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D41/00—Casting melt-holding vessels, e.g. ladles, tundishes, cups or the like
- B22D41/005—Casting melt-holding vessels, e.g. ladles, tundishes, cups or the like with heating or cooling means
Definitions
- the invention relates to a method for adjusting and / or maintaining the temperature a melt preferably a molten steel, wherein the temperature of the Melt measured in a vessel, the measurement result with a predetermined Temperature range compared in terms of nominal values and the melt supplied by electrical induction of an induction coil so much heat or is removed by means of a cooling device, that the temperature of the melt within the target range.
- the invention also relates to a device to carry out the process.
- tundish In continuous casting, especially steel, is in the distribution vessel, in the following Also called tundish, for quality and operational reasons one as uniform as possible a temperature of the melt, or the observance of a narrow temperature window, aimed. Due to the temperature losses of Melt in the pan, when transferring from the pan to the distributor and in the distributor itself, the casting time is limited in time.
- a device for controlling the temperature of the melt in Manifold can have different melt temperatures in the pans balanced in the distributor and the possible casting time can be extended.
- the Advantages of such a device are still in a greater flexibility in casting disorders and especially in the homogenization of the temperature level in the tundish. From this quality advantages in the continuous casting product expected. Also a casting closer to the liquidus becomes possible.
- Plasma heaters which are usually positioned above the distributor.
- the principle of plasma heating is in a vertical tundish level following chamber with electrodes an arc on one to transfer free metal surface.
- the arc is stabilized with argon-hence the term plasma.
- the steel either over dams and weirs or additional to be attached Flushing, z.
- a disadvantage of this process variant is the necessary free surface of the melt within the chamber so that physical and chemical interactions between the chamber atmosphere and the melt are to be expected. Due to the very high temperatures in the arc, vapor and dust build up within the chamber. Furthermore, inductive Tundish heaters are known in which a distinction is made between so-called crucible inductors and gutter or channel inductors, which are usually firmly flanged connected to the construction of the manifold. The gutter inductors compared to the crucible inductors are relatively expensive to manufacture and maintain.
- US-A-5 084 089 describes at a recessed area of a manifold externally fixedly arranged induction coils and one in the melt in the Distributor submerged cooling device to regulate the melt temperature.
- inductive heating arise from lack of contact with the Melt, as well as by the induced electromagnetic alternating field accompanying force generation in the melt, leading to a stirring movement the melt and thus to a faster Wärmverieilung within of the distribution vessel provides.
- Disadvantages of the previously performed inductive Tundish heaters arise from the firm attachment to the tundish, the has a negative impact on flexibility. Also, the necessary maintenance and Maintenance effort is significant.
- the non-prepublished patent application DE 197 52 548 A1 relates to a Method for adjusting and maintaining the temperature, in particular one Molten steel, in narrow temperature limits over the casting time during continuous casting, wherein the decrease in the temperature is compensated by heating.
- the process is improved by the fact that the temperature of the melt at Outlet of the distribution vessel measured, the measurement result with the specified compared lower temperature limit and the melt when reaching or Falling below the limit value is heated until the temperature is again within the setpoint range. This is also a warming the melt mentioned by an inductively operating heater, without that the necessary means or a corresponding device described are.
- the document EP 0 657 236 A1 describes a batch operation designed for tiltable casting container for casting a molten metal with a inductive heating.
- This includes one with an adjustable distance, parallel arranged to the metal mirror, traceable in the vertical direction, flat circular induction coil, through which the melt by direct coupling of the induced electromagnetic alternating field without contact is heated. Since the efficiency of the inductive field with increasing Distance of the induction coil to the melt decreases sharply, the distance is possible to keep low. For this purpose, an operation without cover slag is necessary whereby a direct contact between melt and atmosphere arises.
- the device described is already due to the design as a batch reactor for the continuous operation of a distribution vessel during continuous casting not suitable.
- an operation under atmospheric access is in steel because of the immediate onset of physical and chemical reactions between molten steel and atmosphere not possible.
- the invention has the object based, a method referred to in the preamble of claim 1 Art and to provide a suitable device for its implementation, which while avoiding the existing disadvantages of the prior art and Difficulties a technically uncomplicated, flexible and therefore economical advantageous temperature control of a molten metal in a distribution vessel allows.
- the melt temperature in a refractory, closed at the bottom Molded induction coil is immersed in the melt.
- the Heating power of the device hereinafter also referred to as heating element, is regulated by the current intensity of the current flowing through the induction coil.
- the induction coil is by a cooling fluid, preferably air, from the inside and / or cooled outside.
- the process provides that the melt heat by heat conduction is transmitted from the wall of the molding, which in turn induced on the coupled electromagnetic alternating field.
- the melt may heat by coupling the electromagnetic Alternating field are supplied. Also, the melt can by means of heat conduction Heat is removed through the wall of the molding.
- the invention further includes an apparatus for carrying out the method according to the invention, wherein the molded part with an inductively coupled, refractory, bottom closed tube is formed, which is the induction coil interchangeable and fluid cooling, in particular air cooling, receives, is immersed in the melt and at the top Outlets for carrying out the fluid-cooled conductors and connections for supplying and removing optionally additional cooling fluid.
- the heater shown in FIG. 1 20 for carrying out the method of the Invention comprises an induction coil 1 of an inside with fluid 45, 45 'cooled, current-carrying conductor 2 with a number of turns 3 along a vertical axis y-y with respect to the coil length L relatively small winding diameter D in a refractory molding 24.
- the molding 24 has a closed bottom 15 and takes to form a tubular Cavity in the form of a sleeve 24 and release of vertical cooling channels 9 the Induction coil 1 interchangeable.
- the sleeve or wall 24 of the heating element 20 consists of a to the electromagnetic alternating field of the induction coils 1 coupling refractory material (See, for example, EP 0 526 718 B1).
- the heat transfer takes place via Heat conduction from the wall 20 in the melt 10.
- the Melt 10 via a change of the induced alternating field by direct Coupling heat to be supplied. Due to special properties the sleeve material 24 can this without external heating and without presence be inductively heated by surrounding coupling material.
- Fig. 1 further shows a section of a manifold 11 with therein contained molten steel melt 10 and a layer of slag floating thereon 22.
- the material of the sleeve 24 is opposite to the molten steel 10th is largely inert, but is in the slag layer 22 with an additional Slag protection jacket 25 against mechanical and chemical Reinforced wear.
- the bottom of the distributor 11 is made of a steel jacket 19 formed with a refractory lining 21.
- the controllable feeder of AC to induction coil 1 is symbolically marked 33.
- FIG. 2a shows the heating element 20 with slag protection jacket 25 and media connections 18 and 33 in conjunction with a manipulator 16.
- the manipulator 16 comprises a guide column 34 on a steel frame 32 with a rotatable and liftable sleeve 43 and is on the rod arms 23 with the Heating rod 20 hinged.
- the manipulator 16 has on the one hand Lifting and lowering device 26 in the form of a hydraulic element, and on the other a hydraulically operable device 27 for pivoting the linkage arms 23rd
- An alternative device has a fixed guide 35 on a steel frame 32 on which a between guide rollers in vertical Direction movable and also pivotable support member 36 receives.
- the numbers 26 and 27 indicate the required lifting or lowering Manipulators.
- the immersed in the melt 10 heating rod 20 or Bankstab weakness according to the figures 3 to 5 is assigned a respective temperature sensor 28 and with a signal line 29 of a computing unit 30 aufschaltbar, via control lines 31, the movements of the manipulator 16 and the current 33rd for controlling the alternating electromagnetic field in accordance with Temperaturmeßhong the melt 10 controls or regulates. This is in the corresponding Control scheme in Fig. 3a indicated in principle.
- the arithmetic unit 30 compares the measured values with the nominal value specifications and, if appropriate, with Deviations, the heating power of the heating elements 20 is controlled.
- the arithmetic unit 30 with control lines 31, the cooling fluid supply for the internal cooling of the conductors and the fluid cooling of the heating rods 20 monitored by the cooling fluid supply line 39 and theméfluidanschiuß 18 and be controlled, whereby the heating rods 20 and the melt 10 at Overheating heat can be withdrawn.
- Fig. 3a further shows an elongated design of the manifold 11 with an inlet 12 for liquid steel and an adjustable drain 13. Between inlet 12 and drain 13, at least one temperature sensor 28 is arranged and over the Signal line 29 connected to the arithmetic unit. To the preferred flow line the molten metal is in the distributor or Tundish 11 an intermediate wall 37 arranged with through-flow openings, creating a better Flow distribution around the heating rods 20 for more uniform heat dissipation. or supply according to the plan view in Fig. 3b is achieved.
- Figs. 4a and 4b is another embodiment of the manifold 11 with karangeredem Feed 12 for the melt and two laterally arranged controllable Outlets 13 shown. Due to the multiple arrangement of individual controllable heating rods 20 or Bankstab phenomenon and the associated temperature sensors 28, is an even more accurate monitoring of the melt temperature in the distributor 11 possible.
- FIGS. 5a and 5b show an embodiment of the distributor 11 in L-shape. Between the inlets 12 and the drains 13 is between two each Temperature sensors 28 an arrangement of two heating rods 20 is provided. These are articulated articulated link arms 23 with the manipulator 16th connected and thus in both the vertical and in the horizontal direction hubund rotatably arranged.
- the manipulator 16 is by a frame 41 with the casting platform 40 of the continuous casting firmly connected.
- the arrangement shows otherwise, similar to FIGS. 2a and 2b, lifting and pivoting devices 27 for positioning the heating rods 20 within the melt 10 in the manifold 11th
- the method according to the invention and the trained for its implementation Device according to FIGS. 1 to 5 optimally fits the constructive Conditions of corresponding distributor forms and other casting platform assemblies on. This is a simple retrofitting of existing systems possible with the device.
Abstract
Description
Die Erfindung betrifft ein Verfahren zum Einstellen und/oder Halten der Temperatur einer Schmelze bevorzugt einer Stahlschmelze, wobei die Temperatur der Schmelze in einem Gefäss gemessen, das Messergebnis mit einem vorgebbaren Temperaturbereich in Form von SOLL-Werten verglichen und der Schmelze durch elektrische Induktion einer Induktionsspule soviel Wärme zugeführt oder mittels einer Kühleinrichtung entzogen wird, dass die Temperatur der Schmelze innerhalb des SOLL-Bereiches liegt. Die Erfindung betrifft auch eine Vorrichtung zur Durchführung des Verfahrens.The invention relates to a method for adjusting and / or maintaining the temperature a melt preferably a molten steel, wherein the temperature of the Melt measured in a vessel, the measurement result with a predetermined Temperature range compared in terms of nominal values and the melt supplied by electrical induction of an induction coil so much heat or is removed by means of a cooling device, that the temperature of the melt within the target range. The invention also relates to a device to carry out the process.
Beim Stranggießen, insbesondere von Stahl, wird im Verteilergefäß, im folgenden auch als Tundish bezeichnet, aus Qualitäts- und Betriebsgründen eine möglichst gleichmäßige Temperatur der Schmelze, bzw. die Einhaltung eines engen Temperaturfensters, angestrebt. Aufgrund der Temperaturverluste der Schmelze in der Pfanne, beim Überführen aus der Pfanne in den Verteiler und im Verteiler selbst, ist die Gießdauer zeitlich beschränkt.In continuous casting, especially steel, is in the distribution vessel, in the following Also called tundish, for quality and operational reasons one as uniform as possible a temperature of the melt, or the observance of a narrow temperature window, aimed. Due to the temperature losses of Melt in the pan, when transferring from the pan to the distributor and in the distributor itself, the casting time is limited in time.
Durch den Einbau einer Vorrichtung zur Temperaturregelung der Schmelze im Verteilergefäß können unterschiedliche Schmelzentemperaturen in den Pfannen im Verteiler ausgeglichen und die mögliche Gießzeit verlängert werden. Die Vorteile einer solchen Vorrichtung liegen weiterhin in einer größeren Flexibilität bei Gießstörungen und vor allem in der Vergleichmäßigung des Temperatumiveaus im Tundish. Hiervon werden Qualitätsvorteile beim Stranggießprodukt erwartet. Auch ein Gießen näher am Liquidus wird möglich.By installing a device for controlling the temperature of the melt in Manifold can have different melt temperatures in the pans balanced in the distributor and the possible casting time can be extended. The Advantages of such a device are still in a greater flexibility in casting disorders and especially in the homogenization of the temperature level in the tundish. From this quality advantages in the continuous casting product expected. Also a casting closer to the liquidus becomes possible.
Bekannte Vorrichtungen zum Einstellen der Temperatur im Verteiler sind bspw. Plasmaheizungen, die üblicherweise oberhalb des Verteilers positioniert werden. Das Prinzip der Plasmaheizung besteht darin, in einer vertikal dem Tundish-Füllstand folgenden Kammer mit Elektroden einen Lichtbogen auf eine freie Metallfläche zu übertragen. Der Lichtbogen wird mit Argon stabilisiert-daher der Begriff Plasma. Im Bereich der Kammer entsteht ein heißer Fleck an dem der Stahl entweder über Dämme und Wehre oder zusätzliche anzubringende Spülvorrichtungen, z. B. poröse, für Gas durchlässige Bodenspülsteine, vorbeigeführt werden muß.Known devices for adjusting the temperature in the distributor are, for example. Plasma heaters, which are usually positioned above the distributor. The principle of plasma heating is in a vertical tundish level following chamber with electrodes an arc on one to transfer free metal surface. The arc is stabilized with argon-hence the term plasma. In the area of the chamber creates a hot spot the steel either over dams and weirs or additional to be attached Flushing, z. B. porous, gas permeable soil purging bricks, must be passed.
Nachteilig bei dieser Verfahrensvariante ist die notwendige freie Oberfläche der
Schmelze innerhalb der Kammer, so daß mit physikalischen und chemischen
Wechselwirkungen zwischen Kammeratmosphäre und Schmelze zu rechnen
ist. Aufgrund der sehr hohen Temperaturen im Lichtbogen setzt innerhalb der
Kammer Dampf- und Staubbildung ein.
Weiterhin sind induktive Tundish-Heizungen bekannt, bei welchen zwischen
sogenannten Tiegelinduktoren und Rinnen- bzw. Kanalinduktoren unterschieden
wird, die zumeist fest angeflanscht mit der Konstruktion des Verteilers verbunden
sind. Dabei sind die Rinneninduktoren gegenüber den Tiegelinduktoren
vergleichsweise aufwendig in Fertigung und Wartung.A disadvantage of this process variant is the necessary free surface of the melt within the chamber so that physical and chemical interactions between the chamber atmosphere and the melt are to be expected. Due to the very high temperatures in the arc, vapor and dust build up within the chamber.
Furthermore, inductive Tundish heaters are known in which a distinction is made between so-called crucible inductors and gutter or channel inductors, which are usually firmly flanged connected to the construction of the manifold. The gutter inductors compared to the crucible inductors are relatively expensive to manufacture and maintain.
Die US-A-5 084 089 beschreibt an einem vertieften Bereich eines Verteilers außen ortsfest angeordnete Induktionsspulen und eine in die Schmelze im Verteiler eintauchende Kühleinrichtung zur Regulierung der Schmelzentemperatur.US-A-5 084 089 describes at a recessed area of a manifold externally fixedly arranged induction coils and one in the melt in the Distributor submerged cooling device to regulate the melt temperature.
Vorteile der induktiven Heizung ergeben sich durch fehlenden Kontakt mit der Schmelze, sowie durch die mit dem induzierten elektromagnetischen Wechselfeld einhergehende Krafterzeugung in der Schmelze, die zu einer Rührbewegung der Schmelze und damit zu einer schnelleren Wärmeverieilung innerhalb des Verteilergefäßes sorgt. Nachteile der bisher ausgeführten induktiven Tundish-Heizungen ergeben sich aus dem festen Anbringen an den Tundish, die sich negativ auf die Flexibilität auswirkt. Auch der notwendige Wartungs- und Instandhaltungsaufwand ist erheblich. Advantages of inductive heating arise from lack of contact with the Melt, as well as by the induced electromagnetic alternating field accompanying force generation in the melt, leading to a stirring movement the melt and thus to a faster Wärmverieilung within of the distribution vessel provides. Disadvantages of the previously performed inductive Tundish heaters arise from the firm attachment to the tundish, the has a negative impact on flexibility. Also, the necessary maintenance and Maintenance effort is significant.
Die nicht vorveröffentlichte Patentanmeldung DE 197 52 548 A1 betrifft ein Verfahren zum Einstellen und Halten der Temperatur, insbesondere einer Stahlschmelze, in engen Temperaturgrenzen über die Gießzeit beim Stranggießen, wobei das Absinken der Temperatur durch Erwärmen kompensiert wird. Verbessert wird das Verfahren dadurch, daß die Temperatur der Schmelze am Auslauf des Verteilergefäßes gemessen, das Meßergebnis mit der vorgegebenen unteren Temperaturgrenze verglichen und die Schmelze bei Erreichen oder Unterschreiten des Grenzwertes so lange erwärmt wird, bis die Temperatur wieder innerhalb des Sollwert-Bereiches liegt. Dabei wird auch eine Erwärmung der Schmelze durch eine induktiv arbeitende Heizvorrichtung erwähnt, ohne daß die hierfür erforderlichen Mittel bzw. eine entsprechende Vorrichtung beschrieben sind.The non-prepublished patent application DE 197 52 548 A1 relates to a Method for adjusting and maintaining the temperature, in particular one Molten steel, in narrow temperature limits over the casting time during continuous casting, wherein the decrease in the temperature is compensated by heating. The process is improved by the fact that the temperature of the melt at Outlet of the distribution vessel measured, the measurement result with the specified compared lower temperature limit and the melt when reaching or Falling below the limit value is heated until the temperature is again within the setpoint range. This is also a warming the melt mentioned by an inductively operating heater, without that the necessary means or a corresponding device described are.
Das Dokument EP 0 657 236 A1 beschreibt eine für einen Chargenbetrieb ausgelegten, kippbaren Gießbehälter zum Gießen einer Metallschmelze mit einer induktiven Heizung. Diese umfaßt eine mit einem einstellbaren Abstand, parallel zum Metallspiegel angeordnete, in vertikaler Richtung nachführbare, flache kreisförmige Induktionsspule, durch welche die Schmelze durch direktes Ankoppeln des induzierten elektromagnetischen Wecheselfeldes berührungslos beheizt wird. Da der Wirkungsgrad des induktiven Feldes mit zunehmendem Abstand der Induktionsspule zur Schmelze stark abnimmt, ist der Abstand möglichst gering zu halten. Dazu ist ein Betrieb ohne Abdeckschlacke notwendig, wodurch ein direkter Kontakt zwischen Schmelze und Atmosphäre entsteht.The document EP 0 657 236 A1 describes a batch operation designed for tiltable casting container for casting a molten metal with a inductive heating. This includes one with an adjustable distance, parallel arranged to the metal mirror, traceable in the vertical direction, flat circular induction coil, through which the melt by direct coupling of the induced electromagnetic alternating field without contact is heated. Since the efficiency of the inductive field with increasing Distance of the induction coil to the melt decreases sharply, the distance is possible to keep low. For this purpose, an operation without cover slag is necessary whereby a direct contact between melt and atmosphere arises.
Die beschriebene Vorrichtung ist schon aufgrund der Auslegung als Chargenreaktor für den kontinuierlichen Betrieb eines Verteilergefäßes beim Stranggießen ungeeignet. Außerdem ist ein Betrieb unter Atmosphärenzutritt bei Stahl wegen der sofort einsetzenden physikalischen und chemischen Reaktionen zwischen Stahlschmelze und Atmosphäre nicht möglich.The device described is already due to the design as a batch reactor for the continuous operation of a distribution vessel during continuous casting not suitable. In addition, an operation under atmospheric access is in steel because of the immediate onset of physical and chemical reactions between molten steel and atmosphere not possible.
Beide Vorveröffentlichungen beschreiben nur Vorrichtungen bzw. Verfahren zum Aufheizen der Metallschmelze, wodurch einer Regelung der Schmelzentemperatur enge Grenzen gesetzt sind.Both prior publications describe only devices or methods for heating the molten metal, whereby a control of the melt temperature narrow limits are set.
Ausgehend vom vorgenannten Stand der Technik liegt der Erfindung die Aufgabe
zugrunde, ein Verfahren der im Oberbegriff von Anspruch 1 genannten Art
sowie eine zu dessen Durchführung geeignete Vorrichtung anzugeben, welche
unter Vermeidung der beim Stand der Technik bestehenden Nachteile und
Schwierigkeiten eine technisch unkomplizierte, flexible und damit wirtschaftlich
vorteilhafte Temperaturregelung einer Metallschmelze in einem Verteilergefäß
ermöglicht.Based on the aforementioned prior art, the invention has the object
based, a method referred to in the preamble of
Zur Lösung der Aufgabe wird mit der Erfindung vorgeschlagen, daß bei einem
Verfahren der im Oberbegriff von Anspruch 1 genannten Art zur Regulierung
der Schmelzentemperatur die in einem feuerfesten, bodenseitig geschlossenen
Formteil aufgenommene Induktionsspule in die Schmelze eingetaucht wird. Die
Heizleistung der Vorrichtung, im folgenden auch als Heizstab bezeichnet, wird
durch die Stromstärke des die Induktionsspule durchfließenden Stromes geregelt.
Die Induktionsspule wird durch ein Kühlfluid, bevorzugt Luft, von innen
und/oder außen gekühlt.To solve the problem is proposed with the invention that at a
Method of regulation mentioned in the preamble of
Dabei sieht das Verfahren vor, daß der Schmelze Wärme durch Wärmeleitung von der Wandung des Formteils übertragen wird, das seinerseits an das induzierte elektromagnetische Wechselfeld ankoppelt.The process provides that the melt heat by heat conduction is transmitted from the wall of the molding, which in turn induced on the coupled electromagnetic alternating field.
Alternativ kann der Schmelze Wärme durch Ankoppeln des elektromagnetischen Wechselfeldes zugeführt werden. Auch kann der Schmelze mittels Wärmeleitung durch die Wandung des Formteils Wärme entzogen werden.Alternatively, the melt may heat by coupling the electromagnetic Alternating field are supplied. Also, the melt can by means of heat conduction Heat is removed through the wall of the molding.
Die Erfindung umfaßt weiterhin eine Vorrichtung zur Durchführung des Verfahrens nach der Erfindung, wobei das Formteil mit einem induktiv ankoppelbaren, feuerfesten, bodenseitig geschlossenen Rohr ausgebildet ist, das die Induktionsspule austauschbar sowie eine Fluidkühlung, insbesondere Luftkühlung, aufnimmt, in die Schmelze eintauchbar angeordnet ist und am oberen Ende Auslässe zur Durchführung der fluidgekühlten Stromleiter sowie Anschlüsse zum Zu- und Abführen von gegebenenfalls zusätzlichem Kühlfluid aufweist.The invention further includes an apparatus for carrying out the method according to the invention, wherein the molded part with an inductively coupled, refractory, bottom closed tube is formed, which is the induction coil interchangeable and fluid cooling, in particular air cooling, receives, is immersed in the melt and at the top Outlets for carrying out the fluid-cooled conductors and connections for supplying and removing optionally additional cooling fluid.
Weitere Einzelheiten und Merkmale der Erfindung ergeben sich aus der nachstehenden Erläuterung eines in den Zeichnungen schematisch dargestellten Ausführungsbeispieles. Further details and features of the invention will become apparent from the following Explanation of a schematically illustrated in the drawings Embodiment.
Es zeigen:
Figur 1- Einen Heizstab nach der Erfindung, im Längsschnitt
- Figur 2a
- den Heizstab in Seitenansicht im Zusammenwirken mit einem Manipulator
- Figur 2b
- den Heizstab in Seitenansicht mit einem anderen Manipulator
- Figur 3a
- einen Schnitt in Seitenansicht durch einen Verteiler mit in die Schmelze eingetauchten Heizstäben sowie mit einem Temperaturfühler im Zusammenwirken mit einer Einrichtung zur Regelung der Temperatur der Schmelze
- Figur 3b
- einen Verteiler gemäß Figur 3a in Draufsicht
- Figur 4a
- einen Schnitt in Seitenansicht durch einen anders ausgestalteten Verteiler
- Figur 4b
- eine Anordnung gemäß Figur 4a in Draufsicht
- Figur 5a
- eine Anordnung im Schnitt durch V-V in Figur 5b bei alternativer Verteilerform mit eingetauchten Heizstäben in Führung mittels eines auf der Gießbühne installierten Ständers
- Figur 5b
- eine Anordnung gemäß Figur 5a in Draufsicht.
- FIG. 1
- A heating rod according to the invention, in longitudinal section
- FIG. 2a
- the heating element in side view in cooperation with a manipulator
- FIG. 2b
- the heating element in side view with another manipulator
- FIG. 3a
- a section in side view through a manifold with immersed in the melt heating elements and with a temperature sensor in cooperation with a device for controlling the temperature of the melt
- FIG. 3b
- a distributor according to Figure 3a in plan view
- FIG. 4a
- a section in side view through a differently designed manifold
- FIG. 4b
- an arrangement according to Figure 4a in plan view
- FIG. 5a
- an arrangement in section through VV in Figure 5b in alternative distribution form with immersed heating rods in leadership by means of a stand installed on the casting platform
- FIG. 5b
- an arrangement according to Figure 5a in plan view.
Der in Fig. 1 gezeigte Heizstab 20 zur Durchführung des Verfahrens nach der
Erfindung umfaßt eine Induktionsspule 1 eines innen mit Fluid 45, 45' gekühlten,
stromdurchflossenen Leiters 2 mit einer Anzahl Windungen 3 entlang einer
vertikalen Achse y-y mit im Vergleich zur Spulenlänge L relativ kleinem Windungsdurchmesser
D in einem feuerfesten Formteil 24. Das Formteil 24 besitzt
einen geschlossenen Boden 15 und nimmt unter Ausbildung eines rohrförmigen
Hohlraums in Form einer Hülse 24 und Freilassung vertikaler Kühlkanäle 9 die
Induktionsspule 1 austauschbar auf. Am oberen Ende sind Auslässe 17 zur
Durchführung der innen gekühlten Stromleiter 2 sowie Anschlüsse 18 zum Zuund
Abführen von zusätzlichem Kühlfluid und Halteelemente 14 zur Anlenkung
von Gestängearmen 23 eines Manipulators 16 vorgesehen.The heater shown in FIG. 1 20 for carrying out the method of the
Invention comprises an
Die Hülse bzw. Wandung 24 des Heizstabes 20 besteht aus einem an das
elektromagnetische Wechselfeld der Induktionsspulen 1 ankoppelbaren Feuerfestmaterial
(vgl. z.B. EP 0 526 718 B1). Der Wärmeübergang erfolgt über
Wärmeleitung von der Wandung 20 in die Schmelze 10. Zudem kann der
Schmelze 10 über eine Veränderung des induzierten Wechselfeldes durch direktes
Ankoppeln Wärme zugeführt werden. Aufgrund besonderer Eigenschaften
des Hülsenmaterials 24 kann dieses ohne Fremdheizung und ohne Vorhandensein
von umgebendem ankoppelbarem Material induktiv geheizt werden.The sleeve or
Fig. 1 zeigt weiter einen Ausschnitt aus einem Verteiler 11 mit darin enthaltener
flüssiger Stahlschmelze 10 und einer darauf schwimmenden Schlackenschicht
22. Das Material der Hülse 24 verhält sich gegenüber der Stahlschmelze 10
weitgehend inert, ist jedoch im Bereich der Schlackenschicht 22 mit einem zusätzlichen
Schlackenschutzmantel 25 gegen mechanischen und chemischen
Verschleiß verstärkt. Der Boden des Verteilers 11 wird von einem Stahlmantel
19 mit einer Feuerfestauskleidung 21 gebildet. Die regelbare Zuführung von
Wechselstrom zur Induktionsspule 1 ist symbolisch mit 33 gekennzeichnet.Fig. 1 further shows a section of a manifold 11 with therein contained
In den weiteren Figuren 2a, 2b bis 5a, 5b sind jeweils gleiche Elemente mit gleichen Bezugsziffern gekennzeichnet.In the other figures 2a, 2b to 5a, 5b are each identical elements with the same reference numerals.
Figur 2a zeigt den Heizstab 20 mit Schlackenschutzmantel 25 und Medienanschlüssen
18 und 33 in Verbindung mit einem Manipulator 16. FIG. 2a shows the
Der Manipulator 16 umfaßt eine Führungssäule 34 auf einem Stahlgerüst 32 mit
einer dreh- und hebbaren Hülse 43 und ist über die Gestängearme 23 mit dem
Heizstab 20 gelenkig verbunden. Der Manipulator 16 besitzt zum einen eine
Hub- und Senkvorrichtung 26 in Form eines Hydraulikelements, und zum anderen
eine hydraulisch betreibbare Vorrichtung 27 zum Schwenken der Gestängearme
23.The
Eine alternative Vorrichtung gemäß Fig. 2b weist eine feststehende Führung 35
auf einem Stahlgerüst 32 auf, die ein zwischen Führungsrollen in vertikaler
Richtung bewegliches sowie ebenfalls schwenkbares Tragelement 36 aufnimmt.
Die Ziffern 26 und 27 kennzeichnen die erforderlichen Hub- bzw. Senkund
Schwenkvorrichtungen.An alternative device according to FIG. 2b has a fixed
Dem in die Schmelze 10 eintauchenden Heizstab 20 bzw. Heizstabgruppen
gemäß den Figuren 3 bis 5 ist je ein Temperaturfühler 28 zugeordnet und mit
einer Signalleitung 29 einer Recheneinheit 30 aufschaltbar, die über Steuerleitungen
31 die Bewegungsabläufe des Manipulators 16 und die Stromstärke 33
zur Regelung des elektromagnetischen Wechselfeldes nach Maßgabe der
Temperaturmeßwerte der Schmelze 10 steuert bzw. regelt. Dies ist in dem entsprechenden
Regelschema in Fig. 3a prinzipiell angedeutet. Die Recheneinheit
30 vergleicht die Meßwerte mit den Soll-Wertvorgaben und bei entsprechenden
Abweichungen wird die Heizleistung der Heizstäbe 20 gesteuert. Darüber hinaus
kann durch die Recheneinheit 30 mit Steuerleitungen 31 die Kühlfluidzufuhr
für die Innenkühlung der Stromleiter und die Fluidkühlung der Heizstäbe 20
durch die Kühlfluidzuleitung 39 und den Kühlfluidanschiuß 18 überwacht und
angesteuert werden, wodurch den Heizstäben 20 und der Schmelze 10 bei
Überhitzung Wärme entzogen werden kann.The immersed in the
Fig. 3a zeigt weiter eine langgestreckte Bauart des Verteilers 11 mit einem Zulauf
12 für flüssigen Stahl und einem regelbaren Ablauf 13. Zwischen Zulauf 12
und Ablauf 13 ist wenigstens ein Temperaturfühler 28 angeordnet und über die
Signalleitung 29 mit der Recheneinheit verbunden. Zur bevorzugten Strömungsleitung
der Metallschmelze ist im Verteiler bzw. Tundish 11 eine Zwischenwand
37 mit durchströmbaren Öffnungen angeordnet, wodurch eine bessere
Strömungsverteilung um die Heizstäbe 20 zur gleichmäßigeren Wärmeab-
bzw. -zufuhr entsprechend der Draufsicht in Fig. 3b erzielt wird.Fig. 3a further shows an elongated design of the manifold 11 with an
In den Fig. 4a und 4b ist eine andere Ausgestaltung des Verteilers 11 mit mittelseitigem
Zulauf 12 für die Schmelze und zwei seitlich angeordneten regelbaren
Ausläufen 13 dargestellt. Durch die Mehrfachanordnung von einzelnen
steuerbaren Heizstäben 20 bzw. Heizstabgruppen und den zugeordneten Temperaturfühlern
28, ist eine noch exaktere Überwachung der Schmelzentemperatur
im Verteiler 11 möglich.In Figs. 4a and 4b is another embodiment of the manifold 11 with
In den Fig. 5a und 5b ist eine Ausgestaltung des Verteilers 11 in L-Form dargestellt.
Zwischen den Zuläufen 12 und den Abläufen 13 ist zwischen jeweils zwei
Temperaturfühlern 28 eine Anordnung von zwei Heizstäben 20 vorgesehen.
Diese sind über gelenkig anlenkbare Gestängearme 23 mit dem Manipulator 16
verbunden und damit sowohl in vertikaler als auch in horizontaler Richtung hubund
drehbeweglich angeordnet. Der Manipulator 16 ist durch ein Gestell 41 mit
der Gießbühne 40 der Stranggießanlage fest verbunden. Die Anordnung zeigt
im übrigen, ähnlich wie in den Fig. 2a und 2b, Hub- 26 und Schwenkvorrichtungen
27 zur Positionierung der Heizstäbe 20 innerhalb der Schmelze 10 im Verteiler
11.FIGS. 5a and 5b show an embodiment of the
Das Verfahren nach der Erfindung und die zu dessen Durchführung ausgebildete Vorrichtung entsprechend den Fig. 1 bis 5 paßt sich optimal den konstruktiven Gegebenheiten entsprechender Verteilerformen und anderer Gießbühnenaufbauten an. Damit ist ein einfaches Nachrüsten bereits bestehender Anlagen mit der Vorrichtung möglich. The method according to the invention and the trained for its implementation Device according to FIGS. 1 to 5 optimally fits the constructive Conditions of corresponding distributor forms and other casting platform assemblies on. This is a simple retrofitting of existing systems possible with the device.
- 11
- Induktionsspuleinduction coil
- 22
- Leiterladder
- 33
- Windungconvolution
- 99
- Kühlkanälecooling channels
- 1010
- Schmelzemelt
- 1111
- Verteilerdistributor
- 1212
- Zulauf für StahlschmelzeFeed for molten steel
- 1313
- Auslauf für StahlschmelzeSpout for molten steel
- 1414
- Halteelementretaining element
- 1515
- Bodenground
- 1616
- Manipulatormanipulator
- 1717
- Auslaß StromleiterOutlet conductor
- 1818
- Anschluß KühlluftConnection cooling air
- 1919
- Stahlmantel (Verteiler)Steel jacket (distributor)
- 2020
- Heizstabheater
- 2121
- Wandung / FeuerfestauskleidungWall / refractory lining
- 2222
- Schlackenschichtslag layer
- 2323
- Gestängearm / VerstellmittelLinkage arm / adjustment means
- 2424
- Hülseshell
- 2525
- SchlackenschutzmantelSlag protective jacket
- 2626
- Hubmittellifting means
- 2727
- Schwenkmittelpivot means
- 2828
- Temperaturfühlertemperature sensor
- 2929
- Signalleitungsignal line
- 3030
- Recheneinheitcomputer unit
- 3131
- Steuerleitungcontrol line
- 3232
- Stahlgerüststeel scaffolding
- 3333
- Zuführung von WechselstromSupply of alternating current
- 3434
- Führungssäuleguide column
- 3535
- Führung guide
- 3636
- Tragelementsupporting member
- 3737
- Zwischenwandpartition
- 3838
- Kühlluft-PumpenaggregatCooling air-pump unit
- 3939
- Kühlluft-LeitungCooling air conduit
- 4040
- Bühnestage
- 4141
- Gestell ManipulatorRack manipulator
- 4242
- Soll-Wert-EingabeTarget value input
- 4343
- Hülseshell
- 4444
- Armpoor
- 4545
- Kühlfluidcooling fluid
Claims (6)
- Method of setting and/or maintaining the temperature of a melt (10), preferably a steel melt, wherein the temperature of the melt (10) in a vessel is measured, the measurement result is compared with a predeterminable temperature range in the form of target values and such an amount of heat is supplied to the melt (10) by electrical induction of an induction coil or is withdrawn from the melt (10) by means of a cooling device that the temperature of the mount lies within the target range, characterised in that for regulation of the melt temperature the induction coil (1), which is received in a refractory shaped member (24) closed at the base, is immersed in the melt (10).
- Method according to claim 1, characterised in that heat is supplied to the melt (10) directly by coupling of the induced electromagnetic alternating field.
- Method according to claim 1 or 2, characterised in that heat is supplied to the melt (10) from the wall of the shaped part (24), which in turn is coupled to the induced electromagnetic alternating field.
- Method according to claim 1, characterised in that heat is withdrawn from the melt (10) by heat conduction or heat transport from the wall of the shaped member (24).
- Method according to any one of claims 1 to 4, characterised in that the induction coil (1) is cooled from the inside and/or the outside by a cooling fluid (45), preferably air.
- Device for regulating the temperature of a melt (10), preferably a steel melt, comprising an induction coil (1) with a number of windings (3) in a refractory shaped member (24), for carrying out the method according to claims 1 to 5, characterised in that the shaped member (24) is constructed with a refractory tube (20), which can be coupled inductively, is closed at the base and receives the induction coil (1) to be exchangeable as well as a fluid cooling, in particular an air cooling, is arranged to be immersible in the melt (10) and has, at the upper end, outlets (17) for the passage of fluid-cooled current conductors (2) as well as connections (18) for the feed and discharge of optional additional cooling fluid.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19900915A DE19900915A1 (en) | 1999-01-13 | 1999-01-13 | Method and device for setting and / or maintaining the temperature of a melt, preferably a steel melt during continuous casting |
DE19900915 | 1999-01-13 | ||
PCT/EP2000/000058 WO2000041829A1 (en) | 1999-01-13 | 2000-01-07 | Method and device for controlling and/or maintaining the temperature of a melt, preferably of a steel melt during continuous casting |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1140391A1 EP1140391A1 (en) | 2001-10-10 |
EP1140391B1 true EP1140391B1 (en) | 2003-06-18 |
Family
ID=7894065
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP00901067A Expired - Lifetime EP1140391B1 (en) | 1999-01-13 | 2000-01-07 | Method and device for controlling and/or maintaining the temperature of a melt, preferably of a steel melt during continuous casting |
Country Status (13)
Country | Link |
---|---|
US (1) | US6474404B1 (en) |
EP (1) | EP1140391B1 (en) |
JP (1) | JP2002534271A (en) |
KR (1) | KR100653556B1 (en) |
CN (1) | CN1227084C (en) |
AT (1) | ATE243083T1 (en) |
AU (1) | AU2106100A (en) |
BR (1) | BR0007512A (en) |
CA (1) | CA2359339A1 (en) |
DE (2) | DE19900915A1 (en) |
EA (1) | EA003040B1 (en) |
MX (1) | MXPA01007179A (en) |
WO (1) | WO2000041829A1 (en) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10035097A1 (en) * | 2000-07-17 | 2002-02-07 | Didier Werke Ag | Immersion heating element used for changing, maintaining and/or comparing the bath temperature of a molten metal comprises an inner inductor arranged in a refractory casing having a flat cross-section and closed on its base |
TW200427972A (en) * | 2003-02-20 | 2004-12-16 | Vesuvius Crucible Co | Submerged sensor in metallurgical vessel |
FR2875513B1 (en) * | 2004-09-21 | 2006-12-08 | Electricite De France | METHOD FOR PROTECTING A THERMOPLONENGER CERAMIC SHEATH, FOR NON-FERROUS METAL BATH, AND THERMOPLONGER EQUIPPED WITH A DEVICE FOR PROTECTING THE SHEATH |
CN103338542A (en) * | 2013-07-02 | 2013-10-02 | 艾科斯(厦门)精密机械有限公司 | Electromagnetic built-in heating device |
CN106077598A (en) * | 2016-04-26 | 2016-11-09 | 重庆大学 | A kind of bath temperature adjusting means of aluminium alloy melt insulated pouring room |
CN108247030B (en) * | 2018-02-08 | 2020-02-04 | 上海东震冶金工程技术有限公司 | Intelligent continuous casting tundish induction heating control method with self-learning function |
CN113319130B (en) * | 2021-06-29 | 2022-03-15 | 燕山大学 | Continuous rolling plate temperature control method and device |
JP7005069B1 (en) * | 2021-08-19 | 2022-02-14 | 株式会社センリョウ | Plasma heating device |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SE415535B (en) * | 1978-06-13 | 1980-10-13 | Asea Ab | DEVICE FOR CONTINUOUS CASTING, LIKE STRING CASTING |
JPS6015054A (en) * | 1983-07-06 | 1985-01-25 | Ishikawajima Harima Heavy Ind Co Ltd | Device for controlling temperature of molten metal at ladle outlet |
JPS61158350U (en) * | 1985-03-25 | 1986-10-01 | ||
JPH0224510Y2 (en) * | 1985-07-10 | 1990-07-05 | ||
JPS62203666A (en) * | 1986-02-28 | 1987-09-08 | Kurosaki Refract Co Ltd | Nozzle for pouring molten metal and its production |
JPH02207949A (en) * | 1989-02-09 | 1990-08-17 | Sumitomo Heavy Ind Ltd | Device for controlling temperature of molten metal in tundish |
JPH02263545A (en) * | 1989-04-04 | 1990-10-26 | Sumitomo Metal Ind Ltd | Device for heating molten metal in tundish |
JPH02263544A (en) * | 1989-04-04 | 1990-10-26 | Aichi Steel Works Ltd | Heater device for submerging into molten metal |
JPH0673723B2 (en) * | 1989-10-02 | 1994-09-21 | 住友金属工業株式会社 | Tundish refining equipment |
JP2969731B2 (en) * | 1990-02-20 | 1999-11-02 | 日本鋼管株式会社 | Heating method of molten steel in tundish |
US5084089A (en) * | 1990-02-21 | 1992-01-28 | Julian Zekely | Method for in-line induction heating of molten metals for supplying continuous casting devices |
JPH0639503A (en) * | 1991-06-27 | 1994-02-15 | Aichi Steel Works Ltd | Method for control-heating molten steel in continuous casting process |
JPH0679422A (en) * | 1991-07-29 | 1994-03-22 | Kawasaki Steel Corp | Method for continuously measuring molten steel temperature in tundish |
DE19526970C2 (en) * | 1995-07-25 | 2000-11-16 | Didier Werke Ag | Process for induction heating of a refractory molded part |
US5902509A (en) * | 1995-07-25 | 1999-05-11 | Dider-Werke Ag | Method and apparatus for inductively heating a refractory shaped member |
US6043472A (en) * | 1996-08-28 | 2000-03-28 | Didier-Werke Ag | Assembly of tapping device and inductor therefor |
CA2181215A1 (en) * | 1995-08-28 | 1997-03-01 | Raimund Bruckner | Method of operating an inductor and inductor for carrying out the method |
DE19752548A1 (en) * | 1997-11-27 | 1999-06-10 | Schloemann Siemag Ag | Adjusting and maintaining the temperature of a steel melt during continuous casting |
-
1999
- 1999-01-13 DE DE19900915A patent/DE19900915A1/en not_active Withdrawn
-
2000
- 2000-01-07 EP EP00901067A patent/EP1140391B1/en not_active Expired - Lifetime
- 2000-01-07 JP JP2000593430A patent/JP2002534271A/en active Pending
- 2000-01-07 KR KR1020017008661A patent/KR100653556B1/en not_active IP Right Cessation
- 2000-01-07 CN CNB00802717XA patent/CN1227084C/en not_active Expired - Fee Related
- 2000-01-07 US US09/869,739 patent/US6474404B1/en not_active Expired - Fee Related
- 2000-01-07 WO PCT/EP2000/000058 patent/WO2000041829A1/en active IP Right Grant
- 2000-01-07 AT AT00901067T patent/ATE243083T1/en not_active IP Right Cessation
- 2000-01-07 CA CA002359339A patent/CA2359339A1/en not_active Abandoned
- 2000-01-07 BR BR0007512-4A patent/BR0007512A/en not_active Application Discontinuation
- 2000-01-07 EA EA200100769A patent/EA003040B1/en not_active IP Right Cessation
- 2000-01-07 MX MXPA01007179A patent/MXPA01007179A/en not_active IP Right Cessation
- 2000-01-07 DE DE50002580T patent/DE50002580D1/en not_active Expired - Lifetime
- 2000-01-07 AU AU21061/00A patent/AU2106100A/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
KR20010101431A (en) | 2001-11-14 |
CA2359339A1 (en) | 2000-07-20 |
WO2000041829A1 (en) | 2000-07-20 |
AU2106100A (en) | 2000-08-01 |
EA200100769A1 (en) | 2002-04-25 |
DE19900915A1 (en) | 2000-07-20 |
MXPA01007179A (en) | 2005-07-01 |
US6474404B1 (en) | 2002-11-05 |
EP1140391A1 (en) | 2001-10-10 |
EA003040B1 (en) | 2002-12-26 |
KR100653556B1 (en) | 2006-12-04 |
CN1227084C (en) | 2005-11-16 |
JP2002534271A (en) | 2002-10-15 |
CN1352582A (en) | 2002-06-05 |
DE50002580D1 (en) | 2003-07-24 |
BR0007512A (en) | 2001-11-20 |
ATE243083T1 (en) | 2003-07-15 |
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