EP0765702B1 - Immersion nozzle for introducing liquid metal into a continuous casting mould - Google Patents
Immersion nozzle for introducing liquid metal into a continuous casting mould Download PDFInfo
- Publication number
- EP0765702B1 EP0765702B1 EP96401849A EP96401849A EP0765702B1 EP 0765702 B1 EP0765702 B1 EP 0765702B1 EP 96401849 A EP96401849 A EP 96401849A EP 96401849 A EP96401849 A EP 96401849A EP 0765702 B1 EP0765702 B1 EP 0765702B1
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- EP
- European Patent Office
- Prior art keywords
- nozzle
- metal
- obstacle
- liquid metal
- tubular
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/10—Supplying or treating molten metal
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/06—Continuous casting of metals, i.e. casting in indefinite lengths into moulds with travelling walls, e.g. with rolls, plates, belts, caterpillars
- B22D11/0637—Accessories therefor
- B22D11/064—Accessories therefor for supplying molten metal
- B22D11/0642—Nozzles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D41/00—Casting melt-holding vessels, e.g. ladles, tundishes, cups or the like
- B22D41/50—Pouring-nozzles
- B22D41/502—Connection arrangements; Sealing means therefor
Definitions
- the invention relates to the continuous casting of metals, in particular steel. More specifically, it relates to tubes made of refractory material called "nozzles" which, usually are connected by their upper end to the container used for liquid metal reservoir, the lower end of which dips into the metal bath liquid contained in the ingot mold where the solidification of the product must begin metallic.
- nozzles tubes made of refractory material which, usually are connected by their upper end to the container used for liquid metal reservoir, the lower end of which dips into the metal bath liquid contained in the ingot mold where the solidification of the product must begin metallic.
- the primary role of these nozzles is to protect from oxidation atmospheric the jet of liquid metal on its path between the container and the mold. They also allow, thanks to appropriate configurations of their end lower, to favorably direct the flow of liquid metal in the mold so that the solidification of the product takes place under the best possible conditions.
- the casting can take place in an ingot mold which must give the product a very elongated rectangular section, which usually designates it by the expression "flat product”.
- This is the case when, in the steel industry, steel is poured under slab shape, i.e. products about 1 to 2 m wide and a thickness generally of the order of 20 cm, but which can go down to a few cm on certain recent installations called “thin slab casting machines”.
- the ingot mold is composed of fixed walls which are energetically cooled on their face which is not in contact with metal. We are also experimenting with installations making it possible to obtain, directly by solidification of the liquid metal, steel strips a few mm thick.
- the casting space is delimited on its long sides by a pair of cooled cylinders internally with parallel horizontal axes and rotating around these axes in a direction inverses, and on its short sides by closing plates (called lateral faces) made of refractory material applied against the ends of the cylinders.
- Cylinders can also be replaced by cooled endless belts.
- the first part is composed of a cylindrical tube whose upper end is connected to an opening in the bottom of the distributor which constitutes the reserve of liquid steel feeding the ingot mold, orifice which can be closed at will by the operator, partially or totally, thanks to a stopper or a drawer system ensuring the regulation of the metal flow.
- the section of this orifice depends on the flow maximum of metal that can flow inside the nozzle.
- the second part fixed at the lower end of the previous tube, for example by screwing, is intended to be immersed in the bath of liquid metal present in the mold.
- She is composed a hollow element inside which opens the lower orifice of the cylindrical tube previous.
- the interior space of this hollow element has a generally elongated shape in its terminal part and is oriented substantially perpendicular to the tube.
- the hollow element is placed parallel to the long sides of the ingot mold, and the liquid metal flows into the ingot mold through two orifices made at each of the ends of the elongated end part of the hollow element, and called "hearing".
- the object of the invention is to provide metallurgists with nozzles which ensure quieter and more fluid metal flow conditions in the mold regular than the nozzles usually used when pouring products metallurgical continuously.
- the invention relates to a nozzle for the introduction of a metal liquid in a continuous metal casting ingot mold, of the type comprising a first tubular part, one end of which is intended to be connected to a container containing said liquid metal, and the other end of which opens into a second hollow part, at least a portion of the interior space of which is oriented substantially perpendicular to said first tubular part, said portion comprising at each of its ends at least one orifice intended to open into the casting space of said ingot mold, characterized in that it comprises an obstacle placed on the path of the liquid metal inside said first tubular part or in its extension, said obstacle consisting of at least one perforated part intended to divert the metal from its preferential path inside the nozzle.
- said obstacle consists of at minus one patch perforated by a multiplicity of holes.
- said obstacle consists of a hollow part, provided with a bottom, penetrating into the interior space of said second part of the nozzle, said hollow part having openings on its side wall.
- the interior space of the assembly of the nozzle has the general shape of a T.
- the invention consists in interposing on the course of the liquid metal an obstacle intended to impede its natural flow, by deviating brutally this flow of its theoretical preferential trajectory and by reducing locally the section of space available for the passage of metal.
- This has the effect, at equal metal flow, limit the speed of flow and improve filling of the interior space of the nozzle as a whole. This reduces variations erratic in the conditions of the flow of metal out of the nozzle, and the symmetry of the flows in the right and left halves of the mold and the regularity in time of these flows are significantly improved.
- the nozzle 1 is formed, as in the previously cited prior art, of two main parts made of a refractory material such as graphite alumina, which here are assembled to each other by screwing the first into the second.
- the first part comprises a cylindrical or substantially cylindrical tube 2, of which the interior space 3 constitutes the path for the passage of the liquid metal.
- This tube 2 is normally intended to be held vertically.
- Its upper part no shown is intended to be connected to a container serving as a metal reservoir liquid, such as a continuous flow distributor, at an orifice through which the metal liquid can flow with a flow that the operator regulates by means of a stopper or of a drawer device.
- the lower end 4 of the tube 2 has a thread 5 on its outer wall, and this thread 5 makes it possible to assemble it to the second part of the nozzle 1.
- This second part is composed of a hollow element 6 which, in the example described and shown, externally has the shape of an inverted T.
- Interior space 7 of the hollow element 6, also in the form of an inverted T thus comprises a portion cylindrical 8 extending the interior space 3 of the tube 2.
- the upper zone of this cylindrical portion 8 has a flare 9, the wall of which is threaded, so as to ability to screw the lower end 4 of the tube 2.
- the cylindrical portion 8 opens out in a tubular portion 10 which is substantially perpendicular thereto, of section approximately circular, oval or rectangular.
- Each end of this tubular portion 29 has an orifice 11, 11 'called "hearing", through which the metal liquid can flow out of the nozzle.
- these vents 10, 11 are intended to be permanently maintained under the surface of the filling liquid metal casting space.
- the cylindrical portion 8 of the interior space 7 of the element hollow 6 has, inside the flare 9 and under the thread of its wall, a housing 12, in which, prior to the assembly of the two parts 2, 6 of the nozzle 1, a stack of three pellets of refractory material can be placed: a upper pad 13, an intermediate pad 14 and a lower pad 15.
- the respective dimensions of the housing 12 and the pads 13, 14, 15 are chosen such that so that, after assembly of the nozzle 1, the lower end of the tube 2 comes in abutment against the upper pad 13.
- the upper pad 13 has a certain number of perforations 16, distributed over the portion of its surface intended to be located at plumb with the interior space 3 of the tube 2.
- the intermediate patch 14 has a single perforation 17 of shape, for example, square or circular, opening at less equal to that of the interior space 3 of the tube 2. Its role is, in fact, that of a spacer used to separate the upper 13 and lower 15 pellets. also has a number of perforations 18, which may be different in number and in size of the perforations 16 of the upper patch 13. But it is important, for obtaining the desired results, that the perforations 16 and 18 are noticeably offset from each other, so that a fraction as small as possible of the liquid metal has the theoretical possibility of cross the obstacle constituted by all the pellets 13, 14, 15 without hitting them. For a better obstacle efficiency, it is also preferable that the tablet upper 13 does not have a perforation in its center, where the probability of presence of liquid metal is most important, so as to slow down the pouring jet as early as possible.
- the total section of the orifices of a given patch should not not be less than the cross section of the distributor outlet, to ensure that we can always sink with a maximum metal flow as high as in the absence obstacle.
- the bottom 19 of the hollow element 6 is equipped with perforations 20 called “leak holes”.
- These leakage holes 20 have for usual functions of deflecting part of the metal flows towards the lower part of the mold. This deviation limits the flow rate and the exit speed of the metal at the gills 11, 11 ′ and thus prevents the metal from hitting violently the small sides of the mold and disturb the conditions of solidification. In the case of casting between cylinders, this also makes it possible to avoid excessive deterioration of the refractory side faces.
- these holes leak 20 ensure a regular supply of hot metal to the lower part of the casting space, directly above the nozzle 1: here again, this goes in the direction of better control of solidification conditions.
- the pellets must be made of a refractory material such as zirconia, in any case compatible with the nature of the cast metal to prevent them from being excessively chemically attacked by the metal.
- pellet obstacle which has just been described is not than a non-limiting example.
- the obstacle inserted in the nozzle 1 is constituted by a tubular part 21, provided with a bottom 22 at one of its ends. At its end open, this tubular part 21 has a shoulder 23 which can be inserted in the housing 12 formed in the hollow element 6 and which contained the pellets 13, 14, 15 in the example of implementation of the preceding invention.
- the tubular part 21 On its side wall 24, the tubular part 21 has perforations 25, 26, 27 which allow the metal liquid to pass from the interior space 28 of the tubular part 21 to the interior space 7 of the hollow element 6, after having lost a large part of its potential energy.
- these perforations 25, 26, 27 are the number of six distributed in three levels over the height of the tubular piece 21, and are shaped approximately oval. They preferentially make it possible to orient the liquid metal on the side wall of the cylindrical portion 8 of the interior space 7 of the hollow element 6. In this way, the impact of the metal against this side wall provides absorption of energy which is added to that undergone inside the tubular part 21. Similarly, for obtain a residence time of the metal in the nozzle 1 as long and uniform as possible, it is preferable that, as shown, the orientation of these perforations is perpendicular to the orientation of the vents 11, 11 '.
- a tubular piece 21, the interior space 28 of which would have a length of 84 mm, diameter of 30 mm, perforations 25, 26, 27 of 10x20 mm, have an influence on the speed and regularity of metal flows substantially comparable to that of the pellets 13, 14, 15 of the obstacle described and shown in Figures 1a to 1d, if it was inserted into an identical nozzle 1.
- the invention is not limited in its application to the field of casting continues flat steel products (slabs, thin slabs, thin strips), even if it finds there a privileged application. It can be applied to many others examples of continuous casting nozzles of all metals in all formats, for which one wishes to obtain a slowing down of the flows providing a better filling of the nozzle and, consequently, greater stability of the flows of the liquid metal coming out of it.
Abstract
Description
L'invention concerne la coulée continue des métaux, notamment de l'acier. Plus précisément, elle concerne les tubes en matériau réfractaire dits "busettes" qui, habituellement, sont connectés par leur extrémité supérieure au récipient servant de réservoir de métal liquide, et dont l'extrémité inférieure plonge dans le bain de métal liquide contenu dans la lingotière où doit s'amorcer la solidification du produit métallique. Le premier rôle de ces busettes est de protéger de l'oxydation atmosphérique le jet de métal liquide sur son parcours entre le récipient et la lingotière. Elles permettent également, grâce à des configurations appropriées de leur extrémité inférieure, d'orienter favorablement les écoulements du métal liquide dans la lingotière pour que la solidification du produit s'effectue dans les meilleures conditions possibles.The invention relates to the continuous casting of metals, in particular steel. More specifically, it relates to tubes made of refractory material called "nozzles" which, usually are connected by their upper end to the container used for liquid metal reservoir, the lower end of which dips into the metal bath liquid contained in the ingot mold where the solidification of the product must begin metallic. The primary role of these nozzles is to protect from oxidation atmospheric the jet of liquid metal on its path between the container and the mold. They also allow, thanks to appropriate configurations of their end lower, to favorably direct the flow of liquid metal in the mold so that the solidification of the product takes place under the best possible conditions.
La coulée peut avoir lieu dans une lingotière devant conférer au produit une section de forme rectangulaire très allongée, qui le fait désigner habituellement par l'expression "produit plat". C'est le cas lorsque, en sidérurgie, on coule l'acier sous forme de brames, c'est à dire de produits ayant environ 1 à 2 m de large et une épaisseur généralement de l'ordre de 20 cm, mais pouvant descendre jusqu'à quelques cm sur certaines installations récentes dites "machines de coulée de brames minces". Dans ces exemples, la lingotière est composée de parois fixes énergiquement refroidies sur leur face qui n'est pas au contact du métal. On expérimente également des installations permettant d'obtenir, directement par solidification du métal liquide, des bandes d'acier de quelques mm d'épaisseur. Pour ce faire, on utilise des lingotières dont l'espace de coulée est délimité sur ses grands côtés par une paire de cylindres refroidis intérieurement à axes horizontaux parallèles et tournant autour de ces axes en sens inverses, et sur ses petits côtés par des plaques de fermeture (appelées faces latérales) en matériau réfractaire appliquées contre les extrémités des cylindres. Les cylindres peuvent également être remplacés par des bandes sans fin refroidies.The casting can take place in an ingot mold which must give the product a very elongated rectangular section, which usually designates it by the expression "flat product". This is the case when, in the steel industry, steel is poured under slab shape, i.e. products about 1 to 2 m wide and a thickness generally of the order of 20 cm, but which can go down to a few cm on certain recent installations called "thin slab casting machines". In these examples, the ingot mold is composed of fixed walls which are energetically cooled on their face which is not in contact with metal. We are also experimenting with installations making it possible to obtain, directly by solidification of the liquid metal, steel strips a few mm thick. To do this, we use ingot molds, the casting space is delimited on its long sides by a pair of cooled cylinders internally with parallel horizontal axes and rotating around these axes in a direction inverses, and on its short sides by closing plates (called lateral faces) made of refractory material applied against the ends of the cylinders. Cylinders can also be replaced by cooled endless belts.
Dans ces types de lingotière, on considère qu'il est préférable d'orienter les écoulements du métal liquide de manière privilégiée en direction des petits côtés de l'espace de coulée. On cherche ainsi, notamment, à obtenir une homogénéisation thermique du métal de manière à atténuer les variations de l'épaisseur solidifiée selon le périmètre de la lingotière. Cette homogénéisation thermique et l'agitation du bain liquide qu'elle nécessite sont particulièrement cruciales dans le cas de la coulée de bandes minces, du fait de l'utilisation des faces latérales en réfractaire. En effet, si on n'assurait pas un renouvellement forcé du métal avoisinant ces faces latérales, ce métal se refroidirait de manière anormalement intense, et on verrait apparaítre des solidifications de métal indésirables sur les faces latérales. In these types of ingot mold, it is considered preferable to orient the liquid metal flows favorably towards the short sides of casting space. We thus seek, in particular, to obtain a homogenization thermal of the metal so as to attenuate variations in the solidified thickness depending on the perimeter of the mold. This thermal homogenization and agitation of the bath liquid it requires are particularly crucial in the case of pouring thin strips, due to the use of the refractory side faces. Indeed, if we did not ensure a forced renewal of the metal surrounding these lateral faces, this metal would cool abnormally intensely, and we would see undesirable metal solidifications on the lateral faces.
Pour obtenir l'homogénéisation désirée, on utilise parfois, notamment en coulée entre cylindres, des busettes en deux parties (voir le document JP-A-60021171). La première partie est composée d'un tube cylindrique dont l'extrémité supérieure est connectée à un orifice pratiqué dans le fond du répartiteur qui constitue la réserve d'acier liquide alimentant la lingotière, orifice qui est obturable à volonté par l'opérateur, partiellement ou totalement, grâce à une quenouille ou un système à tiroir assurant la régulation du débit de métal. De la section de cet orifice dépend le débit maximal de métal qui peut s'écouler à l'intérieur de la busette. La deuxième partie, fixée à l'extrémité inférieure du tube précédent, par exemple par vissage, est destinée à être immergée dans le bain de métal liquide présent dans la lingotière. Elle est composée d'un élément creux à l'intérieur duquel débouche l'orifice inférieur du tube cylindrique précédent. L'espace intérieur de cet élément creux a une forme générale allongée dans sa partie terminale et est orienté sensiblement perpendiculairement au tube. Lorsque la busette est en service, l'élément creux est placé parallèlement aux grands côtés de la lingotière, et le métal liquide s'écoule dans la lingotière par deux orifices pratiqués à chacune des extrémités de la partie terminale allongée de l'élément creux, et appelés "ouïes".To obtain the desired homogenization, it is sometimes used, in particular in casting between cylinders, two-part nozzles (see document JP-A-60021171). The first part is composed of a cylindrical tube whose upper end is connected to an opening in the bottom of the distributor which constitutes the reserve of liquid steel feeding the ingot mold, orifice which can be closed at will by the operator, partially or totally, thanks to a stopper or a drawer system ensuring the regulation of the metal flow. The section of this orifice depends on the flow maximum of metal that can flow inside the nozzle. The second part, fixed at the lower end of the previous tube, for example by screwing, is intended to be immersed in the bath of liquid metal present in the mold. She is composed a hollow element inside which opens the lower orifice of the cylindrical tube previous. The interior space of this hollow element has a generally elongated shape in its terminal part and is oriented substantially perpendicular to the tube. When the nozzle is in service, the hollow element is placed parallel to the long sides of the ingot mold, and the liquid metal flows into the ingot mold through two orifices made at each of the ends of the elongated end part of the hollow element, and called "hearing".
Lorsqu'un débit d'acier important, de l'ordre par exemple de 60 t/h, circule à l'intérieur de la busette, la vitesse du métal dans la partie tubulaire atteint facilement plusieurs mètres par seconde. Dans ces conditions, on n'observe qu'un remplissage très partiel de la section de la partie cylindrique de la busette par le métal liquide. Ce mauvais remplissage a plusieurs inconvénients. En premier lieu, par un "effet de trompe", il tend à favoriser l'aspiration d'air extérieur par les porosités du réfractaire et les éventuels défauts d'étanchéité de la connection entre la busette et le répartiteur, ce qui détériore la qualité du métal. D'autre part, surtout lorsque le dispositif obturant le fond du répartiteur n'est que partiellement ouvert, l'écoulement du métal est tournoyant et irrégulier. Cela conduit à une forte instabilité des courants de métal sortant des ouïes, instabilité qui est encore accrue lorsqu'on insuffle un gaz neutre dans la busette pour atténuer le premier inconvénient que l'on a cité. On peut ainsi observer des dissymétries dans les écoulements qui s'établissent sur les portions droite et gauche de la lingotière. Cette instabilité et cette dissymétrie provoquent l'apparition de vagues à l'intérieur du bain de métal liquide en lingotière qui font varier en permanence le niveau de sa surface, ce qui est très défavorable à la régularité de la solidification du produit. Ces vagues font également réagir indûment le dispositif assurant la détection du niveau de la surface et la régulation de sa position: il va chercher à compenser ce qu'il prend pour des variations du niveau moyen du métal en commandant des modifications rapides et continues du degré d'ouverture de la quenouille ou du tiroir. Et ces modifications incessantes vont, en fait, aggraver les instabilités du niveau de métal. Enfin, les vitesses élevées du métal liquide dans la busette favorisent l'usure des matériaux réfractaires qui la constituent, en particulier au point d'impact du jet sur le fond de l'élément creux horizontal.When a significant steel flow, for example of the order of 60 t / h, circulates at inside the nozzle, the speed of the metal in the tubular part easily reaches several meters per second. Under these conditions, we observe only a very filling partial of the section of the cylindrical part of the nozzle by the liquid metal. This improper filling has several disadvantages. First, by an "effect of ", it tends to favor the suction of outside air through the porosities of the refractory and any leaks in the connection between the nozzle and the distributor, this which deteriorates the quality of the metal. On the other hand, especially when the device closing the bottom of the distributor is only partially open, the flow of metal is swirling and irregular. This leads to a high instability of the metal currents leaving the gills, instability which is further increased when a neutral gas is blown into the nozzle to alleviate the first disadvantage that we mentioned. We can thus observe asymmetries in the flows which are established on the right and left portions of the ingot mold. This instability and this asymmetry cause waves to appear. the interior of the liquid metal bath in an ingot mold which permanently varies the level of its surface, which is very unfavorable to the regularity of the solidification of the product. These waves also cause the device detecting the level to react unduly. of the surface and the regulation of its position: it will seek to compensate for what it takes for variations in the average level of the metal when ordering modifications rapid and continuous opening of the stopper or the drawer. And these Continuous changes will, in fact, worsen the instabilities of the metal level. Finally, the high speeds of the liquid metal in the nozzle favor the wear of the refractory materials which constitute it, in particular at the point of impact of the jet on the bottom of the horizontal hollow element.
Le but de l'invention est de procurer aux métallurgistes des busettes qui assurent des conditions d'écoulement du métal dans la lingotière plus calmes et plus régulières que les busettes habituellement employées lors de la coulée de produits métallurgiques en continu.The object of the invention is to provide metallurgists with nozzles which ensure quieter and more fluid metal flow conditions in the mold regular than the nozzles usually used when pouring products metallurgical continuously.
A cet effet, l'invention a pour objet une busette pour l'introduction d'un métal liquide dans une lingotière de coulée continue des métaux, du type comportant une première partie tubulaire, dont une extrémité est destinée à être connectée à un récipient renfermant ledit métal liquide, et dont l'autre extrémité débouche dans une deuxième partie creuse, dont au moins une portion de l'espace intérieur est orientée sensiblement perpendiculairement à ladite première partie tubulaire, ladite portion comportant à chacune de ses extrémités au moins un orifice destiné à déboucher dans l'espace de coulée de ladite lingotière, caractérisée en ce qu'elle comporte un obstacle placé sur le parcours du métal liquide à l'intérieur de ladite première partie tubulaire ou dans son prolongement, ledit obstacle étant constitué par au moins une pièce perforée destinée à dévier le métal de sa trajectoire préférentielle à l'intérieur de la busette.To this end, the invention relates to a nozzle for the introduction of a metal liquid in a continuous metal casting ingot mold, of the type comprising a first tubular part, one end of which is intended to be connected to a container containing said liquid metal, and the other end of which opens into a second hollow part, at least a portion of the interior space of which is oriented substantially perpendicular to said first tubular part, said portion comprising at each of its ends at least one orifice intended to open into the casting space of said ingot mold, characterized in that it comprises an obstacle placed on the path of the liquid metal inside said first tubular part or in its extension, said obstacle consisting of at least one perforated part intended to divert the metal from its preferential path inside the nozzle.
Selon une première variante de l'invention, ledit obstacle est constitué par au moins une pastille perforée par une multiplicité de trous.According to a first variant of the invention, said obstacle consists of at minus one patch perforated by a multiplicity of holes.
Selon une deuxième variante de l'invention, ledit obstacle est constitué par une pièce creuse, munie d'un fond, pénétrant dans l'espace intérieur de ladite deuxième partie de la busette, ladite pièce creuse comportant des ouvertures sur sa paroi latérale.According to a second variant of the invention, said obstacle consists of a hollow part, provided with a bottom, penetrating into the interior space of said second part of the nozzle, said hollow part having openings on its side wall.
Dans une forme de réalisation de l'invention, l'espace intérieur de l'ensemble de la busette a la forme générale d'un T.In one embodiment of the invention, the interior space of the assembly of the nozzle has the general shape of a T.
Comme on l'aura compris, l'invention consiste à interposer sur le parcours du métal liquide un obstacle destiné à contrarier son écoulement naturel, en déviant brutalement cet écoulement de sa trajectoire préférentielle théorique et en réduisant localement la section de l'espace disponible pour le passage du métal. Cela a pour effet, à débit de métal égal, de limiter la vitesse de l'écoulement et d'améliorer le remplissage de l'espace intérieur de la busette dans son ensemble. On atténue ainsi les variations erratiques dans les conditions de l'écoulement du métal hors de la busette, et la symétrie des écoulements dans les moitiés droite et gauche de la lingotière et la régularité dans le temps de ces écoulements sont notablement améliorées.As will be understood, the invention consists in interposing on the course of the liquid metal an obstacle intended to impede its natural flow, by deviating brutally this flow of its theoretical preferential trajectory and by reducing locally the section of space available for the passage of metal. This has the effect, at equal metal flow, limit the speed of flow and improve filling of the interior space of the nozzle as a whole. This reduces variations erratic in the conditions of the flow of metal out of the nozzle, and the symmetry of the flows in the right and left halves of the mold and the regularity in time of these flows are significantly improved.
L'invention sera mieux comprise à la lecture de la description qui suit, donnée en référence aux figures annexées suivantes:
- la figure 1a qui schématise, vue en coupe longitudinale, une première variante de l'invention, où l'obstacle est constitué par un empilement de pastilles perforées, qui sont elle-mêmes représentées en vue de dessus sur les figures 1b, 1c et 1d;
- la figure 2 qui schématise, vue en coupe longitudinale, une seconde variante de l'invention, où l'obstacle est constitué par une pièce creuse prolongeant la première partie tubulaire de la busette et orientant le métal vers les parois latérales de la deuxième partie de la busette.
- FIG. 1a which schematically shows, in longitudinal section, a first variant of the invention, where the obstacle consists of a stack of perforated pellets, which are themselves shown in plan view in FIGS. 1b, 1c and 1d ;
- Figure 2 which shows schematically, in longitudinal section, a second variant of the invention, where the obstacle is constituted by a hollow part extending the first tubular part of the nozzle and orienting the metal towards the side walls of the second part of the nozzle.
Dans un premier exemple de mise en oeuvre de l'invention, représenté sur les
figures 1a-1d, la busette 1 est formée, comme dans l'Art Antérieur précédemment cité,
de deux parties principales en un matériau réfractaire tel que de l'alumine graphitée, qui
sont ici assemblées l'une à l'autre par vissage de la première dans la seconde. La
première partie comprend un tube 2 cylindrique ou sensiblement cylindrique, dont
l'espace intérieur 3 constitue le chemin de passage du métal liquide. Ce tube 2 est
normalement destiné à être maintenu verticalement. Sa partie supérieure non
représentée est destinée à être connectée à un récipient servant de réservoir de métal
liquide, tel qu'un répartiteur de coulée continue, au droit d'un orifice par lequel le métal
liquide peut s'écouler avec un débit que l'opérateur règle au moyen d'une quenouille ou
d'un dispositif à tiroir. L'extrémité inférieure 4 du tube 2 comporte un filetage 5 sur sa
paroi externe, et ce filetage 5 permet de l'assembler à la deuxième partie de la busette
1. Cette deuxième partie est composée d'un élément creux 6 qui, dans l'exemple décrit
et représenté, a extérieurement la forme d'un T inversé. L'espace intérieur 7 de
l'élément creux 6, lui aussi en forme de T inversé, comporte ainsi une portion
cylindrique 8 prolongeant l'espace intérieur 3 du tube 2. La zone supérieure de cette
portion cylindrique 8 comporte un évasement 9 dont la paroi est filetée, de manière à
pouvoir y visser l'extrémité inférieure 4 du tube 2. La portion cylindrique 8 débouche
dans une portion tubulaire 10 qui lui est sensiblement perpendiculaire, de section
approximativement circulaire, ovale ou rectangulaire. Chaque extrémité de cette
portion tubulaire 29 comporte un orifice 11, 11' appelé "ouïe", par lequel le métal
liquide peut s'écouler hors de la busette. Pendant la coulée, ces ouïes 10, 11 sont
destinées à être maintenues en permanence sous la surface du métal liquide remplissant
l'espace de coulée.In a first example of implementation of the invention, shown in the
FIGS. 1a-1d, the
Selon l'invention, la portion cylindrique 8 de l'espace intérieur 7 de l'élément
creux 6 comporte, à l'intérieur de l'évasement 9 et sous le filetage de sa paroi, un
logement 12, dans lequel, préalablement à l'assemblage des deux parties 2, 6 de la
busette 1, on peut placer un empilement de trois pastilles en matériau réfractaire: une
pastille supérieure 13, une pastille intermédiaire 14 et une pastille inférieure 15. Les
dimensions respectives du logement 12 et des pastilles 13, 14, 15 sont choisies de telle
manière que, après assemblage de la busette 1, l'extrémité inférieure du tube 2 vienne
en butée contre la pastille supérieure 13. La pastille supérieure 13 comporte un certain
nombre de perforations 16, réparties sur la portion de sa surface destinée à être située à
l'aplomb de l'espace intérieur 3 du tube 2. La pastille intermédiaire 14 comporte une
perforation unique 17 de forme, par exemple, carrée ou circulaire, d'ouverture au
moins égale à celle de l'espace intérieur 3 du tube 2. Son rôle est, en fait, celui d'une
entretoise servant à séparer les pastilles supérieure 13 et inférieure 15. Celle-ci
comporte également un certain nombre de perforations 18, qui peuvent être différentes
en nombre et en dimension des perforations 16 de la pastille supérieure 13. Mais il est
important, pour l'obtention des résultats recherchés, que les perforations 16 et 18
soient sensiblement décalées les unes par rapport aux autres, de manière à ce qu'une
fraction aussi réduite que possible du métal liquide ait la possibilité théorique de
franchir l'obstacle constitué par l'ensemble des pastilles 13, 14, 15 sans les heurter.
Pour une meilleure efficacité de l'obstacle, il est également préférable que la pastille
supérieure 13 ne comporte pas de perforation en son centre, là où la probabilité de
présence de métal liquide est la plus importante, de manière à freiner le jet de coulée
aussi précocément que possible.According to the invention, the
De manière générale, la section totale des orifices d'une pastille donnée ne doit pas être inférieure à la section de l'orifice de sortie du répartiteur, afin de garantir que l'on pourra toujours couler avec un débit maximal de métal aussi élevé qu'en l'absence d'obstacle.In general, the total section of the orifices of a given patch should not not be less than the cross section of the distributor outlet, to ensure that we can always sink with a maximum metal flow as high as in the absence obstacle.
Optionnellement, comme il est déjà connu, le fond 19 de l'élément creux 6 est
équipé de perforations 20 appelées "trous de fuite". Ces trous de fuite 20 ont pour
fonctions habituelles de dévier une partie des écoulements de métal en direction de la
partie inférieure de la lingotière. Cette déviation limite le débit et la vitesse de sortie du
métal au niveau des ouïes 11, 11' et évite ainsi que le métal ne vienne percuter
violemment les petits côtés de la lingotière et y perturber les conditions de
solidification. Dans le cas d'une coulée entre cylindres, cela permet également d'éviter
une détérioration excessive des faces latérales en réfractaire. D'autre part, ces trous de
fuite 20 assurent une alimentation régulière en métal chaud de la partie inférieure de
l'espace de coulée, à l'aplomb de la busette 1: là encore, cela va dans le sens d'une
meilleure maítrise des conditions de solidification. L'utilisation d'obstacles selon
l'invention permet de profiter au maximum des avantages procurés par les trous de fuite
20, dans la mesure où ces trous de fuite 20 sont d'autant plus efficaces que les
écoulements à l'intérieur de la busette 1, et en particulier dans l'élément creux 6, sont
plus réguliers. Cela permet, notamment, d'atténuer l'écoulement préférentiel du métal
par les trous de fuite 20 qui sont les plus proches de l'axe de la busette.Optionally, as is already known, the bottom 19 of the
A titre d'exemple, on peut proposer, pour une busette 1 dont le diamètre intérieur du tube 2 est de 60 mm, et dont les ouïes 11, 11' de l'élément creux ont une section circulaire et un diamètre de 30 mm, d'utiliser un obstacle formé de trois pastilles 13, 14, 15 de diamètre extérieur 100 mm et d'épaisseur 25 mm, ayant les caractéristiques suivantes:
la pastille supérieure 13 possède huit perforations 16 de diamètre 13 mm, réparties en deux rangées de trois perforations séparées par une rangée de deux perforations;- la pastille intermédiaire 14 possède une perforation unique 17 ayant une section carrée de 60 mm de côté, ou une section circulaire de 60 mm de diamètre;
- la pastille inférieure 15 possède cinq perforations 18 de diamètre 19 mm, à savoir une perforation centrale entourée par quatre perforations disposées en carré.
- the
upper pad 13 has eightperforations 16 ofdiameter 13 mm, distributed in two rows of three perforations separated by a row of two perforations; - the
intermediate patch 14 has asingle perforation 17 having a square section of 60 mm on the side, or a circular section of 60 mm in diameter; - the
lower pad 15 has fiveperforations 18 ofdiameter 19 mm, namely a central perforation surrounded by four perforations arranged in a square.
Dans cet exemple, lors de la coulée d'acier liquide, si le métal traverse la
busette 1 avec un débit de 60 t/h, en l'absence d'obstacle il ne remplit que partiellement
l'espace intérieur du tube 2. Mais l'obstacle que l'on vient de décrire est suffisant pour
freiner l'écoulement de l'acier liquide de manière à réduire sa vitesse à environ 1 m/s, et
à obtenir un bon remplissage du tube 2, ainsi qu'une vitesse de sortie du métal régulière
et assez sensiblement uniforme sur toute la section des ouïes 11, 11', pour ce même
débit de métal de 60 t/h. Cela procure une stabilité satisfaisante du niveau du métal
dans la lingotière lorsqu'on ne modifie pas le débit du métal traversant la busette 1.In this example, when pouring liquid steel, if the metal crosses the
Les pastilles doivent être en un matériau réfractaire tel que de la zircone, en tout cas compatible avec la nature du métal coulé pour éviter qu'elles ne soient attaquées chimiquement par le métal de manière excessive.The pellets must be made of a refractory material such as zirconia, in any case compatible with the nature of the cast metal to prevent them from being excessively chemically attacked by the metal.
Bien entendu, le type précis d'obstacle à pastilles qui vient d'être décrit n'est
qu'un exemple non limitatif. On peut imaginer, notamment de n'utiliser qu'une seule
pastille perforée si cela s'avère suffisant pour obtenir un résultat acceptable dans des
conditions de coulée usuelles, ou au contraire d'utiliser plus de trois pastilles pour
accentuer l'effet de freinage du jet de coulée. De même, la présence d'une pastille
intermédiaire 14 à large perforation unique 17, ne servant donc que d'entretoise entre
deux pastilles 13, 15 à petites perforations multiples, n'est pas à proprement parler
obligatoire. Mais elle permet de limiter l'usure de la pastille inférieure 15, en évitant une
concentration exclusive des écoulements de métal sur les zones pleines de cette pastille
qui font face aux perforations de la pastille supérieure 13.Of course, the precise type of pellet obstacle which has just been described is not
than a non-limiting example. One can imagine, in particular to use only one
perforated tablet if this is sufficient to obtain an acceptable result in
usual casting conditions, or on the contrary to use more than three pellets to
accentuate the braking effect of the casting jet. Similarly, the presence of a pellet
intermediate 14 with large
Dans un deuxième exemple de mise en oeuvre de l'invention, représenté sur la
figure 2 (sur laquelle les éléments communs à ceux de la figure la sont repérés par les
mêmes signes de référence), l'obstacle inséré dans la busette 1 est constitué par une
pièce tubulaire 21, munie d'un fond 22 à l'une de ses extrémités. A son extrémité
ouverte, cette pièce tubulaire 21 comporte un épaulement 23 qui peut venir s'insérer
dans le logement 12 ménagé dans l'élément creux 6 et qui contenait les pastilles 13, 14,
15 dans l'exemple de mise en oeuvre de l'invention précédent. Sur sa paroi latérale 24,
la pièce tubulaire 21 comporte des perforations 25, 26, 27 qui permettent au métal
liquide de passer de l'espace intérieur 28 de la pièce tubulaire 21 à l'espace intérieur 7
de l'élément creux 6, après avoir perdu une grande partie de son énergie potentielle.
Dans l'exemple représenté sur la figure 2, ces perforations 25, 26, 27 sont au nombre
de six réparties en trois niveaux sur la hauteur de la pièce tubulaire 21, et sont de forme
approximativement ovale. Elles permettent préférentiellement d'orienter le métal liquide
sur la paroi latérale de la portion cylindrique 8 de l'espace intérieur 7 de l'élément creux
6. De cette manière, le choc du métal contre cette paroi latérale procure une absorption
d'énergie qui s'ajoute à celle subie à l'intérieur de la pièce tubulaire 21. De même, pour
obtenir un temps de séjour du métal dans la busette 1 aussi long et uniforme que
possible, il est préférable que, comme représenté, l'orientation de ces perforations soit
perpendiculaire à l'orientation des ouïes 11, 11'.In a second example of implementation of the invention, shown in the
Figure 2 (on which the elements common to those of Figure la are identified by the
same reference signs), the obstacle inserted in the
A titre d'exemple, une pièce tubulaire 21, dont l'espace intérieur 28 aurait une
longueur de 84 mm, un diamètre de 30 mm, des perforations 25, 26, 27 de 10x20 mm,
aurait sur la vitesse et la régularité des écoulements de métal une influence
sensiblement comparable à celle des pastilles 13, 14, 15 de l'obstacle décrit et
représenté sur les figures 1a à 1d, s'il était inséré dans une busette 1 identique.By way of example, a
Bien entendu, les exemples décrits ci-dessus ne sont pas limitatifs. On
pourrait, par exemple, imaginer d'insérer l'obstacle à l'intérieur même du tube 2, et non
pas simplement dans son prolongement. On pourrait aussi insérer dans la busette 1 une
pluralité d'obstacles similaires à ceux que l'on a décrits, ou différents dans leur forme
mais pouvant remplir les mêmes fonctions.Of course, the examples described above are not limiting. We
could, for example, imagine inserting the obstacle inside the
L'invention n'est pas limitée dans son application au domaine de la coulée continue des produits plats en acier (brames, brames minces, bandes minces), même si elle y trouve une application privilégiée. Elle peut être appliquée à bien d'autres exemples de busettes de coulée continue de tous métaux en tous formats, pour lesquelles on souhaite obtenir un ralentissement des écoulements procurant un meilleur remplissage de la busette et, partant, une plus grande stabilité des écoulements du métal liquide qui en sort.The invention is not limited in its application to the field of casting continues flat steel products (slabs, thin slabs, thin strips), even if it finds there a privileged application. It can be applied to many others examples of continuous casting nozzles of all metals in all formats, for which one wishes to obtain a slowing down of the flows providing a better filling of the nozzle and, consequently, greater stability of the flows of the liquid metal coming out of it.
Claims (8)
- Nozzle (1) for introducing a liquid metal into a mould for continuous casting of metals, of the type comprising a tubular first part (2), one end of which is intended to be connected to a receptacle enclosing the said liquid metal, and the other end (4) of which opens into a hollow second part (6) in which at least one portion (29) of the internal space (7) is oriented substantially perpendicularly to the said tubular first part (2), the said portion (29) comprising at each of its ends at least one orifice (10, 11) intended to open into the casting space of the said mould, characterized in that it comprises an obstacle placed in the path of the liquid metal inside the said tubular first part (2) or in its extension, the said obstacle consisting of at least one perforated component intended to divert the metal from its preferential trajectory inside the nozzle.
- Nozzle according to Claim 1, characterized in that the said obstacle consists of at least one disc perforated with a multiplicity of holes.
- Nozzle according to Claim 1, characterized in that the said obstacle consists of a plurality of discs (13, 15) perforated with a multiplicity of holes (16, 18) and separated from each other by other discs (14) perforated with a single hole (17) of section approaching the internal section of the said tubular first part (2).
- Nozzle according to Claim 1, characterized in that the said obstacle consists of a tubular component (21) provided with a bottom (22), intended to receive the liquid metal inside it, the said tubular component (21) comprising perforations (25, 26, 27) in its side wall (24), the said perforations (25, 26, 27) permitting the metal to pass into the internal space (7) of the said second part (6) of the nozzle (1).
- Nozzle according to Claim 4, characterized in that the said perforations (25, 26, 27) are oriented towards the inner wall of the said second part (6) of the nozzle (1).
- Nozzle according to one of Claims 1 to 5, characterized in that the said first part (2) and the said second part (6) of the nozzle (1) are assembled by screwing the first part (2) into the second part (6) and in that the said obstacle is inserted into a housing (12) arranged in the internal wall of the said second part (6).
- Nozzle according to one of Claims 1 to 6, characterized in that the said portion (29) of the internal space (7) of the second part (6) which is oriented substantially perpendicularly to the first part (2) has an elongate shape, giving the internal space of the whole of the nozzle the general form of a T.
- Nozzle according to one of Claims 1 to 7, characterized in that the bottom (19) of the hollow member (6) comprises at least one leakage hole (20).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9511375A FR2739313B1 (en) | 1995-09-28 | 1995-09-28 | NOZZLE FOR THE INTRODUCTION OF A LIQUID METAL INTO A CONTINUOUS CASTING LINGOTIERE OF METALS |
FR9511375 | 1995-09-28 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0765702A1 EP0765702A1 (en) | 1997-04-02 |
EP0765702B1 true EP0765702B1 (en) | 1999-05-26 |
Family
ID=9483001
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP96401849A Expired - Lifetime EP0765702B1 (en) | 1995-09-28 | 1996-08-29 | Immersion nozzle for introducing liquid metal into a continuous casting mould |
Country Status (24)
Country | Link |
---|---|
US (1) | US5733469A (en) |
EP (1) | EP0765702B1 (en) |
JP (1) | JP3978794B2 (en) |
KR (1) | KR100369257B1 (en) |
CN (1) | CN1064286C (en) |
AT (1) | ATE180427T1 (en) |
AU (1) | AU702389B2 (en) |
BR (1) | BR9603908A (en) |
CA (1) | CA2186084C (en) |
CZ (1) | CZ285931B6 (en) |
DE (1) | DE69602565T2 (en) |
DK (1) | DK0765702T3 (en) |
ES (1) | ES2132857T3 (en) |
FR (1) | FR2739313B1 (en) |
GR (1) | GR3030610T3 (en) |
MX (1) | MX9604288A (en) |
PL (1) | PL181356B1 (en) |
RO (1) | RO117242B1 (en) |
RU (1) | RU2163179C2 (en) |
SK (1) | SK281773B6 (en) |
TR (1) | TR199600774A2 (en) |
TW (1) | TW345508B (en) |
UA (1) | UA42764C2 (en) |
ZA (1) | ZA968126B (en) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2767082B1 (en) * | 1997-08-06 | 1999-10-29 | Vesuvius France Sa | CASTING NOZZLE FOR TRANSFERRING LIQUID METAL FROM A DISTRIBUTOR INTO A LINGOTIERE |
FR2769862B1 (en) * | 1997-10-20 | 1999-11-19 | Usinor | CASTING NOZZLE FOR CONTINUOUS CASTING OF METALS, IN PARTICULAR CASTING BETWEEN CYLINDERS |
FR2777485B1 (en) * | 1998-04-16 | 2000-05-19 | Usinor | NOZZLE FOR INTRODUCING LIQUID METAL INTO A CONTINUOUS CASTING LINGOTIERE OF METALS |
GB9906116D0 (en) * | 1999-03-17 | 1999-05-12 | Didier Werke Ag | Refractory product |
US6425505B1 (en) | 1999-09-03 | 2002-07-30 | Vesuvius Crucible Company | Pour tube with improved flow characteristics |
CH691762A5 (en) * | 2000-06-28 | 2001-10-15 | Main Man Inspiration Ag | Intermediate container used for casting molten metal in a continuous casting machine has an inner part divided into at least two chambers connected to each other by an opening |
FR2818567B1 (en) * | 2000-12-22 | 2003-03-28 | Usinor | NOZZLE EQUIPPED WITH A RULE FOR THE INTRODUCTION OF LIQUID METAL INTO A CONTINUOUS CASTING LINGOTIERE OF METALS |
US7753273B2 (en) * | 2002-07-26 | 2010-07-13 | Es&S Automark, Llc | Ballot marking system and apparatus utilizing multiple key switch voter interface |
DE10240491A1 (en) * | 2002-09-03 | 2004-01-15 | Refractory Intellectual Property Gmbh & Co.Kg | Refractory ceramic immersion tube used in a continuous casting installation comprises a through-channel for connecting a feed opening for a metal melt on one end to an outlet opening for the metal melt on another end |
KR100946659B1 (en) * | 2002-11-28 | 2010-03-10 | 주식회사 포스코 | Submerged entry nozzle for continuous casting |
UA85179C2 (en) * | 2003-03-17 | 2009-01-12 | Везувиус Крусибл Компани | pour tube for casting molten metal and method of its use |
JP2005230826A (en) * | 2004-02-17 | 2005-09-02 | Ishikawajima Harima Heavy Ind Co Ltd | Nozzle for supplying molten metal |
CN103251994B (en) * | 2013-04-02 | 2016-03-30 | 周春华 | A kind of for the blood kettle device under swing vibration condition |
ES2553784B1 (en) * | 2014-06-09 | 2016-09-14 | Refractaria, S.A. | Distributor for steel casting |
CN107470568A (en) * | 2017-07-24 | 2017-12-15 | 嘉善优联物流装备有限公司 | A kind of casting mold apparatus used in casting device |
RU2691021C2 (en) * | 2017-11-07 | 2019-06-07 | Публичное акционерное общество "Русполимет" | Pouring device for pouring metal from tundish into molds |
CN107803492A (en) * | 2017-12-05 | 2018-03-16 | 重庆庆龙新材料科技有限公司 | Strontium aluminium alloy forming machine |
CN108904222B (en) * | 2018-07-30 | 2020-08-07 | 北京航空航天大学 | Novel choke ring suitable for manufacturing soft driver by inverse airflow method |
CN108840795A (en) * | 2018-08-08 | 2018-11-20 | 江南大学 | A method of lanolin fatty acid and lanonol are prepared by lanolin |
CN109465436B (en) * | 2018-11-12 | 2020-08-28 | 莱芜钢铁集团银山型钢有限公司 | Immersion type water gap for casting central point of ultrathin special-shaped blank |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6021171A (en) * | 1983-07-16 | 1985-02-02 | Nisshin Steel Co Ltd | Continuous casting device for broad and thin plate |
JP2583513B2 (en) * | 1987-07-03 | 1997-02-19 | 新日本製鐵株式会社 | Nozzle for pouring molten metal |
FR2647698A1 (en) * | 1989-05-31 | 1990-12-07 | Siderurgie Fse Inst Rech | LIQUID METAL SUPPLY DEVICE FOR A CONTINUOUS CASTING PLANT FOR THIN PRODUCTS AND METHOD FOR ITS IMPLEMENTATION |
GB9008538D0 (en) * | 1990-04-17 | 1990-06-13 | Rolls Royce Plc | A launder system for supplying molten metal and a launder nozzle |
JPH1011055A (en) * | 1996-06-18 | 1998-01-16 | Kawai Musical Instr Mfg Co Ltd | Electronic keyboard musical instrument |
-
1995
- 1995-09-28 FR FR9511375A patent/FR2739313B1/en not_active Expired - Fee Related
-
1996
- 1996-08-29 EP EP96401849A patent/EP0765702B1/en not_active Expired - Lifetime
- 1996-08-29 DE DE69602565T patent/DE69602565T2/en not_active Expired - Fee Related
- 1996-08-29 ES ES96401849T patent/ES2132857T3/en not_active Expired - Lifetime
- 1996-08-29 DK DK96401849T patent/DK0765702T3/en active
- 1996-08-29 AT AT96401849T patent/ATE180427T1/en not_active IP Right Cessation
- 1996-09-04 AU AU64435/96A patent/AU702389B2/en not_active Ceased
- 1996-09-11 TW TW085111086A patent/TW345508B/en not_active IP Right Cessation
- 1996-09-13 US US08/718,050 patent/US5733469A/en not_active Expired - Fee Related
- 1996-09-16 SK SK1182-96A patent/SK281773B6/en not_active IP Right Cessation
- 1996-09-20 CA CA002186084A patent/CA2186084C/en not_active Expired - Fee Related
- 1996-09-20 KR KR1019960041336A patent/KR100369257B1/en not_active IP Right Cessation
- 1996-09-24 CZ CZ962799A patent/CZ285931B6/en not_active IP Right Cessation
- 1996-09-24 MX MX9604288A patent/MX9604288A/en unknown
- 1996-09-24 CN CN96112972A patent/CN1064286C/en not_active Expired - Fee Related
- 1996-09-26 UA UA96093708A patent/UA42764C2/en unknown
- 1996-09-26 RU RU96120071/02A patent/RU2163179C2/en not_active IP Right Cessation
- 1996-09-26 BR BR9603908A patent/BR9603908A/en not_active IP Right Cessation
- 1996-09-27 TR TR96/00774A patent/TR199600774A2/en unknown
- 1996-09-27 JP JP27736896A patent/JP3978794B2/en not_active Expired - Lifetime
- 1996-09-27 PL PL96316322A patent/PL181356B1/en not_active IP Right Cessation
- 1996-09-27 RO RO96-01886A patent/RO117242B1/en unknown
- 1996-09-27 ZA ZA968126A patent/ZA968126B/en unknown
-
1999
- 1999-06-25 GR GR990401692T patent/GR3030610T3/en unknown
Also Published As
Publication number | Publication date |
---|---|
KR100369257B1 (en) | 2003-03-15 |
TR199600774A2 (en) | 1997-04-22 |
DE69602565D1 (en) | 1999-07-01 |
FR2739313B1 (en) | 1997-10-31 |
TW345508B (en) | 1998-11-21 |
CA2186084C (en) | 2008-01-29 |
FR2739313A1 (en) | 1997-04-04 |
RO117242B1 (en) | 2001-12-28 |
CN1064286C (en) | 2001-04-11 |
CZ285931B6 (en) | 1999-11-17 |
ES2132857T3 (en) | 1999-08-16 |
AU702389B2 (en) | 1999-02-18 |
SK118296A3 (en) | 1998-01-14 |
DK0765702T3 (en) | 1999-12-06 |
CZ279996A3 (en) | 1997-04-16 |
JPH09108794A (en) | 1997-04-28 |
EP0765702A1 (en) | 1997-04-02 |
ATE180427T1 (en) | 1999-06-15 |
SK281773B6 (en) | 2001-07-10 |
CA2186084A1 (en) | 1997-03-29 |
UA42764C2 (en) | 2001-11-15 |
ZA968126B (en) | 1997-04-21 |
CN1154885A (en) | 1997-07-23 |
MX9604288A (en) | 1997-08-30 |
JP3978794B2 (en) | 2007-09-19 |
DE69602565T2 (en) | 1999-12-16 |
RU2163179C2 (en) | 2001-02-20 |
KR970014880A (en) | 1997-04-28 |
BR9603908A (en) | 1998-06-09 |
AU6443596A (en) | 1997-04-10 |
GR3030610T3 (en) | 1999-10-29 |
PL181356B1 (en) | 2001-07-31 |
PL316322A1 (en) | 1997-04-01 |
US5733469A (en) | 1998-03-31 |
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