EP0725386B1 - Disk storage system, thin film magnetic head therefor and fabricating method thereof - Google Patents

Disk storage system, thin film magnetic head therefor and fabricating method thereof Download PDF

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Publication number
EP0725386B1
EP0725386B1 EP96101287A EP96101287A EP0725386B1 EP 0725386 B1 EP0725386 B1 EP 0725386B1 EP 96101287 A EP96101287 A EP 96101287A EP 96101287 A EP96101287 A EP 96101287A EP 0725386 B1 EP0725386 B1 EP 0725386B1
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EP
European Patent Office
Prior art keywords
magnetic
film
head
recording
thin film
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EP96101287A
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German (de)
French (fr)
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EP0725386A3 (en
EP0725386A2 (en
Inventor
Sano Masaaki
Kita Yoshiaki
Narumi Shun-Ichi
Kawabe Takashi
Fuyama Moriaki
Takano Hisashi
Yamamoto Hisano
Masuda Kenzo
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Hitachi Ltd
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Hitachi Ltd
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Publication of EP0725386A3 publication Critical patent/EP0725386A3/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y25/00Nanomagnetism, e.g. magnetoimpedance, anisotropic magnetoresistance, giant magnetoresistance or tunneling magnetoresistance
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/012Recording on, or reproducing or erasing from, magnetic disks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y10/00Nanotechnology for information processing, storage or transmission, e.g. quantum computing or single electron logic
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/127Structure or manufacture of heads, e.g. inductive
    • G11B5/31Structure or manufacture of heads, e.g. inductive using thin films
    • G11B5/3109Details
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/127Structure or manufacture of heads, e.g. inductive
    • G11B5/31Structure or manufacture of heads, e.g. inductive using thin films
    • G11B5/3163Fabrication methods or processes specially adapted for a particular head structure, e.g. using base layers for electroplating, using functional layers for masking, using energy or particle beams for shaping the structure or modifying the properties of the basic layers
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/127Structure or manufacture of heads, e.g. inductive
    • G11B5/33Structure or manufacture of flux-sensitive heads, i.e. for reproduction only; Combination of such heads with means for recording or erasing only
    • G11B5/39Structure or manufacture of flux-sensitive heads, i.e. for reproduction only; Combination of such heads with means for recording or erasing only using magneto-resistive devices or effects
    • G11B5/3903Structure or manufacture of flux-sensitive heads, i.e. for reproduction only; Combination of such heads with means for recording or erasing only using magneto-resistive devices or effects using magnetic thin film layers or their effects, the films being part of integrated structures
    • G11B5/3967Composite structural arrangements of transducers, e.g. inductive write and magnetoresistive read
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/14Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying magnetic films to substrates
    • H01F41/24Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying magnetic films to substrates from liquids
    • H01F41/26Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying magnetic films to substrates from liquids using electric currents, e.g. electroplating
    • GPHYSICS
    • G11INFORMATION STORAGE
    • G11BINFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B5/00Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
    • G11B5/127Structure or manufacture of heads, e.g. inductive
    • G11B5/33Structure or manufacture of flux-sensitive heads, i.e. for reproduction only; Combination of such heads with means for recording or erasing only
    • G11B5/39Structure or manufacture of flux-sensitive heads, i.e. for reproduction only; Combination of such heads with means for recording or erasing only using magneto-resistive devices or effects
    • G11B2005/3996Structure or manufacture of flux-sensitive heads, i.e. for reproduction only; Combination of such heads with means for recording or erasing only using magneto-resistive devices or effects large or giant magnetoresistive effects [GMR], e.g. as generated in spin-valve [SV] devices

Definitions

  • the invention relates to a thin film magnetic head according to the preamble of claim 1 and to a disk storage system comprising such a thin film magnetic head according to EP 0 012 326 A.
  • resistivity of the 80Ni-Fe alloy film is as low as 16 to 20 ⁇ cm, the eddy current loss becomes large in a high frequency band. Therefore, the strength of recording magnetic field of the magnetic head in a high frequency band is decreased, and accordingly the recording frequency is limited to about 30 MHz at maximum.
  • Co systems amorphous materials Fe-Al-Si sendust alloy thin film are proposed.
  • the former is thermally instable since the material is amorphous, and the latter has a disadvantage in the fabrication process as the magnetic core material for the inductive head since it requires a high temperature heat treatment at nearly 500°C.
  • saturation magnetic flux density (B S ) of these three-element system materials is as high as 1.5 T, resistivity is not large and the crystal grain size is not small in the 80Ni-Fe alloy and in addition to this there is a disadvantage in the high frequency characteristic as in the 80Ni-Fe alloy.
  • the data recording frequency is nearly 27 MHz which is near the performance limit of a magnetic head using the 80Ni-Fe alloy film or the Co-Ni-Fe alloy film.
  • JP-3-68,744 A a magnetic film for high frequency use formed by adding Nb, Ta, Cr, Mo to (40-50)Ni-Fe through a sputtering method, it is difficult to magnetically form a thick film through sputtering method because the material has large magnetocrystalline anisotropy.
  • EP 0 012 326 A discloses - as closest prior art - a thin film magnetic recording head comprising a lower magnetic layer deposited on a target. Above this layer there is deposited an insulator in which copper coils are embedded. An upper pole piece layer is curved down on one side to form a throat and a gap for reading a magnetic recording medium. On the other side, the upper pole piece layer is curved down to join the lower layer and to form a back gap. The upper layer is deposited by evaporating a metal upon the lower layer applying a resist mask and then electroplating through the mask onto the metal.
  • An object of the invention is to provide a thin film magnetic head and a disk storage system with a magnetic head for high density recording in a high frequency band, capable of performing high speed access and a high transfer rate.
  • the thin film magnetic head according to the invention is mounted on a disk storage system according to claim 3 with high transfer rate and high recording density, having a magnetic disk rotated above 4000 rpm when the disk storage system is recording or reproducing, and setting in recording frequency higher than 45 MHz.
  • the magnetic core of the write head is made of a material having large saturation magnetic flux density (B S ), small magnetic coercive force in the hard axis direction and large resistivity.
  • the range of composition obtainable of large resistivity and high saturation magnetic flux density is a range containing Ni of 38 to 60 wt% for Ni-Fe alloy.
  • a plating method has been employed in order to suppress the crystal grain size small, and it has been studied to add the third element such as Co, Mn, Cr, Pd, B, In and the like to a base of 38 to 60 wt% Ni-Fe two-element alloy.
  • composition range and a fabrication method of an outstanding thin film having a saturation magnetic flux density (B S ) larger than 1.5 T, a magnetic coercive force in the hard axis direction (H CH ) smaller than 795,8 A/m (1.0 Oe) and resistivity larger than 40 ⁇ •cm with keeping the film thickness of 2 to 5 ⁇ m which is required for the recording magnetic field.
  • B S saturation magnetic flux density
  • H CH hard axis direction
  • the magnetic disk has a transfer rate larger than 15 mega-bytes per second, an areal density of recording data larger than 500 mega-bits per 6.45 cm 2 (square inch) and a diameter of a magnetic disk smaller than 29 cm (3.5 inches).
  • one end of the upper magnetic film formed on the lower magnetic film contacts one end of the lower magnetic film, the other end faces the other end of the lower magnetic film through a magnetic gap, thereby the upper magnetic film forming a magnetic circuit having the magnetic gap in the part together with the lower magnetic film, a conductive coil forming a coil having a given number of winding turns passing between both of the magnetic films.
  • a fabrication method of the thin film magnetic head according to claim 1 comprises the steps of forming an upper magnetic film on a lower magnetic film, contacting one end of the upper magnetic film to one end of the lower magnetic film, facing the other end at the upper magnetic film to the other end of the lower magnetic film through a magnetic gap, thereby the upper magnetic film forming a magnetic circuit having the magnetic gap in the part together with the lower magnetic film, and forming a conductive coil having a given number of winding turns passing between both of the magnetic films.
  • At least one of the lower and the upper magnetic films is formed by electroplating using a Ni-Fe electroplating bath containing the metallic ion concentration of Ni ++ ions of 15 to 20 g/l and Fe ++ ions of 2.0 to 2.7 g/l, the ratio of the Ni ++ ions and the Fe ++ ions ( Ni ++ /Fe ++ ) being 7 to 8, containing a stress release agent and a surface active agent, the pH being 2.5 to 3.5.
  • the thin film magnetic head is formed by electroplating though a mask in a magnetic field under condition of keeping the temperature of the plating bath at 20 to 35°C and the current density of 5 to 30 mA/cm 2 .
  • the thin film magnetic head described in claim 1 the film being formed using a plating bath each ions added Co ions of 0.4 to 0.6 g/l and/or Cr, Mo, Pd, In, B less than 0.1 g/l, and that the magnetic film is formed by electroplating though a mask in a magnetic field.
  • writing blur due to the recording frequency and fluctuation of an over-write value are prevented by designing the thickness, resistivity and relative permeability of a magnetic film of a magnetic pole for a write head in taking eddy current loss into consideration, and at the same time by setting the data recording frequency to a high value and rotating a magnetic disk fitting to the above head at a high speed.
  • the head efficiency (efficiency to induce magnetic flux) of the magnetic head is dominated by the eddy current loss.
  • the eddy current loss it is most effective to decrease the film thickness of the magnetic core, decreasing of the film thickness causes recording incapability due to shortage in the recording magnetic flux.
  • the film thickness is required to be larger than 2 ⁇ m as well as saturation magnetic flux density is required to be high.
  • employing a multi-layer film is for decreasing the eddy current loss, but the head process for coping with the high recording density is difficult to obtain a high accuracy in the dimension.
  • the Ni-Fe magnetic film (3 ⁇ m film thickness) shows a saturation magnetic flux density (B S ) larger than 1.5 T and resistivity ( ⁇ ) of 40 to 50 ⁇ •cm when Ni concentration is within the range of 38 to 60 wt%. That is, when the Ni concentration is below 38 wt%, the specific resistivity ( ⁇ ) is large, but saturation magnetic flux density (B S ) becomes lower than 1.5 T.
  • saturation magnetic flux density (B S ) also becomes lower than 1.5 T.
  • concentration of Ni is 40 to 50 wt%.
  • a plating process is suitable for fabricating a film having such a composition. That is, since the crystal grain size can be made very small by an electroplating method, magnetic coercive force can be made small and the orientation of crystal can be decreased as low as possible even in a case of such a composition having large magnetocrystalline anisotropy. For example, it is preferable that the orientation ratio of crystal is suppressed below 5.0, that is (1 1 1)/(2 0 0) ⁇ 5.0.
  • the composition of a plating bath for fabricating such a film is that the Ni and Fe ion concentrations are Ni ++ : 15 to 20 g/l, Fe ++ : 2.0 to 2.7 g/l, and the ion ratio (Ni ++ /Fe ++ ) is 7 to 8.
  • plating current density is 10 to 20 mA/cm 2
  • the pH is 3.0
  • the bath temperature is 30°C.
  • the Co is less than 15 wt% and the Mo is less than 3 wt% in order to keep saturation magnetic flux density (B s ) higher than 1.5 T and resistivity ( ⁇ ) larger than 4 0 ⁇ •cm.
  • CoSO 4 •6H 2 O 100 g/l (Co ions of 21 g/l)
  • Mo Na 2 MoO 4 •2H 2 O of 4.8 g/l
  • resistivity ( ⁇ ) is increased not so large as about 10%.
  • the adding amount of Mo, Cr should be limited to 3 wt% or less.
  • the adding amount should be limited as the same as above.
  • the plating condition may be the same as in the case of a Ni-Fe magnetic film as described above.
  • the high frequency loss (tan ⁇ ) of the magnetic film is only the eddy current loss
  • the high frequency loss can be expressed by the following equation.
  • ⁇ ' and ⁇ " are a real part and an imaginary part of the complex magnetic permeability.
  • C is a constant determined by the shape of the film, and ⁇ 0 is permeability of vacuum.
  • Equation (2) by specifying the value ⁇ d 2 / ⁇ which can be obtained from relative permeability ⁇ inherent to the magnetic film, the film thickness d and resistivity ⁇ , the head efficiency ⁇ for an arbitrary frequency f can be extrapolated.
  • the capacity per one magnetic disk device is 550 MB, it is possible to handle an OS (Operation Software) such as Windows, Workplace and the like.
  • OS Operating Software
  • areal density capable of recording the data is required to be 500 MB/6,45cm 2 (in 2 ).
  • a recording head which is capable of performing sufficient recording to a medium having a high magnetic coercive force and at a high frequency range, is fabricated by a specified composition and through a low cost electroplating method.
  • Fig. 1 and Fig. 2 are a whole view and a plan view showing an embodiment of a disk storage system in accordance with the present invention.
  • the disk storage system is composed of a magnetic disk 1 for recording information, a DC motor (not shown in the figures) for a means to rotate the magnetic disk, a magnetic head 2 for writing and reading the information, a positioning device for a means to support the magnetic head 2 and change the position of the magnetic head 2 to the magnetic disk 1 which is composed of an actuator 4, a voice coil motor 5 and an air filter 6 for keeping the inside of the system clean.
  • the actuator 4 is composed of a carriage 7, a rail 8, a bearing 9.
  • the voice coil motor 5 is composed of a voice coil 10 and a magnet 11.
  • Fig. 3 is a front view of a disk storage system in accordance with the present invention
  • Fig. 4 is a plan view of the disk storage system.
  • the reference character 1 is a magnetic disk
  • the reference character 2 is a magnetic head
  • the reference character 3 is a gimbals system supporting device
  • the reference character 4 is a positioning device (actuator).
  • the magnetic disk 1 is rotated in the direction of the arrow a by a rotating driving mechanism.
  • the magnetic head 2 is supported by the supporting device 3 and moved in the direction of the arrow b 1 or b 2 on the rotating diameter O 1 and positioned, and thereby to perform magnetic recording or reproducing using a proper one of cylinders T 1 to T n .
  • the magnetic disk 1 is a medium having a surface roughness R MAX less than 10 nm (100 ⁇ ) preferably a medium having a better surface condition of a surface roughness less than 5 nm (50 ⁇ ).
  • the magnet disk 1 is made by forming a magnetic recording film on the surface of a rigid substrate through a vacuum film forming method.
  • the magnetic recording film is formed as a magnetic thin film made of ⁇ -Fe 2 O 3 or Co-Ni, Co-Cr or the like.
  • the surface characteristic of the rigid substrate directly reflects on the surface characteristic of the recording film.
  • the rigid substrate having a surface roughness R MAX less than 10 nm (100 ⁇ ) is used.
  • a rigid substrate having the major component of glass, chemically reinforced soda-alumina silicate glass or ceramic is suitable for such a rigid substrate.
  • the magnetic recording film may be formed of a magnetic iron oxide such as ⁇ -Fe 2 O 3 or the like or a magnetic nitride.
  • a magnetic iron oxide such as ⁇ -Fe 2 O 3 or the like
  • a magnetic nitride it is preferable that an oxide film or a nitride film is provided on the surface or an oxide covering film is formed on the surface. It is also preferable to use a carbon protecting film.
  • the durability of the magnetic recording film is improved and accordingly the magnetic disk 1 is prevented from damage which may be caused in a case where recording or reproducing is performed under a very low floating condition or at a contact-start-stop condition.
  • the oxide film or the nitride film may be formed through reactive sputtering, reactive vapor depositing or the like.
  • the oxide coating film may be formed by intentionally oxidizing the surface of the magnetic recording film made of a metal or an alloy containing at least one kind of iron, cobalt and nickel such as Co-Ni or Co-Cr through reactive plasma treatment or the like.
  • the magnetic disk 1 may be either of perpendicular recording type where the recording residual magnetization in the magnetic recording film has a component in the perpendicular direction to the film surface as the major component, or of a longitudinal recording type where the recording residual magnetization has a longitudinal component as the major component.
  • Fig. 5 and Fig. 6 are views showing the assembled construction of the magnetic head 2 and the gimbals system supporting device 3.
  • the magnetic head 2 has reading and writing elements 22 in the side of an air flow-out end of a slider 25 of a ceramic structure body and supported by the supporting device 3 driven by a positioning device 4 so as to be allowed pitching motion and rolling motion by adding a load on the surface 24 opposite to a floating surface 23.
  • the reading and writing element 22 is a thin film element formed through the same process as that of IC fabricating technology.
  • the supporting device 3 is constructed by attaching and fixing one end of a supporting body 37 formed of an elastic metallic sheet to a rigid arm part 51 attached to the positioning device 4 using jointing members 12, and by attaching a flexible body 36 formed of a similar metallic sheet to a free end on the other end in the lateral direction of the supporting body 37, and by attaching the magnetic head 2 on the underside surface of the flexible body 36 (refer to Fig. 3 and Fig. 4).
  • the portion of the supporting body 37 attached to the rigid arm part 51 has an elastic spring part 41, and forms a rigid beam part 42 by connecting to the elastic spring part 41.
  • the rigid beam part 42 has flanges 42a, 42b formed by bending on the both sides.
  • the flexible body 36 comprises two outer flexible frame parts 31, 32 extending nearly in parallel to the axial line in the lateral direction of the supporting body 36, and a side frame 33 jointing the outer flexible frame parts 31, 32 in the end far from the supporting body.
  • the flexible body 36 comprises further a middle tongue-shaped part 34 having one end as a free end extending from near the middle portion of the side frame 33 along and nearly in parallel to the outer flexible frame parts 31,32 and the one end in the opposite side to the side frame 33 is attached to the vicinity of the free end of the supporting body 37 by welding or the like.
  • a projection 35 for load for example, a semi-spherical projection is provided, and a load is transmitted from the free end of the supporting body 37 to the middle tongue-shaped part 34.
  • the surface 24 of the magnetic head 2 is fixed to the under surface of the middle tongue-shaped part 34 by adhesive.
  • a magnetic disk 1 having a surface roughness R MAX is used and the floating amount g at starting of floating the magnetic head 2 is set within the range of 0.01 ⁇ m to 0.04 ⁇ m.
  • the floating amount g of the innermost cylinder T n among the reading and writing cylinders T 1 to T n provided in the magnetic disks 1 is set between the floating amount g at starting of floating of 0.01 ⁇ m to 0.04 ⁇ m and a value several times of the floating amount.
  • the shape of the slider 25 constructing the magnetic head 2, the load applied from the supporting device 3 to the magnetic head 2, the rotating speed of the magnetic disk 1 and so on are set so as to obtain the floating amount as described above.
  • Fig. 7 is a perspective view showing a negative pressure slider.
  • the load slider 70 comprises an air intake surface 71 and a negative pressure generating surface 73 surrounded by two positive pressure generating surfaces 72, 72 for generating the floating force, and a groove 74 having a step larger than the negative pressure generating surface 73 in the boundary between the air intake surface 71, the two positive pressure generating surfaces 72, 72 and the negative pressure generating surface 73.
  • the negative pressure slider 70 On an air outlet end 75, the negative pressure slider 70 also has thin film magnetic head elements 76 for recording and reproducing information on and from a magnetic disk 1.
  • the air introduced through the air intake surface 71 is expanded at the negative pressure generating surface 73. At that time, since an air flow flowing toward the groove 74 is also generated, there exists inside the groove 74 an air flow flowing from the air intake surface 71 toward the air outlet end 75.
  • Fig. 8 is a conceptual view of a dual element head forming a recording head.
  • the dual element head comprises an inductive head and a reproducing head, and a shield part for preventing disturbance in the reproducing head due to leakage magnetic flux.
  • the magnetoresistive element according to the present invention may be used for a perpendicular recording by combining with a head for vertical magnetic recording.
  • the head is formed with a reproducing head composed of a lower shield film 82 on a substrate 80, a magnetoresistive film 86, an electrode 85 and an upper shield film 81, and a recording head composed of a lower magnetic film 84, a coil 87 and an upper magnetic film 83.
  • This head By using this head, signals are written in on the recording medium and signals read out from a recording medium.
  • the magnetic gap between the sensing part of the reproducing head and the recording head can be positioned at the same track at a time by forming at an overlapping position on the same slider, as described above.
  • This head is formed in a slider and mounted on a disk storage system.
  • the upper and the lower magnetic films of the inductive head are formed through the following fabrication method.
  • an inductive head having an upper and a lower magnetic cores which are electroplated in a plating bath containing Ni ++ of 16.7 g/l, Fe ++ of 2.4 g/l, and a common stress-release agent and a surface active agent under a condition of pH of 3.0, plating current density of 15 mA.
  • the track width is 4.0 ⁇ m, and gap length is 0.4 ⁇ m.
  • the composition of this magnetic film is 42.4 Ni-Fe (wt %), and as to the magnetic characteristics, saturation magnetic flux density (B S ) is 1.64 T, the magnetic coercive force in the hard axis direction (H CH ) is 39.789 A/m (0.5 Oe), and resistivity ( ⁇ ) is 48.1 ⁇ •cm.
  • the inductive head comprises an upper magnetic core 83, a lower magnetic core 84 also serves as an upper shield film, a coil 87, a magnetoresistive element 86, an electrode 85 for conducting sense current to the magnetoresistive element, a lower shield film 82 and a slider 80.
  • Fig. 9 shows the evaluated result of the performance (over-write characteristic) of the recording head according to the present invention having such a construction.
  • An outstanding recording characteristic of nearly -50 dB in a high frequency range above 40 MHz have been obtained.
  • Fig. 10 shows the relationship between magnetic coercive force in the hard axis direction and average crystal grain size of magnetic films obtained through the plating method and the sputtering method in this embodiment. It can be understood that when the crystal grain size is smaller than 50 nm (500 ⁇ ), low magnetic coercive force lower than 79.577 A/m (1.0 Oe) can be obtained.
  • Ni-Fe alloy thin film composed of Ni 70 to 80 wt%, Fe of the remainder may be formed through electroplating, as the same way described above, or the alloy film may be also formed through sputtering method.
  • Fig. 11 is a cross-sectional view and Fig. 12 is a plan view showing an inductive head according to the present invention.
  • the thin film head comprises an upper shield film 81, a lower magnetic film 84 attached onto the upper shield film and an upper magnetic film 83 which are made of the aforementioned magnetic film.
  • Fig. 11 is a cross-sectional view being taken on the plane of the line A-A of Fig. 12.
  • a non-magnetic insulator body 89 is put between the films 83 and 84.
  • a part of an insulator body determines a magnetic gap 88, and this interacts in a conversion relationship with, for example, a magnetic medium placed in an air-bearing relation, as the prior art.
  • a supporting body serves as a slider having an air-bearing surface (ABS), and this accesses to and is in a floating relation with a rotating disk during disk file operation.
  • ABS air-bearing surface
  • the thin film magnetic head has a back gap 90 formed by connecting an upper magnetic film 83 with a lower magnetic film 84.
  • the back gap 90 is separated from the magnetic gap by a coil 87 interposed between.
  • the continuing coil 87 forms a layer formed on the lower magnetic film 84, for example, through plating to electromagnetically couple with the lower magnetic film.
  • the coil 87 has an electric contact point 91 in the center of coil which is berried with insulator body 89, and also has a large area as an electric contact point 92 in the outer end terminal point of the coil.
  • the contact points are connected to external lead wires and reading and writing signal processing head circuit (not shown).
  • the coil 87 formed in a single layer is slightly deformed elliptical, and the portion having small cross-sectional area is placed in the nearest position to the magnetic gap and the cross-sectional area gradually increases as the distance from the magnetic gap increases.
  • the back gap 90 positions relatively near the ABS of the magnetic gap. However, there exists relatively densely many windings of the elliptical coil between the back gap 90 and the magnetic gap 88, and the width or the cross-sectional diameter of the coil is small in this region. The large cross-sectional diameter in the farthest region from the magnetic gap decreases the electrical resistance.
  • the elliptical coil does not have any angle or sharp corner or edge, and therefore resistance to current is small. Further, the total length of conductor of the elliptical coil is short compared with a rectangular or a circular (ring-shaped) coil.
  • the total resistance of the coil is relatively small, consequently heat generation is small, and heat is properly radiated. Since heat generation is substantially decreased, collapse, extension and expansion of the thin film are prevented and the cause of ball-tip projection is eliminated.
  • the shape of the elliptical coil, width of which uniformly changes, can be formed through a conventional economical technology such as sputtering or vapor deposition method.
  • plating deposition is apt to become non-uniform in width.
  • a coil removed corners or sharp edge portions is subjected to small mechanical stress.
  • a nearly elliptical coil having multiple winding turns is formed between magnetic cores, the cross-sectional diameter of the coil gradually expands from the magnetic gap toward the back gap, the signal output power is increased and the heat generation is decreased.
  • Fig. 13 is a conceptual view showing the construction on the surface of a substrate of a magnetoresistance effect element in accordance with the present invention formed on the bottom portion of the above mentioned inductive head.
  • the magnetoresistive film 110 is formed along a surface 183 opposed to a recording medium in a long rectangular shape having a width 143 of the element on a substrate 150. This definition on the shape has an effect to provide a proper shape magnetic anisotropy in the perpendicular direction with respect to a direction in which the magnetic field to be detected by the magnetoresistive film 110 is applied.
  • a current is conducted in the magnetoresistive film 110 from electrodes 140 electrically contacting to the film, and an output is obtained from the resistance change of the film caused by the magnetic field applied to the magnetic field detecting portion having the size of the width 141 in the direction parallel to and the width 142 in the direction perpendicular to the surface of the recording medium.
  • the mechanical durability of the element can be increased by arranging a yoke-shaped soft magnetic body on the opposite surface to guide the magnetic field from a recording medium and by magnetically coupling to a magnetoresistive element arranged inside.
  • the resistance of the magnetic circuit is reduced and the sensitivity can be improved by decreasing the MR height of the element.
  • the magnetoresistive element according to the present invention has a construction, for example, as shown in Fig. 14.
  • the magnetoresistive element is formed by laminating on a substrate 150 a magnetoresistive film 110, that is, a bias film 132, a magnetic film 111, a non-magnetic conductive film 120, a magnetic film 112, a non-magnetic conductive film layer 120, a magnetic film layer 111, a bias film 131, and further on the laminated layer by electrically jointing an electrode 140.
  • an electrode 140 is placed under a bias film 131.
  • the electrode may be formed in such a manner, for example, that a bias film is partially formed and then an electrode is formed over the bias film.
  • a conductive bias film for example, Fe-Mn film, Co-Pt film or the like is formed and then an electrode is formed directly on the conductive bias film.
  • the present element is constructed by alternatively laminating a magnetic film applied with a strong anisotropy by a bias film, a magnetic film applied with a weaker anisotropy than the above anisotropy by uniaxial magnetic anisotropy, a shape magnetic anisotropy or a soft film bias through a non-magnetic conductive film so as to conduct current to each other but not cause magnetic coupling between them.
  • a bias film a magnetic film applied with a weaker anisotropy than the above anisotropy by uniaxial magnetic anisotropy
  • a shape magnetic anisotropy or a soft film bias through a non-magnetic conductive film so as to conduct current to each other but not cause magnetic coupling between them.
  • the applying direction of the anisotropy will be described below.
  • Fig. 15 is a conceptual view showing an example of anisotropy control in a magnetoresistive element in accordance with the present invention, and is a perspective view of a part of the element shown by A-A' of Fig. 14.
  • the bias films 131 and 132 apply anisotropy by switched connection in the directions indicated by the arrows 171 and 172 in the figure.
  • the arrow 160 in the figure indicates the direction of the magnetic field to be detected, and the arrow 161 indicates the direction of unidirectional magnetic anisotropy induced in the magnetic film 111.
  • the easy magnetizing direction of the magnetic film 112 sandwiched by the non-magnetic conductive films 120 is applied in the direction indicated by the arrow 162 in the figure by induction of uniaxial magnetic anisotropy. This can be attained by applying a magnetic field in a proper direction during growing the magnetic film.
  • the embodiment shown by the figure is an example where application of the anisotropy is attained by the bias film and the inductive magnetic anisotropy.
  • the arrows 161 and 162 intersect at right angle with each other on the surface of the film.
  • the magnetization of the magnetic film 111 can be fixed to a nearly constant value and only the magnetization of the magnetic film 111 can largely react to an external magnetic field.
  • the magnetization of the magnetic film 111 is in a state of easy axis excitation with respect to the magnetic field to be detected where the directions of magnetization and external magnetic field are parallel to each other by anisotropy 161.
  • the magnetization of the magnetic film 112 is in a state of hard axis excitation where the directions of magnetization and external magnetic field are perpendicular to each other. With this effect, the response described above becomes further outstanding.
  • the element becomes capable of operating at a high frequency since there appears a state where the element is driven by an external magnetic field in the hard axis excitation due to rotation of the magnetization of the magnetic film 112 with respect to the direction of the arrow 162 as an origin and accordingly the noise accompanied by excitation of movement of magnetic domain wall is prevented.
  • magnetoresistive element in which application of anisotropy is performed by two different kinds of bias films, that is, an anti-ferromagnetic film and a hard-magnetic film.
  • the magnetoresistive element is formed by laminating on a substrate 150 an anti-ferromagnetic film 132, a magnetic film 111, a non-magnetic film 120, a magnetic film 112 and a hard-magnetic film 133, and then by connecting an electrode on the laminated film. Both of the anti-ferromagnetic film 132 and the hard-magnetic film 133 are respectively fixed to two films of the magnetic films 111, 112 separated by the non-magnetic film.
  • the directions of magnetization of the magnetic films 111 and 112 are induced in the directions indicated by the arrows 161 and 162 respectively by performing thermal treatment under magnetic field or magnetizing treatment in the directions 172 and 173, a parallel direction and a perpendicular direction to the direction 160 of the magnetic field to be detected.
  • the anti-ferromagnetic film is formed of, for example, nickel oxide, and the hard-magnetic film is formed of a cobalt-platinum alloy.
  • the same effect may be obtained when the positions of the hard-magnetic film and the anti-ferromagnetic film are reversed, or the directions of induced magnetization are reversed.
  • the films composing the magnetoresistive element according to the present embodiment are fabricated using a high frequency magnetron sputtering apparatus in a manner as follows.
  • Magnetoresistive elements have been fabricated by successively laminating the following materials on a ceramic substrate and a Si single crystal substrate of 1 mm thickness and 76.2 mm (3 inches) diameter in an argon atmosphere of 4 mbar (3 mill-Torrs).
  • a sputtering target used are targets of nickel oxide, cobalt, a nickel-20 at% iron alloy and copper.
  • Addition of cobalt to nickel-20 at% iron is preformed by placing a cobalt chip on a nickel-20 at% iron target. Addition of nickel and iron to cobalt is performed by placing nickel and iron chips on a cobalt target.
  • the laminated film is formed by applying a high frequency electric power to each cathode placing each of the targets to generate a plasma inside the system and then by opening and closing a shutter provided each of the cathodes one by one to form each of the films successively.
  • a magnetic field of approximately 3978.85 A/m (50 Oe) is applied in parallel to the substrate using two pairs of magnets crossing at right angle to each other on the surface of the substrate to form uniaxial magnetic anisotropy in the film and to induce the direction of the switched connection bias of a nickel oxide film to each direction.
  • Induction of anisotropy is performed by applying a magnetic field in the direction to be induced during forming each magnetic film using two pairs of magnets provided near a substrate. Otherwise, the direction of anti-ferromagnetic bias is induced in the direction of a magnetic field by performing heat treatment under magnetic field at a temperature near the Neel temperature of the anti-ferromagnetic film after forming the multi-layer film.
  • Evaluation of performance of the magnetoresistive element is conducted by patterning the film in a rectangular shape and forming electrodes. In this time, the patterning and electrode forming are performed so that the direction of uniaxial magnetic anisotropy of the magnetic film becomes parallel to the direction of current in the element.
  • the measurement is performed by conducting a constant current between the electrode terminals, applying a magnetic field in the surface of the element in the direction perpendicular to the direction of current flow, measuring the electrical resistance of the element as the voltage between the electrode terminals, and detecting the measured results as the magnetoresistance ratio.
  • the characteristic of the element is expressed by the magnetoresistance ratio and the saturation magnetic field.
  • the reproducing output of the element corresponds to the largeness of the magnitude of the magnetoresistance ratio and the sensitivity corresponds to the smallness of the magnitude of the saturation magnetic field.
  • the magnetoresistive elements No. 1 to No. 5 have a magnetoresistance ratio larger than 4% and a better magnetic characteristic, and are outstanding particularly in the resistance changing rate compared to No. 6 and No. 7.
  • the specimen No. 1, No. 2, No. 4 show an excellent magnetic field sensitivity of about 795.77 A/m (10 Oe) saturation magnetic field and a high output of 6 to 7% magnetoresistance ratio.
  • the region sandwiched by a pair of electrode 85, which becomes a reproducing track width, is set to 2 ⁇ m.
  • current of 15 mA op is conducted to the coil 87 having 20 winding turns to record any information on a medium.
  • a disk storage system is constructed by combining this magnetic head with a 89.0 mm (3.5 inch) magnetic disk with a CoCrTa (adding amount of Cr is 16 at%) recording film having a magnetic coercive force in the recording bit direction of 167122 A/m (2100 Oe) and a magnetic coercive force orientation ratio of 1.2.
  • the production Br ⁇ of the residual magnetic flux density and the film thickness of the magnetic disk recording film used hear is 100 Gauss• ⁇ m.
  • the specification of the magnetic memory apparatus constructed in this embodiment is shown in Table 2. Specification of a 89.0 mm (3.5 inch) Type Apparatus using a Dual Element Head Memory Capacity 5.5 GB Number of Disks 4 Number of Data Surfaces 8 Number of Heads 8 Number of Tracks/Disk Surface 7378 Maximum Linear Recording Density 170 kBPI Track Density 8.3 kTPI Rotating Speed 4491 RPM Recording Frequency 80.0 MHz Transfer Rate (to/from Media) 18 MB/sec
  • Figs. 16A, 16B and 16C are graphs showing the relationships between component of magnetic film, magnetic characteristics and resistivity ( ⁇ ) when metallic ion concentrations, that is, amounts of Ni ++ and Fe ++ in a plating bath are varied.
  • Ni ++ is added using NiCl 2 •6H 2 O
  • Fe ++ is added using FeSO 4 •7H 2 O
  • a common stress release agent and a surface active agent are added.
  • Plating is performed under a condition of pH of 3.0 and plating current density of 15 mA/cm 2 .
  • the film thickness is 3.0 ⁇ m.
  • the saturation magnetic flux density (B S ) is larger than 1.5 T and resistivity ( ⁇ ) is larger than 40 ⁇ •cm, that is, the film has outstanding characteristics in that saturation magnetic flux density (B S ) is 1.5 times as large as and resistivity ( ⁇ ) is twice as large as those of well known 80Ni-Fe permalloy film.
  • the magnetic coercive force in the hard axis direction (H CH ) is smaller than 79.577A/m (1 Oe), similar to 80Ni-Fe permalloy.
  • the varying trends of saturation magnetic flux density (B S ) and resistivity ( ⁇ ) are nearly the same as those of the bulk material, but the decreasing rates as the Ni content increases are smaller than those of the bulk material. The reason is that the film has a very small crystal grain size of 4 to 8 nm (40 to 80 ⁇ ) compared with that of the bulk material.
  • Such characteristics are not largely varied when the pH is varied within the range of 2.5 to 3.5, and the plating current density is varied within the range of 5 to 30 mA/cm 2 .
  • the plating bath temperature is varied within the range of 25 to 35 °C, the content of Ni is slightly increased as the temperature is increased, but the characteristics themselves are not affected.
  • the magnetic film of the present embodiment is suitable for an upper magnetic core of an inductive head having a lower magnetic core using an Fe-Ni series alloy containing Ni of 70 to 80 wt%, but the film may be used both of the upper and the lower magnetic cores.
  • B S shows the highest value of 1.6 T at Ni of 40 to 50 wt%, and it is preferable to combine with a film having an (Ni/Fe) ratio of 0.667 to 1.00.
  • the (Ni/Fe) ratio of a film having Ni of 38 to 60 wt% is 0.613 to 1.50.
  • Figs. 17A, 17B and 17C show test results on the magnetic characteristics and resistivity ( ⁇ ) of a magnetic film containing Mo in a (Ni 44 wt%-Fe) series alloy.
  • the figure shows the magnetic characteristics and resistivity ( ⁇ ) of a magnetic film formed by adding Mo as an element to increase resistivity ( ⁇ ) to a plating bath containing N ++ of 16.7 g/l and Fe ++ of 2.2 g/l.
  • the Mo is added using Na 2 MoO 4 •4H 2 O by 5 g/l at maximum.
  • resistivity ( ⁇ ) of the magnetic film is increased in proportion to the amount of added Mo.
  • resistivity ( ⁇ ) of the magnetic film having Mo of 2 wt% shows above 60 ⁇ •cm which is about three times as large as that of the 80Ni-Fe permalloy film.
  • the saturation magnetic flux density (B S ) is decreased only 5% and nearly 1.50 T which is 1.5 times as high as that of the 80Ni-Fe permalloy film.
  • Figs. 18A, 18B and 18C show test results on an (Ni 44 wt%-Fe)-Co 15 wt%-Mo magnetic film to which Co and Mo are added at a time in order to further increase saturation magnetic flux density (B S ) and resistivity ( ⁇ ) without degrading the magnetic characteristics of the magnetic film.
  • the Co is added using CoSO 4 •7H 2 O, and the Mo is added using Na 2 MoO 4 •4H 2 O, as the same as in Embodiment 3.
  • the examples shown are in a case where the adding amount of Co is a constant of 13 wt% (100 g/l on the base of CoSO 4 •7H 2 O) and on the other hand the adding amount of Mo is varied up to 4 wt%.
  • saturation magnetic flux density (B S ) is 1.55 T which is slightly higher value than the film without Co. Further, since addition of Co increases anisotropy of a film, magnetic characteristic of the film is stabilized.
  • the magnetic film of this embodiment may be used in the same way as in the previous embodiments.
  • Fig. 19 shows permeability ( ⁇ ) of the typical magnetic films fabricated through the manufacturing methods described in Embodiments 2 to 4, in the figure permeability is normalized with the value ⁇ at frequency of 1 MHz. For the purpose of comparison, permeability ( ⁇ ) of the 80Ni-Fe permalloy film is also measured. The thicknesses of all the film are 3 ⁇ m.
  • the frequency (f) where permeability ( ⁇ ) decreases by 25 % is up to the range of 40 MHz to 70 MHz. This range is 3 to 5 times as wide as 15 MHz for the permalloy. It can be understood that the frequency characteristics of the films of the present embodiment are improved.
  • Fig. 20 and Fig. 21 are cross-sectional views showing an inductive head having a two stage winding coil using the magnetic films according to the present invention for an upper and a lower magnetic films as the same as in Embodiment 1.
  • the thin film magnetic head 210 involves a lower portion and an upper portion magnetic film formed of two films 212 and 214 made of a magnetic material, for example, permalloy.
  • the films 212 and 214 are deposited by two stages containing shaping films 221 and 213, respectively.
  • These films 212 and 214 are separated by insulating films 215, 216 and 217 except for a back portion region 218 where the films are physically contact and a top end region 219 where the films are separated by a thin film 220 of a non-magnetic material to form a magnetic gap 221.
  • the coil 222 has two inter-layer multi-windings 223a to 223n deposited in an elliptical pattern between the films 215, 216 and 217 of insulating material.
  • the top end portion of the transducer gap 221 is even with an air bearing surface (ABS) formed on a non-magnetic substrate attached with the above mentioned films.
  • ABS air bearing surface
  • the transducer gap 221 reacts with a rotating magnetic recording medium (not shown) such as a rotating magnetic disk in an air bearing relation.
  • a rotating magnetic recording medium such as a rotating magnetic disk in an air bearing relation.
  • the head flies on the air bearing surface (ABS) very near the recording surface of the disk.
  • the thin film magnetic head is fabricated by depositing a magnetic film 212 and a shaping film 211 on a substrate 224 using a proper mask in order to form a thin deposited film in the top den region 219 of a magnetic pole chip. Then a non-magnetic film 220 is formed on the films 211 an 212 except for the back gap region 218.
  • a first insulating film 215 is deposited onto the film 220 except for the magnetic gap 221.
  • a continuous and flat conductive first film of elliptical swirl-shaped winding 223a to 223n is deposited on the insulating film 215 through, for example, electroplating.
  • An insulating film 216 is deposited on the first film of the coil, and a second film winding of the coil is deposited, on the coil an insulating film 217 is deposited. Then, as described above, the magnetic film 214 is deposited on the insulated coil except for the back portion gap region 218 which physically contacts the magnetic film 212.
  • the top end 219 of the magnetic pole chip has a per-selected nearly constant width W.
  • the width W is equal to or slightly narrower than the width of a track on the corresponding rotatable magnetic medium.
  • the selected width W of the top end of the magnetic pole chip is obtained by cutting the top end of the magnetic pole chip, and the step to cut the top end of the magnetic pole chip is performed before the step to deposit the shaping film 213 for the second magnetic film 214.
  • the top end of the magnetic pole chip can be cut with a very higher accuracy than a conventional process.
  • the thin film head assembly After depositing the magnetic film 214 and before depositing the shaping film 213, the thin film head assembly is covered with a photo-resist mask 230. Then a window 232 is formed on the photo-resist mask in either of the sides of the top end region of the magnetic pole chip of the head.
  • the masked head is performed an ion milling process. During the process, the portion of head not covered by the mask is milled to be carved in a desired width as shown in Fig. 5.
  • the ion milling process affects on a surface to be worked the same effect as normal condition, and accordingly a structure not covered with a mask is also milled together with a photo-resist mask. Therefore, the milled material produced from the head is re-deposited onto the remaining portion of the mask and onto the head structure having been milled before.
  • the un-masked structure is milled up to the substrate 224 through the magnetic film 14, the non-magnetic gap film 220 and the magnetic film 212.
  • the first step is performed until the substrate 224 is slightly milled.
  • the second step of the ion milling process is performed to remove all the re-deposited materials, and performed in a large angle inclining state in such a state as inclining 75 to 80 degree to the vertical direction.
  • a permalloy magnetic material is milled with an etching rate of about 55 nm (550 ⁇ ) per minute by electric power of about 2 watt per cubic centi-meter. Then the photo-resist is removed, a shaping magnetic film is deposited, and thus a thin film magnetic head is completed.
  • the photo-resist mask is milled during ion milling, and the thickness of the photo-resist on the head becomes thinner than the thickness of the photo-resist on the magnetic pole chip region depending on the shape of the magnetic film 214.
  • the thin film magnetic head fabricated according to the present invention is of a yoke structure having a transducer magnetic gap in one end and a back gap region in the other end, and the yoke structure having a conductive coil for energizing a magnetic yoke attached between the magnetic gap and the back gap region of the yoke structure is formed with two films made of a magnetic material.
  • the disk storage system constructed using the thin film magnetic head fabricated in the present embodiment will be described.
  • the disk storage system according to the present embodiment comprises a magnetic disk having an outer diameter of approximately 8.90 mm (3.5 inches), a spindle for rotating the disk, a positioning mechanism for a magnetic head and a housing.
  • the magnetic head is an inductive head, and the track width is 5.0 ⁇ m.
  • the upper and the lower magnetic films of the head are formed with (Ni 44 wt%-Fe)-2 wt%Mo alloy thin films having saturation magnetic flux density of 1.3 T, resistivity ( ⁇ ) of 60 ⁇ •cm, relative permeability ⁇ of 1000, a film thickness d of 3 ⁇ m, and the gap length is 0.4 ⁇ m.
  • An equivalent effect may be obtained using the following material for the magnetic pole, that is, a similar Ni-Fe series alloy having saturation magnetic flux density of 1.6 T, a Fe-Co-Ni/Al 2 O 3 / Fe-Co-Ni multi-layer film, a thin film of Ni-Fe thin film containing ZrO 2 , Y 2 O 3 , HfO 2 , Al 2 O 3 or SiO 2 having grain size of 2 nm to 3 nm.
  • the grain size is preferably 0.5 nm to 5 nm. This is because when the oxide grain size is within the above range, only resistivity can be increased without degrading saturation magnetic flux density or the soft magnetic characteristic so much.
  • resistivity can be increased up to approximately 60 ⁇ •cm, and relative permeability shows as a good soft magnetic characteristic as nearly 1000.
  • the high frequency characteristic can be improved by decreasing relative magnetic permeability up to 500 or less.
  • a recording film of a magnetic disk is formed of CoCrTa (adding amount of Cr is 16 at%) having a magnetic coercive force in the recording bit direction of 167112 A/m (2100 Oe) and magnetic coercive force orientation ratio of 1.2.
  • the product Br ⁇ of the residual magnetic flux density and the film thickness of the recording medium is 0.03 T ⁇ nm (300 gauss ⁇ m).
  • the recording medium By employing the recording medium, it is possible to improve the linear recording density characteristic and to substantially decreasing the medium noise in a high linear recording density range.
  • the medium magnetic coercive force is lower than 15915 A/m (200 Oe)
  • the bit error rate is decreased to cause the apparatus disable.
  • the rotating speed of the spindle during recording and reproducing is set to 4491 rpm, and the floating amount of the head at the outermost periphery of the data recording region on the magnetic disk at that time is 0.05 ⁇ m.
  • the linear recording density on each track is set so as to becomes equal from the inner most periphery to the outermost periphery of the data recording region, and the recording frequency at the outermost periphery is set to 67.5 MHz.
  • the linear recording density of data on each of tracks is set to 144 kBPI (kilo Bit Per 25.4 mm (Inch)), the track density is set to 5 kTPI (kiro Track Per 25.4 mm (Inch)), and accordingly areal density is 720 mega-bit per 6.45 cm 2 (square inch).
  • the format capacity of the system is 2.8 giga-bytes
  • the transfer rate is 15 mega-bytes per second.
  • the 8/9 conversion is used for data recording
  • a system having the same performance as this embodiment may be constructed even when the conventional 1-7 method is used for data recording.
  • the recording frequency becomes 45 MHz.
  • the specification of the disk storage system constructed in this embodiment is shown in Table 3. Specification of a 89 mm (3.5 inch) Type Apparatus Memory Capacity 2.8 GB Number of Disks 4 Number of Data Surfaces 8 Number of Heads 8 Number of Tracks/Disk Surface 4427 Maximum Linear Recording Density 144 kBPI Track Density 5 kTPI Rotating Speed 4491 RPM Recording Frequency 67.5 MHz Transfer Rate (to/from Media) 15 MB/sec
  • the magnetic head and the magnetic disks used in this embodiment are the same as those used in Embodiment 6, linear recording density of data on each of tracks is set to 144 kBPI, and track density is set to 5 kTPI.
  • the rotating speed of the spindle is set so that the transfer rate becomes 15 MB/sec for each of the disks.
  • a system having the same performance as this embodiment may be constructed even when the conventional 1-7 method is used for data recording. However, in that case, the recording frequency becomes 45 MHz.
  • Type Apparatus Memory Capacity 1.8 GB Number of Disks 4 Number of Data Surfaces 8 Number of Heads 8 Number of Tracks/Disk Surface 2951 Maximum Linear Recording Density 144 kBPI Track Density 5 kTPI Rotating Speed 6736 RPM Recording Frequency 67.5 MHz Transfer Rate (to/from Media) 15 MB/sec Specification of a 45.72 mm (1.8) inch
  • Two kinds of inductive heads using magnetic poles having different resistivity ⁇ , film thickness d and relative permeability ⁇ are fabricated, and frequency dependence of recording magnetic field intensity for each of the heads is measured using an electron beam tomography method.
  • the magnetic pole material, the magnetic pole thickness d, resistivity ⁇ and relative permeability ⁇ in a low frequency band below 1 MHz for each of the prototype heads are shown in Table 7.
  • the head A comprises a magnetic pole formed of a Ni-Fe alloy single film having the composition described in Embodiment 1 and film thickness of 3 ⁇ m.
  • the head B comprises a magnetic pole formed by laminating Fe-Co-Ni-Mo films of 2.2 ⁇ m film thickness through an Al 2 O 3 intermediate film of 0.1 ⁇ m film thickness, as the same as in Embodiment 4. Thereby, the total thickness of the magmatic pole film of this head is 4.5 ⁇ m.
  • the thickness of the Fe-Co-Ni-Mo film is set to 2.2 ⁇ m.
  • the head C comprises a lower magnetic film of a magnetic pole which is a Co-Ta-Zr amorphous single layer film having film thickness of 3 ⁇ m and resistivity of 90 ⁇ •cm.
  • a magnetic pole which is a Co-Ta-Zr amorphous single layer film having film thickness of 3 ⁇ m and resistivity of 90 ⁇ •cm.
  • Head efficiencies ⁇ are calculated from the measured results of the normalized frequency dependence of recording magnetic field intensity.
  • the recording magnetic field intensity begins to decrease near a point exceeding 10 MHz and the intensity at 100 MHz is attenuated lower than 60 % of the intensity in the low frequency band.
  • the head B uses the Fe-Co-Ni-Mn films having the magnetic permeability and resistivity equivalent to those of the NiFe film used in the head A, the eddy current loss is substantially decreased since the films are of a multi-layer structure through the Al 2 O 3 insulating film.
  • the attenuation of magnetic field intensity at 100 MHz is nearly 20 % and the frequency characteristic is improved.
  • the attenuation of magnetic field intensity at 100 MHz is nearly 0 % and the frequency characteristic is outstanding.
  • an upper and a lower magnetic films are formed by the following method.
  • an inductive head having an upper and a lower magnetic cores which are electroplated through a mask in a plating bath containing Ni ++ of 16.7 g/l, Fe ++ of 2.4 g/l, and a common stress-release agent and a surface-active agent under a condition of pH of 3.0, plating current density of 15 mA.
  • the track width is 4.0 ⁇ m, and gap length is 0.4 ⁇ m.
  • the composition of this magnetic film is 42.4Ni-Fe (weight %), and as to the magnetic characteristics, saturation magnetic flux density (B S ) is 1.64 T, magnetic coercive force in the hard axis direction (H CH ) is 39.289 A/m (0.5 Oe), and resistivity ( ⁇ ) is 48.1 ⁇ •cm.
  • Fig. 22 is a perspective view showing a dual element head
  • Fig. 23 is a plan view of the write.
  • the write head comprises an upper magnetic core 320, a lower magnetic core 321 also serves as an upper shield film, a coil 325.
  • the read head comprises a magnetoresistive element 323, an electrode 324 for conducting sense current to the magnetoresistive element 323 and a lower shield film 322.
  • the write and read heads are formed on a slider 326.
  • This inductive head is mounted on the disk storage system shown in Embodiment 1 to evaluate the recording performance.
  • the medium used has an outer diameter of 3.5 inches and magnetic coercive force of 198943 A/m (2500 Oe).
  • the performance (over-write characteristic) of the recording head according to the present invention evaluated under such a construction shows an outstanding characteristic which is approximately -50 dB at a high frequency band above 40 MHz.
  • a disk storage system of this embodiment employs a dual element head, shown in Fig. 22, which uses an inductive head for recording and a magnetoresistive element for reproducing.
  • the upper magnetic film of the recording magnetic pole of the inductive head is formed as described above.
  • a multi-layer film of Fe-Co-Ni/Al 2 O 3 /Fe-Co-Ni having a single layer thickness of Fe-Co-Ni film of 2.2 ⁇ m is used.
  • the thickness of the Al 2 O 3 intermediate film is set to 0.1 ⁇ m, and the track width of the recording pole is set to 3 ⁇ m.
  • a Ni-Fe alloy film having thickness of 1 ⁇ m is used for the lower shield film 82.
  • a Ni-Fe alloy film having thickness of 15 nm is used for the magnetoresistive element 86 which is driven utilizing a soft film bias method.
  • magnetoresistive element 86 using the Ni-Fe alloy film
  • a spin valve type element composed of an Ni-Fe film, a Cu film, a Co film and an anti-ferromagnetic film of Ni-O series, Fe-Mn series or Cr-Mn series
  • a multi-layer type giant-magnetoresistive element of Co/Cr, Fe/Cr, Co/Cu or NiFe/Cu series a spin valve type element composed of an Ni-Fe film, a Cu film, a Co film and an anti-ferromagnetic film of Ni-O series, Fe-Mn series or Cr-Mn series
  • the disk storage system constructed according to this embodiment can attain the same specification as shown in Table 2.

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Description

  • The invention relates to a thin film magnetic head according to the preamble of claim 1 and to a disk storage system comprising such a thin film magnetic head according to EP 0 012 326 A.
  • As in recent years the recording density of a disk storage system is growing higher and the magnetic coercive force of recording medium is increased, there is required a thin film magnetic head capable of sufficiently recording to the recording medium having high magnetic coercive force.
  • In order to realize this, it is necessary to use a material having a high saturation magnetic flux density (BS) as a core material of the magnetic head. In the past, a 80Ni-Fe alloy film of 3 µm thickness has been used for the material.
  • However, since resistivity of the 80Ni-Fe alloy film is as low as 16 to 20 µΩ·cm, the eddy current loss becomes large in a high frequency band. Therefore, the strength of recording magnetic field of the magnetic head in a high frequency band is decreased, and accordingly the recording frequency is limited to about 30 MHz at maximum.
  • As an alternative material, Co systems amorphous materials, Fe-Al-Si sendust alloy thin film are proposed. However, they are not practically used yet because the former is thermally instable since the material is amorphous, and the latter has a disadvantage in the fabrication process as the magnetic core material for the inductive head since it requires a high temperature heat treatment at nearly 500°C.
  • In recent years, three-element group materials of Co-Ni-Fe are disclosed in JP-60-82,638 A, JP-61-76,642 A, JP-64-8,605, A, JP-2-68,906 A and in JP-2-290,995.
  • Although saturation magnetic flux density (BS) of these three-element system materials is as high as 1.5 T, resistivity is not large and the crystal grain size is not small in the 80Ni-Fe alloy and in addition to this there is a disadvantage in the high frequency characteristic as in the 80Ni-Fe alloy.
  • On the other hand, the memory capacity of the disk storage system is steadily growing year by year, and areal density of a 3.5-inch type disk in production now is increased up to 350 MB/6.45 cm2 (in2).
  • In this case, the data recording frequency is nearly 27 MHz which is near the performance limit of a magnetic head using the 80Ni-Fe alloy film or the Co-Ni-Fe alloy film.
  • Although there is proposed in JP-3-68,744 A a magnetic film for high frequency use formed by adding Nb, Ta, Cr, Mo to (40-50)Ni-Fe through a sputtering method, it is difficult to magnetically form a thick film through sputtering method because the material has large magnetocrystalline anisotropy.
  • EP 0 012 326 A discloses - as closest prior art - a thin film magnetic recording head comprising a lower magnetic layer deposited on a target. Above this layer there is deposited an insulator in which copper coils are embedded. An upper pole piece layer is curved down on one side to form a throat and a gap for reading a magnetic recording medium. On the other side, the upper pole piece layer is curved down to join the lower layer and to form a back gap. The upper layer is deposited by evaporating a metal upon the lower layer applying a resist mask and then electroplating through the mask onto the metal.
  • An object of the invention is to provide a thin film magnetic head and a disk storage system with a magnetic head for high density recording in a high frequency band, capable of performing high speed access and a high transfer rate.
  • This object will be solved by the features of claims 1 and 3, respectively. The thin film magnetic head according to the invention is mounted on a disk storage system according to claim 3 with high transfer rate and high recording density, having a magnetic disk rotated above 4000 rpm when the disk storage system is recording or reproducing, and setting in recording frequency higher than 45 MHz.
  • It is required that the magnetic core of the write head is made of a material having large saturation magnetic flux density (BS), small magnetic coercive force in the hard axis direction and large resistivity.
  • In other words, the range of composition obtainable of large resistivity and high saturation magnetic flux density is a range containing Ni of 38 to 60 wt% for Ni-Fe alloy.
  • However, when a magnetic film having thickness of above 2 pm usually applied to a thin film magnetic head or the like fabricated through a sputtering method, the crystal grain size of the film becomes large, magnetic coercive force in the hard axis direction is large and uniaxial magnetic anisotropy is hardly induced since this composition region is a range where magnetocrystalline anisotropy is largest.
  • Therefore, a plating method has been employed in order to suppress the crystal grain size small, and it has been studied to add the third element such as Co, Mn, Cr, Pd, B, In and the like to a base of 38 to 60 wt% Ni-Fe two-element alloy.
  • The results found are a composition range and a fabrication method of an outstanding thin film having a saturation magnetic flux density (BS) larger than 1.5 T, a magnetic coercive force in the hard axis direction (HCH) smaller than 795,8 A/m (1.0 Oe) and resistivity larger than 40 µΩ•cm with keeping the film thickness of 2 to 5 µm which is required for the recording magnetic field.
  • By using the material for a thin film magnetic head, it is possible to provide a high performance disk storage system having areal density of 500 MB/(6.45 cm2) (in2), a recording frequency of 45 MHz and a transmission speed of above 15 MB/s.
  • In the disk storage system of claim 3 the magnetic disk has a transfer rate larger than 15 mega-bytes per second, an areal density of recording data larger than 500 mega-bits per 6.45 cm2 (square inch) and a diameter of a magnetic disk smaller than 29 cm (3.5 inches).
  • In the thin film magnetic head one end of the upper magnetic film formed on the lower magnetic film, contacts one end of the lower magnetic film, the other end faces the other end of the lower magnetic film through a magnetic gap, thereby the upper magnetic film forming a magnetic circuit having the magnetic gap in the part together with the lower magnetic film, a conductive coil forming a coil having a given number of winding turns passing between both of the magnetic films.
  • A fabrication method of the thin film magnetic head according to claim 1 comprises the steps of forming an upper magnetic film on a lower magnetic film, contacting one end of the upper magnetic film to one end of the lower magnetic film, facing the other end at the upper magnetic film to the other end of the lower magnetic film through a magnetic gap, thereby the upper magnetic film forming a magnetic circuit having the magnetic gap in the part together with the lower magnetic film, and forming a conductive coil having a given number of winding turns passing between both of the magnetic films.
  • In the fabrication method of said thin film magnetic head at least one of the lower and the upper magnetic films is formed by electroplating using a Ni-Fe electroplating bath containing the metallic ion concentration of Ni++ ions of 15 to 20 g/l and Fe++ ions of 2.0 to 2.7 g/l, the ratio of the Ni++ ions and the Fe++ ions ( Ni++/Fe++) being 7 to 8, containing a stress release agent and a surface active agent, the pH being 2.5 to 3.5.
  • Particularly, it is preferable that the thin film magnetic head is formed by electroplating though a mask in a magnetic field under condition of keeping the temperature of the plating bath at 20 to 35°C and the current density of 5 to 30 mA/cm2.
  • Further, it is preferable that the thin film magnetic head described in claim 1, the film being formed using a plating bath each ions added Co ions of 0.4 to 0.6 g/l and/or Cr, Mo, Pd, In, B less than 0.1 g/l, and that the magnetic film is formed by electroplating though a mask in a magnetic field.
  • In the present invention, writing blur due to the recording frequency and fluctuation of an over-write value are prevented by designing the thickness, resistivity and relative permeability of a magnetic film of a magnetic pole for a write head in taking eddy current loss into consideration, and at the same time by setting the data recording frequency to a high value and rotating a magnetic disk fitting to the above head at a high speed.
  • (1) It is preferable to provide a means having a transfer rate higher than 15 mega bytes per second, areal density larger than 500 mega bits per 6.45 cm2 (square inch).
  • (2) It is preferable that when storing of information is performed using a magnetic disk having a diameter smaller than 8,9 cm (3.5 inches), the magnetic disk is rotated at 4000 rpm during recording and reproducing, and the recording frequency is set to a value above 45 MHz.
  • (3) It is preferable to provide a magnetic disk using a metallic film having magnetic coercive force larger than 159154 A/m (2 kOe).
  • (4) It is preferable to set the build-up time of the recording current to a value smaller than 5 nano-seconds (ns).
  • (5) It is preferable that the coil of an inductive head for performing recording of information on a magnetic disk is formed through a thin film process, and the number of terminals is three, and the inductance between the terminals is smaller than 1 micro-henry (µH).
  • (6) It is preferable that the coil of an inductive head for performing recording of information on a magnetic disk is of a two-layer structure, and the number of winding turns in the first layer is equal to that in the second layer, and the direction of the winding is opposite to each other.
  • (7) It is preferable that the coil of an inductive head for performing recording of information on a magnetic disk is of a single-layer structure, and an additional terminal is connected to a position (c) corresponding to one-half of the number of winding turns between the starting point of the coil (a) and the end point of the coil (b), and the current flowing between (c) and (a) and the current flowing between (c) and (b) are in opposite phase to each other.
  • (8) Letting the film thickness of a magnetic film of a core of an inductive head be d (µm), resistivity be ρ (µΩ•cm) and relative permeability at a low frequency be µ, it is preferable to provide a means in which these parameters satisfies the relation µd2/ρ ≤ 500.
  • (9) It is preferable that at least a part of the recording magnetic pole of a magnetic head used for data recording or data recording and reproducing is of a multi-layer structure in which a magnetic layer and an insulator layer are alternatively laminated, and the thickness of the film is thinner than 2.7 µm.
  • (10) It is preferable that the Fe-Ni alloy described above is used for at least the upper magnetic film of the recording magnetic films of a magnetic head used for data recording or data recording and reproducing, and a Co base amorphous alloy or an Fe base amorphous alloy is used for the lower magnetic film.
  • (11) It is preferable that the material of the recording magnetic pole contains at least one kind of Zr, Y, Ti, Hf, Al and Si.
  • (12) It is preferable that the recording magnetomotive force, that is, the product of recording current and number of winding turns of the coil of a magnetic head used for data recording or data recording and reproducing is set to a value larger than 0.5 ampere turns (AT).
  • (13) It is preferable that the resistivity of at least a part of the recording magnetic pole of a magnetic head used for data recording or data recording and reproducing is larger than 40 µΩ•cm and the relative permeability is larger than 500.
  • (14) It is preferable that the recording coil of an inductive head for performing recording of information on a magnetic disk medium is of a single-layer structure, and an additional terminal is connected to a position (c) corresponding to one-half of the number of winding turns between the starting point of the coil (a) and the end point of the coil (b), and the current flowing between (c) and (a) and the current flowing between (c) and (b) are in opposite phase to each other, and a dual element head using a spin valve element and a giant magnetoresistive element is used as the reproducing head.
  • In the high frequency band over the recording frequency of 45 MHz, the head efficiency (efficiency to induce magnetic flux) of the magnetic head is dominated by the eddy current loss. Although in order to decrease the eddy current loss it is most effective to decrease the film thickness of the magnetic core, decreasing of the film thickness causes recording incapability due to shortage in the recording magnetic flux.
  • In order to sufficiently record on a medium having high magnetic coercive force larger than 159154 A/m (2000 Oe); particularly above 183027 A/m (2300 Oe), the film thickness is required to be larger than 2 µm as well as saturation magnetic flux density is required to be high. In general, employing a multi-layer film is for decreasing the eddy current loss, but the head process for coping with the high recording density is difficult to obtain a high accuracy in the dimension.
  • Therefore, it is necessary to decrease the eddy current loss by increasing resistivity of the magnetic core in order to extend the frequency characteristic of the permeability (µ) of the magnetic core up to a high frequency side.
  • The Ni-Fe magnetic film (3 µm film thickness) shows a saturation magnetic flux density (BS) larger than 1.5 T and resistivity ( ρ) of 40 to 50 µΩ•cm when Ni concentration is within the range of 38 to 60 wt%. That is, when the Ni concentration is below 38 wt%, the specific resistivity (ρ) is large, but saturation magnetic flux density (BS) becomes lower than 1.5 T.
  • On the other hand, when the Ni concentration is above 60 wt%, saturation magnetic flux density (BS) also becomes lower than 1.5 T. Especially, it is preferable that the concentration of Ni is 40 to 50 wt%.
  • A plating process is suitable for fabricating a film having such a composition. That is, since the crystal grain size can be made very small by an electroplating method, magnetic coercive force can be made small and the orientation of crystal can be decreased as low as possible even in a case of such a composition having large magnetocrystalline anisotropy. For example, it is preferable that the orientation ratio of crystal is suppressed below 5.0, that is (1 1 1)/(2 0 0) < 5.0.
  • The composition of a plating bath for fabricating such a film is that the Ni and Fe ion concentrations are Ni++: 15 to 20 g/l, Fe++: 2.0 to 2.7 g/l, and the ion ratio (Ni++/Fe++) is 7 to 8. In this case, plating current density is 10 to 20 mA/cm2, the pH is 3.0, and the bath temperature is 30°C.
  • On the other hand, in the case of adding at least one kind of the elements Co, Mo, Cr, B, In and Pd, it is preferable that the Co is less than 15 wt% and the Mo is less than 3 wt% in order to keep saturation magnetic flux density (Bs) higher than 1.5 T and resistivity (ρ) larger than 4 0 µΩ•cm.
  • In a case of using Co as a component in the bath, it is preferable to add up to CoSO4•6H2O of 100 g/l (Co ions of 21 g/l), and in a case of Mo, Na2MoO4•2H2O of 4.8 g/l (Mo ions of 1.9 g/l). For example, in a case of adding Cr [Cr2(SO4)3•18H2O] instead of Mo, the same effect can be observed. In a case of adding B or In, resistivity (ρ) is increased not so large as about 10%.
  • On the other hand, in the case of adding Co, saturation magnetic flux density (BS) is increased by nearly 10% though resistivity (ρ) of the film is slightly deceased. Therefore, it is preferable to use Co together with Mo. Further, since Co increases the anisotropic magnetic field (HK), Co is preferable for stabilizing the magnetic characteristic.
  • When Co is added more than 15 wt%, saturation magnetic flux density (BS) of the film is increased, but resistivity (ρ) of the film is decreased too small. Therefore, resistivity (ρ) of the film cannot be increased up to a desired value unless a large amount of Mo, Cr are added.
  • This is not preferable because the magnetic coercive force of the film becomes large. In order to increase resistivity (ρ) without increasing the magnetic coercive force of the film, the adding amount of Mo, Cr should be limited to 3 wt% or less.
  • In the case of adding B, In, Pd or the like, the adding amount should be limited as the same as above. In these cases, the plating condition may be the same as in the case of a Ni-Fe magnetic film as described above.
  • Assuming that the high frequency loss (tan δ) of the magnetic film is only the eddy current loss, the high frequency loss can be expressed by the following equation. tan δ = µ"/µ' = R/ωL = µ0µπd2f/Cρ where µ' and µ" are a real part and an imaginary part of the complex magnetic permeability. C is a constant determined by the shape of the film, and µ0 is permeability of vacuum.
  • From the above equation (1), when relative permeability µ inherent to the magnetic film, the film thickness d, resistivity ρ are given, the eddy current loss tan δ corresponding to the frequency f can be obtained. Since the change of the head efficiency (efficiency to induce magnetic flux) corresponding to the frequency is proportional to the change in the real part of the complex permeability, the frequency dependence of the head efficiency can be obtained by calculating δ from Equation (1) and taking the cosine component.
  • That is, the head efficiency η for each frequency can be expressed by the following equation. η = cos[arctan(µ0µπd2f/Cρ)]
  • From Equation (2), by specifying the value µd2/ρ which can be obtained from relative permeability µ inherent to the magnetic film, the film thickness d and resistivity ρ, the head efficiency η for an arbitrary frequency f can be extrapolated.
  • By combining the above head and a magnetic disk using a metallic magnetic film having magnetic coercive force larger than 159154 A/m (2 kOe) which is small in write blurring during high frequency recording and in fluctuation of overwriting, it is possible to obtain a high performance disk storage system having areal density larger than 500 MB/6.451 cm2 (in2), a recording frequency higher than 45 MHz and a transfer rate higher than 15 MB/s.
  • In a case of using a fast and wide SCSI (Small Computer System Interface) having a data bus of two-byte width as an I/O interface, from the relationship between a price of an input/output device and a transfer rate per one magnetic disk device composing the input/output device, it is possible to transmit data up to 20 MB/s at maximum when the fast and wide SCSI having a data bus of two-byte width as an I/O interface is used.
  • In this case, when the transfer rate per one magnetic disk device is above 15 MB/s, it can be understood that the price of the input/output device can be decreased.
  • Further, when the capacity per one magnetic disk device is 550 MB, it is possible to handle an OS (Operation Software) such as Windows, Workplace and the like. In order to realize this capacity with one magnetic disk of 89 mm (3.5 inch) type, areal density capable of recording the data is required to be 500 MB/6,45cm2 (in2).
  • According to the present invention, a recording head, which is capable of performing sufficient recording to a medium having a high magnetic coercive force and at a high frequency range, is fabricated by a specified composition and through a low cost electroplating method.
  • Thereby, it is possible to obtain a disk storage system with a high recording density capable of a high rate transfer, decreasing access time and increasing memory capacity by keeping a transfer rate higher than 15 MB/s, a recording frequency higher than 45 MHz, and a rotating speed of a magnetic disk higher than 4000 rpm.
  • Brief Description of Drawings:
  • Fig. 1 is a perspective view showing a disk storage system;
  • Fig. 2 is a cross-sectional view showing a disk storage system;
  • Fig. 3 is a front view showing a disk storage system;
  • Fig. 4 is a plan view showing a disk storage system;
  • Fig. 5 is an assembled view of a magnetic head and a supporting device;
  • Fig. 6 is an assembled view of a magnetic head and a supporting device;
  • Fig. 7 is a perspective view showing a slider having a thin film magnetic head;
  • Fig. 8 is a perspective view showing a dual element head;
  • Fig. 9 is a graph showing the relationship between frequency and overwrite;
  • Fig. 10 is a graph showing the relationship between crystal grain size and magnetic coercive force in the hard axis direction;
  • Fig. 11 is a cross-sectional view showing an inductive head;
  • Fig. 12 is a plan view showing an inductive head;
  • Fig. 13 is a plan view showing the construction of a film of a magnetoresistive head;
  • Fig. 14 is a view showing the construction of a film of a magnetoresistive head;
  • Fig. 15 is a view showing the construction of a film of a magnetoresistive head;
  • Fig. 16A is a graph showing the relationships between content of Ni or (Ni/Fe) ratio and BS;
  • Fig. 16B is a graph showing the relationships between content of Ni or (Ni/Fe) ratio and ρ;
  • Fig. 16C is a graph showing the relationships between content of Ni or (Ni/Fe) ratio and HCH;
  • Fig. 17A is a graph showing the relationship between content of Mo and BS;
  • Fig. 17B is a graph showing the relationship between content of Mo and ρ;
  • Fig. 17C is a graph showing the relationship between content of Mo and HCH;
  • Fig. 18A is a graph showing the relationship between content of Mo and BS;
  • Fig. 18B is a graph showing the relationship between content of Mo and ρ;
  • Fig. 18C is a graph showing the relationship between content of Mo and HCH;
  • Fig. 19 is a graph showing the relationship between frequency and (µf/µ1MHz);
  • Fig. 20 is a plan view showing a thin film magnetic head;
  • Fig. 21 is a cross-sectional view showing a thin film magnetic head;
  • Fig. 22 is a perspective view showing a dual element head; and
  • Fig. 23 is a plan view showing an inductive head.
  • Description of the Invention:
  • Hereinafter, various embodiments of a disk storage system, a thin film magnetic head therefor and a fabrication method thereof according to the present invention will explained referring to drawings.
  • Embodiment 1
  • Fig. 1 and Fig. 2 are a whole view and a plan view showing an embodiment of a disk storage system in accordance with the present invention. The disk storage system is composed of a magnetic disk 1 for recording information, a DC motor (not shown in the figures) for a means to rotate the magnetic disk, a magnetic head 2 for writing and reading the information, a positioning device for a means to support the magnetic head 2 and change the position of the magnetic head 2 to the magnetic disk 1 which is composed of an actuator 4, a voice coil motor 5 and an air filter 6 for keeping the inside of the system clean.
  • The actuator 4 is composed of a carriage 7, a rail 8, a bearing 9. The voice coil motor 5 is composed of a voice coil 10 and a magnet 11. These figures show an example where eight magnet disks are attached to a single rotating shaft to make the memory capacity large.
  • Fig. 3 is a front view of a disk storage system in accordance with the present invention, and Fig. 4 is a plan view of the disk storage system. In the figures, the reference character 1 is a magnetic disk, the reference character 2 is a magnetic head, the reference character 3 is a gimbals system supporting device, and the reference character 4 is a positioning device (actuator).
  • The magnetic disk 1 is rotated in the direction of the arrow a by a rotating driving mechanism. The magnetic head 2 is supported by the supporting device 3 and moved in the direction of the arrow b1 or b2 on the rotating diameter O1 and positioned, and thereby to perform magnetic recording or reproducing using a proper one of cylinders T1 to Tn.
  • The magnetic disk 1 is a medium having a surface roughness RMAX less than 10 nm (100 Å) preferably a medium having a better surface condition of a surface roughness less than 5 nm (50 Å).
  • The magnet disk 1 is made by forming a magnetic recording film on the surface of a rigid substrate through a vacuum film forming method. The magnetic recording film is formed as a magnetic thin film made of γ-Fe2O3 or Co-Ni, Co-Cr or the like.
  • Since the film thickness of the magnetic recording film formed through the vacuum film forming method is thinner than 0.5 µm, the surface characteristic of the rigid substrate directly reflects on the surface characteristic of the recording film.
  • Therefore, the rigid substrate having a surface roughness RMAX less than 10 nm (100 Å) is used. A rigid substrate having the major component of glass, chemically reinforced soda-alumina silicate glass or ceramic is suitable for such a rigid substrate.
  • The magnetic recording film may be formed of a magnetic iron oxide such as γ-Fe2O3 or the like or a magnetic nitride. In a case where the magnetic film is a metal or an alloy, it is preferable that an oxide film or a nitride film is provided on the surface or an oxide covering film is formed on the surface. It is also preferable to use a carbon protecting film.
  • By doing so, the durability of the magnetic recording film is improved and accordingly the magnetic disk 1 is prevented from damage which may be caused in a case where recording or reproducing is performed under a very low floating condition or at a contact-start-stop condition.
  • The oxide film or the nitride film may be formed through reactive sputtering, reactive vapor depositing or the like. The oxide coating film may be formed by intentionally oxidizing the surface of the magnetic recording film made of a metal or an alloy containing at least one kind of iron, cobalt and nickel such as Co-Ni or Co-Cr through reactive plasma treatment or the like.
  • The magnetic disk 1 may be either of perpendicular recording type where the recording residual magnetization in the magnetic recording film has a component in the perpendicular direction to the film surface as the major component, or of a longitudinal recording type where the recording residual magnetization has a longitudinal component as the major component.
  • It is also possible to apply a lubricant on the surface of the magnetic recording film though its figure is omitted here.
  • Fig. 5 and Fig. 6 are views showing the assembled construction of the magnetic head 2 and the gimbals system supporting device 3.
  • The magnetic head 2 has reading and writing elements 22 in the side of an air flow-out end of a slider 25 of a ceramic structure body and supported by the supporting device 3 driven by a positioning device 4 so as to be allowed pitching motion and rolling motion by adding a load on the surface 24 opposite to a floating surface 23. The reading and writing element 22 is a thin film element formed through the same process as that of IC fabricating technology.
  • The supporting device 3 is constructed by attaching and fixing one end of a supporting body 37 formed of an elastic metallic sheet to a rigid arm part 51 attached to the positioning device 4 using jointing members 12, and by attaching a flexible body 36 formed of a similar metallic sheet to a free end on the other end in the lateral direction of the supporting body 37, and by attaching the magnetic head 2 on the underside surface of the flexible body 36 (refer to Fig. 3 and Fig. 4).
  • The portion of the supporting body 37 attached to the rigid arm part 51 has an elastic spring part 41, and forms a rigid beam part 42 by connecting to the elastic spring part 41. The rigid beam part 42 has flanges 42a, 42b formed by bending on the both sides.
  • The flexible body 36 comprises two outer flexible frame parts 31, 32 extending nearly in parallel to the axial line in the lateral direction of the supporting body 36, and a side frame 33 jointing the outer flexible frame parts 31, 32 in the end far from the supporting body.
  • The flexible body 36 comprises further a middle tongue-shaped part 34 having one end as a free end extending from near the middle portion of the side frame 33 along and nearly in parallel to the outer flexible frame parts 31,32 and the one end in the opposite side to the side frame 33 is attached to the vicinity of the free end of the supporting body 37 by welding or the like.
  • On the upper surface of the middle tongue-shaped part 34 of the flexible body 36, a projection 35 for load, for example, a semi-spherical projection is provided, and a load is transmitted from the free end of the supporting body 37 to the middle tongue-shaped part 34. The surface 24 of the magnetic head 2 is fixed to the under surface of the middle tongue-shaped part 34 by adhesive.
  • In this embodiment, a magnetic disk 1 having a surface roughness RMAX is used and the floating amount g at starting of floating the magnetic head 2 is set within the range of 0.01 µm to 0.04 µm.
  • The floating amount g of the innermost cylinder Tn among the reading and writing cylinders T1 to Tn provided in the magnetic disks 1 is set between the floating amount g at starting of floating of 0.01 µm to 0.04 µm and a value several times of the floating amount.
  • The shape of the slider 25 constructing the magnetic head 2, the load applied from the supporting device 3 to the magnetic head 2, the rotating speed of the magnetic disk 1 and so on are set so as to obtain the floating amount as described above.
  • Fig. 7 is a perspective view showing a negative pressure slider. The load slider 70 comprises an air intake surface 71 and a negative pressure generating surface 73 surrounded by two positive pressure generating surfaces 72, 72 for generating the floating force, and a groove 74 having a step larger than the negative pressure generating surface 73 in the boundary between the air intake surface 71, the two positive pressure generating surfaces 72, 72 and the negative pressure generating surface 73.
  • On an air outlet end 75, the negative pressure slider 70 also has thin film magnetic head elements 76 for recording and reproducing information on and from a magnetic disk 1.
  • During floating of the negative pressure slider 70, the air introduced through the air intake surface 71 is expanded at the negative pressure generating surface 73. At that time, since an air flow flowing toward the groove 74 is also generated, there exists inside the groove 74 an air flow flowing from the air intake surface 71 toward the air outlet end 75.
  • Therefore, dust floating in air is forced to flow by the air flow inside the groove 74 and is exhausted from the air outlet end 75 to the outside of the negative pressure slider 70 even if the dust floating in air is entered into the air intake surface 71 during floating of the negative pressure slider 70.
  • Further, since there is an air flow and not exists stagnation inside the groove 74 during floating of the negative pressure slider 70, dust is not accumulated the inside.
  • Fig. 8 is a conceptual view of a dual element head forming a recording head. The dual element head comprises an inductive head and a reproducing head, and a shield part for preventing disturbance in the reproducing head due to leakage magnetic flux.
  • Although mounting of the recording head for a perpendicular magnetic recording is shown in this embodiment, the magnetoresistive element according to the present invention may be used for a perpendicular recording by combining with a head for vertical magnetic recording.
  • The head is formed with a reproducing head composed of a lower shield film 82 on a substrate 80, a magnetoresistive film 86, an electrode 85 and an upper shield film 81, and a recording head composed of a lower magnetic film 84, a coil 87 and an upper magnetic film 83.
  • By using this head, signals are written in on the recording medium and signals read out from a recording medium. The magnetic gap between the sensing part of the reproducing head and the recording head can be positioned at the same track at a time by forming at an overlapping position on the same slider, as described above. This head is formed in a slider and mounted on a disk storage system.
  • In this embodiment, the upper and the lower magnetic films of the inductive head are formed through the following fabrication method.
  • There is fabricated an inductive head having an upper and a lower magnetic cores which are electroplated in a plating bath containing Ni++ of 16.7 g/l, Fe++ of 2.4 g/l, and a common stress-release agent and a surface active agent under a condition of pH of 3.0, plating current density of 15 mA. The track width is 4.0 µm, and gap length is 0.4 µm.
  • The composition of this magnetic film is 42.4 Ni-Fe (wt %), and as to the magnetic characteristics, saturation magnetic flux density (BS) is 1.64 T, the magnetic coercive force in the hard axis direction (HCH) is 39.789 A/m (0.5 Oe), and resistivity (ρ) is 48.1 µΩ•cm.
  • The inductive head comprises an upper magnetic core 83, a lower magnetic core 84 also serves as an upper shield film, a coil 87, a magnetoresistive element 86, an electrode 85 for conducting sense current to the magnetoresistive element, a lower shield film 82 and a slider 80.
  • Fig. 9 shows the evaluated result of the performance (over-write characteristic) of the recording head according to the present invention having such a construction. An outstanding recording characteristic of nearly -50 dB in a high frequency range above 40 MHz have been obtained.
  • Fig. 10 shows the relationship between magnetic coercive force in the hard axis direction and average crystal grain size of magnetic films obtained through the plating method and the sputtering method in this embodiment. It can be understood that when the crystal grain size is smaller than 50 nm (500 Å), low magnetic coercive force lower than 79.577 A/m (1.0 Oe) can be obtained.
  • Further, for the lower magnetic film, a Ni-Fe alloy thin film composed of Ni 70 to 80 wt%, Fe of the remainder may be formed through electroplating, as the same way described above, or the alloy film may be also formed through sputtering method.
  • Fig. 11 is a cross-sectional view and Fig. 12 is a plan view showing an inductive head according to the present invention. The thin film head comprises an upper shield film 81, a lower magnetic film 84 attached onto the upper shield film and an upper magnetic film 83 which are made of the aforementioned magnetic film.
  • Fig. 11 is a cross-sectional view being taken on the plane of the line A-A of Fig. 12. A non-magnetic insulator body 89 is put between the films 83 and 84. A part of an insulator body determines a magnetic gap 88, and this interacts in a conversion relationship with, for example, a magnetic medium placed in an air-bearing relation, as the prior art.
  • A supporting body serves as a slider having an air-bearing surface (ABS), and this accesses to and is in a floating relation with a rotating disk during disk file operation.
  • The thin film magnetic head has a back gap 90 formed by connecting an upper magnetic film 83 with a lower magnetic film 84. The back gap 90 is separated from the magnetic gap by a coil 87 interposed between.
  • The continuing coil 87 forms a layer formed on the lower magnetic film 84, for example, through plating to electromagnetically couple with the lower magnetic film. The coil 87 has an electric contact point 91 in the center of coil which is berried with insulator body 89, and also has a large area as an electric contact point 92 in the outer end terminal point of the coil. The contact points are connected to external lead wires and reading and writing signal processing head circuit (not shown).
  • In the present invention, the coil 87 formed in a single layer is slightly deformed elliptical, and the portion having small cross-sectional area is placed in the nearest position to the magnetic gap and the cross-sectional area gradually increases as the distance from the magnetic gap increases.
  • The back gap 90 positions relatively near the ABS of the magnetic gap. However, there exists relatively densely many windings of the elliptical coil between the back gap 90 and the magnetic gap 88, and the width or the cross-sectional diameter of the coil is small in this region. The large cross-sectional diameter in the farthest region from the magnetic gap decreases the electrical resistance.
  • The elliptical coil does not have any angle or sharp corner or edge, and therefore resistance to current is small. Further, the total length of conductor of the elliptical coil is short compared with a rectangular or a circular (ring-shaped) coil.
  • From these advantages, the total resistance of the coil is relatively small, consequently heat generation is small, and heat is properly radiated. Since heat generation is substantially decreased, collapse, extension and expansion of the thin film are prevented and the cause of ball-tip projection is eliminated.
  • The shape of the elliptical coil, width of which uniformly changes, can be formed through a conventional economical technology such as sputtering or vapor deposition method.
  • In a coil having a different shape, particularly a shape having corners, plating deposition is apt to become non-uniform in width. A coil removed corners or sharp edge portions is subjected to small mechanical stress.
  • In this embodiment, a nearly elliptical coil having multiple winding turns is formed between magnetic cores, the cross-sectional diameter of the coil gradually expands from the magnetic gap toward the back gap, the signal output power is increased and the heat generation is decreased.
  • Fig. 13 is a conceptual view showing the construction on the surface of a substrate of a magnetoresistance effect element in accordance with the present invention formed on the bottom portion of the above mentioned inductive head.
  • The magnetoresistive film 110 is formed along a surface 183 opposed to a recording medium in a long rectangular shape having a width 143 of the element on a substrate 150. This definition on the shape has an effect to provide a proper shape magnetic anisotropy in the perpendicular direction with respect to a direction in which the magnetic field to be detected by the magnetoresistive film 110 is applied.
  • A current is conducted in the magnetoresistive film 110 from electrodes 140 electrically contacting to the film, and an output is obtained from the resistance change of the film caused by the magnetic field applied to the magnetic field detecting portion having the size of the width 141 in the direction parallel to and the width 142 in the direction perpendicular to the surface of the recording medium.
  • Although in this conceptual view the end portions of the magnetoresistive element are exposed to the opposite surface to the recording medium, the mechanical durability of the element can be increased by arranging a yoke-shaped soft magnetic body on the opposite surface to guide the magnetic field from a recording medium and by magnetically coupling to a magnetoresistive element arranged inside.
  • Especially, the resistance of the magnetic circuit is reduced and the sensitivity can be improved by decreasing the MR height of the element.
  • The magnetoresistive element according to the present invention has a construction, for example, as shown in Fig. 14. The magnetoresistive element is formed by laminating on a substrate 150 a magnetoresistive film 110, that is, a bias film 132, a magnetic film 111, a non-magnetic conductive film 120, a magnetic film 112, a non-magnetic conductive film layer 120, a magnetic film layer 111, a bias film 131, and further on the laminated layer by electrically jointing an electrode 140.
  • In the construction of the element shown in Fig. 12, an electrode 140 is placed under a bias film 131. This is an example of effective constructions in a case where an insulator film such as nickel oxide film is used for the upper bias film.
  • Another construction of the electrode may be formed in such a manner, for example, that a bias film is partially formed and then an electrode is formed over the bias film. There are still other methods where a conductive bias film, for example, Fe-Mn film, Co-Pt film or the like is formed and then an electrode is formed directly on the conductive bias film.
  • The present element is constructed by alternatively laminating a magnetic film applied with a strong anisotropy by a bias film, a magnetic film applied with a weaker anisotropy than the above anisotropy by uniaxial magnetic anisotropy, a shape magnetic anisotropy or a soft film bias through a non-magnetic conductive film so as to conduct current to each other but not cause magnetic coupling between them. Especially, the applying direction of the anisotropy will be described below.
  • Fig. 15 is a conceptual view showing an example of anisotropy control in a magnetoresistive element in accordance with the present invention, and is a perspective view of a part of the element shown by A-A' of Fig. 14.
  • The bias films 131 and 132 apply anisotropy by switched connection in the directions indicated by the arrows 171 and 172 in the figure. The arrow 160 in the figure indicates the direction of the magnetic field to be detected, and the arrow 161 indicates the direction of unidirectional magnetic anisotropy induced in the magnetic film 111.
  • The easy magnetizing direction of the magnetic film 112 sandwiched by the non-magnetic conductive films 120 is applied in the direction indicated by the arrow 162 in the figure by induction of uniaxial magnetic anisotropy. This can be attained by applying a magnetic field in a proper direction during growing the magnetic film.
  • The embodiment shown by the figure is an example where application of the anisotropy is attained by the bias film and the inductive magnetic anisotropy. As a result, the arrows 161 and 162 intersect at right angle with each other on the surface of the film.
  • By setting so that anisotropy of the magnetic film 111 is larger and anisotropy of the magnetic film 112 is smaller than the magnitude of the magnetic field to be detected, the magnetization of the magnetic film 111 can be fixed to a nearly constant value and only the magnetization of the magnetic film 111 can largely react to an external magnetic field.
  • Further, the magnetization of the magnetic film 111 is in a state of easy axis excitation with respect to the magnetic field to be detected where the directions of magnetization and external magnetic field are parallel to each other by anisotropy 161.
  • On the other hand, the magnetization of the magnetic film 112 is in a state of hard axis excitation where the directions of magnetization and external magnetic field are perpendicular to each other. With this effect, the response described above becomes further outstanding.
  • In addition to this, the element becomes capable of operating at a high frequency since there appears a state where the element is driven by an external magnetic field in the hard axis excitation due to rotation of the magnetization of the magnetic film 112 with respect to the direction of the arrow 162 as an origin and accordingly the noise accompanied by excitation of movement of magnetic domain wall is prevented.
  • There is another embodiment of magnetoresistive element in which application of anisotropy is performed by two different kinds of bias films, that is, an anti-ferromagnetic film and a hard-magnetic film.
  • The magnetoresistive element is formed by laminating on a substrate 150 an anti-ferromagnetic film 132, a magnetic film 111, a non-magnetic film 120, a magnetic film 112 and a hard-magnetic film 133, and then by connecting an electrode on the laminated film. Both of the anti-ferromagnetic film 132 and the hard-magnetic film 133 are respectively fixed to two films of the magnetic films 111, 112 separated by the non-magnetic film.
  • The directions of magnetization of the magnetic films 111 and 112 are induced in the directions indicated by the arrows 161 and 162 respectively by performing thermal treatment under magnetic field or magnetizing treatment in the directions 172 and 173, a parallel direction and a perpendicular direction to the direction 160 of the magnetic field to be detected.
  • The anti-ferromagnetic film is formed of, for example, nickel oxide, and the hard-magnetic film is formed of a cobalt-platinum alloy. The same effect may be obtained when the positions of the hard-magnetic film and the anti-ferromagnetic film are reversed, or the directions of induced magnetization are reversed.
  • The films composing the magnetoresistive element according to the present embodiment are fabricated using a high frequency magnetron sputtering apparatus in a manner as follows.
  • Magnetoresistive elements have been fabricated by successively laminating the following materials on a ceramic substrate and a Si single crystal substrate of 1 mm thickness and 76.2 mm (3 inches) diameter in an argon atmosphere of 4 mbar (3 mill-Torrs). As a sputtering target used are targets of nickel oxide, cobalt, a nickel-20 at% iron alloy and copper.
  • Addition of cobalt to nickel-20 at% iron is preformed by placing a cobalt chip on a nickel-20 at% iron target. Addition of nickel and iron to cobalt is performed by placing nickel and iron chips on a cobalt target.
  • The laminated film is formed by applying a high frequency electric power to each cathode placing each of the targets to generate a plasma inside the system and then by opening and closing a shutter provided each of the cathodes one by one to form each of the films successively.
  • During forming the films, a magnetic field of approximately 3978.85 A/m (50 Oe) is applied in parallel to the substrate using two pairs of magnets crossing at right angle to each other on the surface of the substrate to form uniaxial magnetic anisotropy in the film and to induce the direction of the switched connection bias of a nickel oxide film to each direction.
  • Induction of anisotropy is performed by applying a magnetic field in the direction to be induced during forming each magnetic film using two pairs of magnets provided near a substrate. Otherwise, the direction of anti-ferromagnetic bias is induced in the direction of a magnetic field by performing heat treatment under magnetic field at a temperature near the Neel temperature of the anti-ferromagnetic film after forming the multi-layer film.
  • Evaluation of performance of the magnetoresistive element is conducted by patterning the film in a rectangular shape and forming electrodes. In this time, the patterning and electrode forming are performed so that the direction of uniaxial magnetic anisotropy of the magnetic film becomes parallel to the direction of current in the element.
  • The measurement is performed by conducting a constant current between the electrode terminals, applying a magnetic field in the surface of the element in the direction perpendicular to the direction of current flow, measuring the electrical resistance of the element as the voltage between the electrode terminals, and detecting the measured results as the magnetoresistance ratio.
  • In Table 1, the characteristic of the element is expressed by the magnetoresistance ratio and the saturation magnetic field. The reproducing output of the element corresponds to the largeness of the magnitude of the magnetoresistance ratio and the sensitivity corresponds to the smallness of the magnitude of the saturation magnetic field.
  • It is clear from the result of Table 1 that the magnetoresistive elements No. 1 to No. 5 have a magnetoresistance ratio larger than 4% and a better magnetic characteristic, and are outstanding particularly in the resistance changing rate compared to No. 6 and No. 7.
  • Among them, the specimen No. 1, No. 2, No. 4 show an excellent magnetic field sensitivity of about 795.77 A/m (10 Oe) saturation magnetic field and a high output of 6 to 7% magnetoresistance ratio.
    Spe. Composition/Thickness of film (Å) MS HS
    No.1 NiO/NiFe/Cu/NiFe/Cu/NiFe/NiO
    300/ 60 /21/ 40 /21/ 60 /300
    6.5 12
    2 NiO/Co/Cu/NiFe/Cu/Co/NiO
    300/50/21/ 40 /21/50/300
    7.2 13
    3 NiO/NiFe/Cu/NiFe/Cu/NiFe/Cu/NiFe/NiO
    300/ 60 /21/ 40 /21/ 40 /21/ 60 /300
    5.5 11
    4 NiO/Co/Cu/Co/NiFe/Co/Cu/Co/NiO
    300/60/21/15/ 40 /15/21/60/300
    7.5 16
    5 NiO/NiFe/Cu/NiFe
    300/ 60 /21/ 40
    4.5 15
    6 NiFe/Cu/NiFe/NiO
    60 /21/ 40 /300
    3.0 14
    7 NiFe/Cu/NiFe/NiO
    60 /21/ 40 /150
    3.9 10
    Note
    Spe.: specimen, MR: magnetoresistance ratio (%)
       HS: saturation magnetic field (Oe)
       1 Oe = 79.577 A/m
  • In the disk storage system of the present embodiment, the region sandwiched by a pair of electrode 85, which becomes a reproducing track width, is set to 2 µm. During recording, current of 15 mAop is conducted to the coil 87 having 20 winding turns to record any information on a medium.
  • On the other hand, during reproducing, direct current of 8 mA is conducted to the lead wire to detect leakage magnetic field from a medium.
  • A disk storage system is constructed by combining this magnetic head with a 89.0 mm (3.5 inch) magnetic disk with a CoCrTa (adding amount of Cr is 16 at%) recording film having a magnetic coercive force in the recording bit direction of 167122 A/m (2100 Oe) and a magnetic coercive force orientation ratio of 1.2.
  • The production Br·δ of the residual magnetic flux density and the film thickness of the magnetic disk recording film used hear is 100 Gauss•µm. The specification of the magnetic memory apparatus constructed in this embodiment is shown in Table 2.
    Specification of a 89.0 mm (3.5 inch) Type Apparatus using a Dual Element Head
    Memory Capacity 5.5 GB
    Number of Disks 4
    Number of Data Surfaces 8
    Number of Heads 8
    Number of Tracks/Disk Surface 7378
    Maximum Linear Recording Density 170 kBPI
    Track Density 8.3 kTPI
    Rotating Speed 4491 RPM
    Recording Frequency 80.0 MHz
    Transfer Rate (to/from Media) 18 MB/sec
  • Embodiment 2
  • Figs. 16A, 16B and 16C are graphs showing the relationships between component of magnetic film, magnetic characteristics and resistivity (ρ) when metallic ion concentrations, that is, amounts of Ni++ and Fe++ in a plating bath are varied.
  • Ni++ is added using NiCl2•6H2O, Fe++ is added using FeSO4•7H2O, and a common stress release agent and a surface active agent are added. Plating is performed under a condition of pH of 3.0 and plating current density of 15 mA/cm2. The film thickness is 3.0 µm.
  • It can be understood that when the content of Ni in the film is within the range of 38 to 60 wt%, the saturation magnetic flux density (BS) is larger than 1.5 T and resistivity (ρ) is larger than 40 µΩ•cm, that is, the film has outstanding characteristics in that saturation magnetic flux density (BS) is 1.5 times as large as and resistivity (ρ) is twice as large as those of well known 80Ni-Fe permalloy film.
  • Further, the magnetic coercive force in the hard axis direction (HCH) is smaller than 79.577A/m (1 Oe), similar to 80Ni-Fe permalloy. The varying trends of saturation magnetic flux density (BS) and resistivity (ρ) are nearly the same as those of the bulk material, but the decreasing rates as the Ni content increases are smaller than those of the bulk material. The reason is that the film has a very small crystal grain size of 4 to 8 nm (40 to 80 Å) compared with that of the bulk material.
  • Such characteristics are not largely varied when the pH is varied within the range of 2.5 to 3.5, and the plating current density is varied within the range of 5 to 30 mA/cm2. When the plating bath temperature is varied within the range of 25 to 35 °C, the content of Ni is slightly increased as the temperature is increased, but the characteristics themselves are not affected.
  • The magnetic film of the present embodiment is suitable for an upper magnetic core of an inductive head having a lower magnetic core using an Fe-Ni series alloy containing Ni of 70 to 80 wt%, but the film may be used both of the upper and the lower magnetic cores.
  • Especially, as shown in Figs. 16A, 16B and 16C, BS shows the highest value of 1.6 T at Ni of 40 to 50 wt%, and it is preferable to combine with a film having an (Ni/Fe) ratio of 0.667 to 1.00. Incidentally, the (Ni/Fe) ratio of a film having Ni of 38 to 60 wt% is 0.613 to 1.50.
  • Embodiment 3
  • Figs. 17A, 17B and 17C show test results on the magnetic characteristics and resistivity (ρ) of a magnetic film containing Mo in a (Ni 44 wt%-Fe) series alloy.
  • That is, the figure shows the magnetic characteristics and resistivity (ρ) of a magnetic film formed by adding Mo as an element to increase resistivity (ρ) to a plating bath containing N++ of 16.7 g/l and Fe++ of 2.2 g/l. The Mo is added using Na2MoO4•4H2O by 5 g/l at maximum.
  • It can be understood that resistivity (ρ) of the magnetic film is increased in proportion to the amount of added Mo. For example, resistivity (ρ) of the magnetic film having Mo of 2 wt% shows above 60 µΩ•cm which is about three times as large as that of the 80Ni-Fe permalloy film.
  • In this case, the saturation magnetic flux density (BS) is decreased only 5% and nearly 1.50 T which is 1.5 times as high as that of the 80Ni-Fe permalloy film.
  • However, it is undesirable to add an amount of Mo exceeding 3 wt% (Mo of 5 g/l on the base of Na2MoO4•4H2O) since magnetic coercive force in the hard axis direction (HCH) becomes above 79.577 A/m (1 Oe) and saturation magnetic flux density (BS) becomes below 1.5 T.
  • Adding of Cr, instead of Mo, has been studied, and the results are nearly the same as in the case of adding Mo. The magnetic film of this embodiment may be used in the same way as in the previous embodiments.
  • Embodiment 4
  • Figs. 18A, 18B and 18C show test results on an (Ni 44 wt%-Fe)-Co 15 wt%-Mo magnetic film to which Co and Mo are added at a time in order to further increase saturation magnetic flux density (BS) and resistivity (ρ) without degrading the magnetic characteristics of the magnetic film.
  • The Co is added using CoSO4•7H2O, and the Mo is added using Na2MoO4•4H2O, as the same as in Embodiment 3. The examples shown are in a case where the adding amount of Co is a constant of 13 wt% (100 g/l on the base of CoSO4•7H2O) and on the other hand the adding amount of Mo is varied up to 4 wt%.
  • As a result, by adding Co of 13 wt% saturation magnetic flux density (BS) of the magnetic film is increased by 10 % and becomes 1.78 T. However, resistivity ( ρ) is decreased by 30 % and is 35 µΩ•cm. By adding Mo resistivity (ρ) is recovered. By adding Mo of 2.5 wt%, resistivity (ρ) is increased by nearly 20% on the contrary and becomes 55 µΩ•cm.
  • In this case, saturation magnetic flux density (BS) is 1.55 T which is slightly higher value than the film without Co. Further, since addition of Co increases anisotropy of a film, magnetic characteristic of the film is stabilized.
  • The magnetic film of this embodiment may be used in the same way as in the previous embodiments.
  • Embodiment 5
  • Fig. 19 shows permeability (µ) of the typical magnetic films fabricated through the manufacturing methods described in Embodiments 2 to 4, in the figure permeability is normalized with the value µ at frequency of 1 MHz. For the purpose of comparison, permeability (µ) of the 80Ni-Fe permalloy film is also measured. The thicknesses of all the film are 3 µm.
  • For the films of this embodiment having resistivity of 48 to 60 µΩ•cm, the frequency (f) where permeability (µ) decreases by 25 % (that is, 75 % of initial permeability) is up to the range of 40 MHz to 70 MHz. This range is 3 to 5 times as wide as 15 MHz for the permalloy. It can be understood that the frequency characteristics of the films of the present embodiment are improved.
  • Embodiment 6
  • Fig. 20 and Fig. 21 are cross-sectional views showing an inductive head having a two stage winding coil using the magnetic films according to the present invention for an upper and a lower magnetic films as the same as in Embodiment 1.
  • As shown in the figure, the thin film magnetic head 210 involves a lower portion and an upper portion magnetic film formed of two films 212 and 214 made of a magnetic material, for example, permalloy. The films 212 and 214 are deposited by two stages containing shaping films 221 and 213, respectively.
  • These films 212 and 214 are separated by insulating films 215, 216 and 217 except for a back portion region 218 where the films are physically contact and a top end region 219 where the films are separated by a thin film 220 of a non-magnetic material to form a magnetic gap 221.
  • There is provided a flat conductive coil 222 in the space between the films 212 and 214 of a magnetic material. The coil 222 has two inter-layer multi-windings 223a to 223n deposited in an elliptical pattern between the films 215, 216 and 217 of insulating material.
  • The top end portion of the transducer gap 221 is even with an air bearing surface (ABS) formed on a non-magnetic substrate attached with the above mentioned films.
  • The transducer gap 221 reacts with a rotating magnetic recording medium (not shown) such as a rotating magnetic disk in an air bearing relation. When the disk is rotated, the head flies on the air bearing surface (ABS) very near the recording surface of the disk.
  • The thin film magnetic head is fabricated by depositing a magnetic film 212 and a shaping film 211 on a substrate 224 using a proper mask in order to form a thin deposited film in the top den region 219 of a magnetic pole chip. Then a non-magnetic film 220 is formed on the films 211 an 212 except for the back gap region 218.
  • Then a first insulating film 215 is deposited onto the film 220 except for the magnetic gap 221. A continuous and flat conductive first film of elliptical swirl-shaped winding 223a to 223n is deposited on the insulating film 215 through, for example, electroplating.
  • An insulating film 216 is deposited on the first film of the coil, and a second film winding of the coil is deposited, on the coil an insulating film 217 is deposited. Then, as described above, the magnetic film 214 is deposited on the insulated coil except for the back portion gap region 218 which physically contacts the magnetic film 212.
  • The top end 219 of the magnetic pole chip has a per-selected nearly constant width W. The width W is equal to or slightly narrower than the width of a track on the corresponding rotatable magnetic medium.
  • The selected width W of the top end of the magnetic pole chip is obtained by cutting the top end of the magnetic pole chip, and the step to cut the top end of the magnetic pole chip is performed before the step to deposit the shaping film 213 for the second magnetic film 214. By changing the process in such a manner, the top end of the magnetic pole chip can be cut with a very higher accuracy than a conventional process.
  • After depositing the magnetic film 214 and before depositing the shaping film 213, the thin film head assembly is covered with a photo-resist mask 230. Then a window 232 is formed on the photo-resist mask in either of the sides of the top end region of the magnetic pole chip of the head.
  • The masked head is performed an ion milling process. During the process, the portion of head not covered by the mask is milled to be carved in a desired width as shown in Fig. 5.
  • The ion milling process affects on a surface to be worked the same effect as normal condition, and accordingly a structure not covered with a mask is also milled together with a photo-resist mask. Therefore, the milled material produced from the head is re-deposited onto the remaining portion of the mask and onto the head structure having been milled before.
  • In this reason, ion milling is performed in two stages. In the first step, the un-masked structure is milled up to the substrate 224 through the magnetic film 14, the non-magnetic gap film 220 and the magnetic film 212. In order to completely remove the material, it is preferable that the first step is performed until the substrate 224 is slightly milled.
  • The second step of the ion milling process is performed to remove all the re-deposited materials, and performed in a large angle inclining state in such a state as inclining 75 to 80 degree to the vertical direction. In a preferable embodiment of an ion milling step, a permalloy magnetic material is milled with an etching rate of about 55 nm (550 Å) per minute by electric power of about 2 watt per cubic centi-meter. Then the photo-resist is removed, a shaping magnetic film is deposited, and thus a thin film magnetic head is completed.
  • The photo-resist mask is milled during ion milling, and the thickness of the photo-resist on the head becomes thinner than the thickness of the photo-resist on the magnetic pole chip region depending on the shape of the magnetic film 214.
  • The thin film magnetic head fabricated according to the present invention is of a yoke structure having a transducer magnetic gap in one end and a back gap region in the other end, and the yoke structure having a conductive coil for energizing a magnetic yoke attached between the magnetic gap and the back gap region of the yoke structure is formed with two films made of a magnetic material.
  • A disk storage system constructed using the thin film magnetic head fabricated in the present embodiment will be described. The disk storage system according to the present embodiment comprises a magnetic disk having an outer diameter of approximately 8.90 mm (3.5 inches), a spindle for rotating the disk, a positioning mechanism for a magnetic head and a housing.
  • The magnetic head is an inductive head, and the track width is 5.0 µm. The upper and the lower magnetic films of the head are formed with (Ni 44 wt%-Fe)-2 wt%Mo alloy thin films having saturation magnetic flux density of 1.3 T, resistivity (ρ) of 60 µΩ•cm, relative permeability µ of 1000, a film thickness d of 3 µm, and the gap length is 0.4 µm.
  • An equivalent effect may be obtained using the following material for the magnetic pole, that is, a similar Ni-Fe series alloy having saturation magnetic flux density of 1.6 T, a Fe-Co-Ni/Al2O3/ Fe-Co-Ni multi-layer film, a thin film of Ni-Fe thin film containing ZrO2, Y2O3, HfO2, Al2O3 or SiO2 having grain size of 2 nm to 3 nm.
  • In the case of mixing oxide in the magnetic film, the grain size is preferably 0.5 nm to 5 nm. This is because when the oxide grain size is within the above range, only resistivity can be increased without degrading saturation magnetic flux density or the soft magnetic characteristic so much.
  • By mixing such an oxide described above in the Fe-Ni alloy thin film, resistivity can be increased up to approximately 60 µΩ•cm, and relative permeability shows as a good soft magnetic characteristic as nearly 1000.
  • On the other hand, in a case where the NiFe thin film without oxide is employed for a recording magnetic pole of a head, the high frequency characteristic can be improved by decreasing relative magnetic permeability up to 500 or less. However, it is necessary to set the recording magnetomotive force of a head to a value larger than 0.5 T.
  • A recording film of a magnetic disk is formed of CoCrTa (adding amount of Cr is 16 at%) having a magnetic coercive force in the recording bit direction of 167112 A/m (2100 Oe) and magnetic coercive force orientation ratio of 1.2. The product Br·δ of the residual magnetic flux density and the film thickness of the recording medium is 0.03 T·nm (300 gauss·µm).
  • By employing the recording medium, it is possible to improve the linear recording density characteristic and to substantially decreasing the medium noise in a high linear recording density range. When the medium magnetic coercive force is lower than 15915 A/m (200 Oe), the bit error rate is decreased to cause the apparatus disable.
  • The rotating speed of the spindle during recording and reproducing is set to 4491 rpm, and the floating amount of the head at the outermost periphery of the data recording region on the magnetic disk at that time is 0.05 µm.
  • The linear recording density on each track is set so as to becomes equal from the inner most periphery to the outermost periphery of the data recording region, and the recording frequency at the outermost periphery is set to 67.5 MHz.
  • In the disk storage system in this embodiment, the linear recording density of data on each of tracks is set to 144 kBPI (kilo Bit Per 25.4 mm (Inch)), the track density is set to 5 kTPI (kiro Track Per 25.4 mm (Inch)), and accordingly areal density is 720 mega-bit per 6.45 cm2 (square inch).
  • In the embodiment, four magnetic disks are used, the format capacity of the system is 2.8 giga-bytes, and the transfer rate is 15 mega-bytes per second.
  • Although in this embodiment the 8/9 conversion is used for data recording, a system having the same performance as this embodiment may be constructed even when the conventional 1-7 method is used for data recording. However, in that case, the recording frequency becomes 45 MHz.
  • The specification of the disk storage system constructed in this embodiment is shown in Table 3.
    Specification of a 89 mm (3.5 inch) Type Apparatus
    Memory Capacity 2.8 GB
    Number of Disks 4
    Number of Data Surfaces 8
    Number of Heads 8
    Number of Tracks/Disk Surface 4427
    Maximum Linear Recording Density 144 kBPI
    Track Density 5 kTPI
    Rotating Speed 4491 RPM
    Recording Frequency 67.5 MHz
    Transfer Rate (to/from Media) 15 MB/sec
  • Embodiment 7
  • Description will be made on the results obtained from a disk storage system combining a magnetic head according to the present invention with magnetic disks having disk a diameter of 63.5 mm (2.5 inches), 45.72 mm (1.8 inches) and 33.02 mm (1.3 inches).
  • The magnetic head and the magnetic disks used in this embodiment are the same as those used in Embodiment 6, linear recording density of data on each of tracks is set to 144 kBPI, and track density is set to 5 kTPI. The rotating speed of the spindle is set so that the transfer rate becomes 15 MB/sec for each of the disks.
  • Further, as described in Embodiment 6, a system having the same performance as this embodiment may be constructed even when the conventional 1-7 method is used for data recording. However, in that case, the recording frequency becomes 45 MHz.
    Specification of a 63.5 mm (2.5 inch) Type Apparatus
    Memory Capacity 1.8 GB
    Number of Disks 4
    Number of Data Surfaces 8
    Number of Heads 8
    Number of Tracks/Disk Surface 2951
    Maximum Linear Recording Density 144 kBPI
    Track Density 5 kTPI
    Rotating Speed 6736 RPM
    Recording Frequency 67.5 MHz
    Transfer Rate (to/from Media) 15 MB/sec
    Specification of a 45.72 mm (1.8) inch Type Apparatus
    Memory Capacity 1.4 GB
    Number of Disks 4
    Number of Data Surfaces 8
    Number of Heads 8
    Number of Tracks/Disk Surface 2213
    Maximum Linear Recording Density 144 kBPI
    Track Density 5 kTPI
    Rotating Speed 8982 RPM
    Recording Frequency 67.5 MHz
    Transfer Rate (to/from Media) 15 MB/sec
    Specification of a 33.02 mm (1.3 inch) Type Apparatus
    Memory Capacity 0.9 GB
    Number of Disks 4
    Number of Data Surfaces 8
    Number of Heads 8
    Number of Tracks/Disk Surface 1475
    Maximum Linear Recording Density 144 kBPI
    Track Density 5 kTPI
    Rotating Speed 13473 RPM
    Recording Frequency 67.5 MHz
    Transfer Rate (to/from Media) 15 MB/sec
  • Embodiment 8
  • Two kinds of inductive heads using magnetic poles having different resistivity ρ, film thickness d and relative permeability µ are fabricated, and frequency dependence of recording magnetic field intensity for each of the heads is measured using an electron beam tomography method.
  • The magnetic pole material, the magnetic pole thickness d, resistivity ρ and relative permeability µ in a low frequency band below 1 MHz for each of the prototype heads are shown in Table 7.
  • The head A comprises a magnetic pole formed of a Ni-Fe alloy single film having the composition described in Embodiment 1 and film thickness of 3 µm. The head B comprises a magnetic pole formed by laminating Fe-Co-Ni-Mo films of 2.2 µm film thickness through an Al2O3 intermediate film of 0.1 µm film thickness, as the same as in Embodiment 4. Thereby, the total thickness of the magmatic pole film of this head is 4.5 µm.
  • Here, in the multi-layer film of Fe-Co-Ni-Mo/Al2O3/Fe-Co-Ni-Mo, when the thickness of the single layer of the Fe-Co-Ni-Mo film exceeds 2.7 µm, the attenuation of magnetic field intensity at recording frequency of 45 MHz becomes above 10% to cause writ blurring or fluctuation in an over-write film, which is undesirable. In this embodiment the thickness of the Fe-Co-Ni-Mo film is set to 2.2 µm.
  • The head C comprises a lower magnetic film of a magnetic pole which is a Co-Ta-Zr amorphous single layer film having film thickness of 3 µm and resistivity of 90 µΩ•cm.
    Specification of Prototype Thin Film Magnetic Head
    Head Material of Magnetic Pole d (µ) ρ (µΩ•cm) µ
    A NiFe 3.0 16 1000
    B FeCoNiMo multi-layer film 2.2 16 1000
    C CoTaZr 3.0 90 1000
    Note
       d: thickness of magnetic pole
       ρ: resistivity
       µ: relative permeability
  • Head efficiencies η are calculated from the measured results of the normalized frequency dependence of recording magnetic field intensity. For the head A having the magnetic pole of Ni-Fe single layer film, the recording magnetic field intensity begins to decrease near a point exceeding 10 MHz and the intensity at 100 MHz is attenuated lower than 60 % of the intensity in the low frequency band.
  • On the other hand, although the head B uses the Fe-Co-Ni-Mn films having the magnetic permeability and resistivity equivalent to those of the NiFe film used in the head A, the eddy current loss is substantially decreased since the films are of a multi-layer structure through the Al2O3 insulating film.
  • In the case of this head, the attenuation of magnetic field intensity at 100 MHz is nearly 20 % and the frequency characteristic is improved. In the case of the head C, the attenuation of magnetic field intensity at 100 MHz is nearly 0 % and the frequency characteristic is outstanding.
  • Embodiment 9
  • In this embodiment, an upper and a lower magnetic films are formed by the following method.
  • There is fabricated an inductive head having an upper and a lower magnetic cores which are electroplated through a mask in a plating bath containing Ni++ of 16.7 g/l, Fe++ of 2.4 g/l, and a common stress-release agent and a surface-active agent under a condition of pH of 3.0, plating current density of 15 mA.
  • The track width is 4.0 µm, and gap length is 0.4 µm. The composition of this magnetic film is 42.4Ni-Fe (weight %), and as to the magnetic characteristics, saturation magnetic flux density (BS) is 1.64 T, magnetic coercive force in the hard axis direction (HCH) is 39.289 A/m (0.5 Oe), and resistivity (ρ) is 48.1 µΩ•cm.
  • Fig. 22 is a perspective view showing a dual element head, and Fig. 23 is a plan view of the write. The write head comprises an upper magnetic core 320, a lower magnetic core 321 also serves as an upper shield film, a coil 325. The read head comprises a magnetoresistive element 323, an electrode 324 for conducting sense current to the magnetoresistive element 323 and a lower shield film 322. The write and read heads are formed on a slider 326.
  • This inductive head is mounted on the disk storage system shown in Embodiment 1 to evaluate the recording performance. The medium used has an outer diameter of 3.5 inches and magnetic coercive force of 198943 A/m (2500 Oe).
  • The performance (over-write characteristic) of the recording head according to the present invention evaluated under such a construction shows an outstanding characteristic which is approximately -50 dB at a high frequency band above 40 MHz.
  • Embodiment 10
  • A disk storage system of this embodiment employs a dual element head, shown in Fig. 22, which uses an inductive head for recording and a magnetoresistive element for reproducing. The upper magnetic film of the recording magnetic pole of the inductive head is formed as described above.
  • And for the other of the upper shield film 81 also serving as a recording magnetic pole, a multi-layer film of Fe-Co-Ni/Al2O3/Fe-Co-Ni having a single layer thickness of Fe-Co-Ni film of 2.2 µm is used. The thickness of the Al2O3 intermediate film is set to 0.1 µm, and the track width of the recording pole is set to 3 µm.
  • A Ni-Fe alloy film having thickness of 1 µm is used for the lower shield film 82. A Ni-Fe alloy film having thickness of 15 nm is used for the magnetoresistive element 86 which is driven utilizing a soft film bias method.
  • Instead of the magnetoresistive element 86 using the Ni-Fe alloy film, it is also possible to use a spin valve type element composed of an Ni-Fe film, a Cu film, a Co film and an anti-ferromagnetic film of Ni-O series, Fe-Mn series or Cr-Mn series; an alloy type giant-magnetoresistive element of Co-Ag, Co-Au, NiFe-Ag, Co-Cu, Fe-Ag or the like; or a multi-layer type giant-magnetoresistive element of Co/Cr, Fe/Cr, Co/Cu or NiFe/Cu series.
  • The disk storage system constructed according to this embodiment can attain the same specification as shown in Table 2.

Claims (4)

  1. Thin film magnetic head including
    a lower magnetic core (84),
    an upper magnetic core (83) formed on said lower magnetic core (84),
    one end of said upper magnetic core (83) contacting one end of said lower magnetic core (84),
    the other end of said upper magnetic core facing the other end of said lower magnetic core (84) through a magnetic gap, whereby said upper magnetic core (83) forms a magnetic circuit including said magnetic gap together with said lower magnetic core (84),
    a conductive coil (87) having a given number of winding turns passing between both of said upper magnetic core (83) and said lower magnetic core (84),
    characterized in that
    at least one of said upper magnetic core (83) and said lower magnetic core (84) is an electroplated thin film made of an Ni-Fe alloy having Ni of 38 to 60 wt.% and Fe of 40 to 62 wt.%, and
    at least one of the magnetic cores (83, 84) contains a substance composed of at least one of Co less than 15 wt.% and at least one of Mo, Cr, Pd, B or In less than 3 wt.% in the total weight.
  2. Thin film magnetic head according to claim 1, wherein the thin film has a saturation magnetic flux density larger than 1.5 T, a magnetic coercive force in the hard axis direction smaller than 795.77 A/m, a resistivity larger than 40 µΩ·cm and a film thickness of 2 to 5 µm.
  3. Disk storage system comprising:
    a thin film magnetic disk (1) for recording information,
    a supporting device (3) as transfer means for making access to said thin film magnetic disk (1) and
    a thin film magnetic head according to claim 1 movably arranged on the supporting device (3).
  4. Disk storage system according to claim 3, characterized in that said thin film magnetic head (2) is a dual element thin film magnetic head.
EP96101287A 1995-02-03 1996-01-30 Disk storage system, thin film magnetic head therefor and fabricating method thereof Expired - Lifetime EP0725386B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP1666695 1995-02-03
JP16666/95 1995-02-03
JP7016666A JPH08212512A (en) 1995-02-03 1995-02-03 Magnetic storage device and thin-film magnetic head used for the same and its production

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EP0725386A2 EP0725386A2 (en) 1996-08-07
EP0725386A3 EP0725386A3 (en) 1998-03-25
EP0725386B1 true EP0725386B1 (en) 2003-12-17

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EP96101287A Expired - Lifetime EP0725386B1 (en) 1995-02-03 1996-01-30 Disk storage system, thin film magnetic head therefor and fabricating method thereof

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EP (1) EP0725386B1 (en)
JP (1) JPH08212512A (en)
CN (1) CN1068949C (en)
DE (1) DE69631077T2 (en)
SG (1) SG42333A1 (en)

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CN1140296A (en) 1997-01-15
US6490131B2 (en) 2002-12-03
US20020154444A1 (en) 2002-10-24
SG42333A1 (en) 1997-08-15
EP0725386A3 (en) 1998-03-25
DE69631077D1 (en) 2004-01-29
US6262867B1 (en) 2001-07-17
CN1068949C (en) 2001-07-25
US6661606B2 (en) 2003-12-09
US6385009B2 (en) 2002-05-07
EP0725386A2 (en) 1996-08-07
US20030123186A1 (en) 2003-07-03
JPH08212512A (en) 1996-08-20
DE69631077T2 (en) 2004-08-26
US20020008937A1 (en) 2002-01-24
US6118628A (en) 2000-09-12

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