EP0384483A3 - Air rectification process and apparatus - Google Patents

Air rectification process and apparatus Download PDF

Info

Publication number
EP0384483A3
EP0384483A3 EP19900103572 EP90103572A EP0384483A3 EP 0384483 A3 EP0384483 A3 EP 0384483A3 EP 19900103572 EP19900103572 EP 19900103572 EP 90103572 A EP90103572 A EP 90103572A EP 0384483 A3 EP0384483 A3 EP 0384483A3
Authority
EP
European Patent Office
Prior art keywords
rectification process
air rectification
air
rectification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP19900103572
Other languages
German (de)
Other versions
EP0384483A2 (en
EP0384483B1 (en
Inventor
Dietrich Dipl.-Ing. Rottmann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Linde GmbH
Original Assignee
Linde GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19893905521 external-priority patent/DE3905521A1/en
Application filed by Linde GmbH filed Critical Linde GmbH
Publication of EP0384483A2 publication Critical patent/EP0384483A2/en
Publication of EP0384483A3 publication Critical patent/EP0384483A3/en
Application granted granted Critical
Publication of EP0384483B1 publication Critical patent/EP0384483B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04854Safety aspects of operation
    • F25J3/0486Safety aspects of operation of vaporisers for oxygen enriched liquids, e.g. purging of liquids
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04193Division of the main heat exchange line in consecutive sections having different functions
    • F25J3/04206Division of the main heat exchange line in consecutive sections having different functions including a so-called "auxiliary vaporiser" for vaporising and producing a gaseous product
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/0423Subcooling of liquid process streams
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04309Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of nitrogen
    • F25J3/04315Lowest pressure or impure nitrogen, so-called waste nitrogen expansion
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04327Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of argon or argon enriched stream
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04333Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using quasi-closed loop internal vapor compression refrigeration cycles, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04351Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using quasi-closed loop internal vapor compression refrigeration cycles, e.g. of intermediate or oxygen enriched (waste-)streams of nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04654Producing crude argon in a crude argon column
    • F25J3/04666Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
    • F25J3/04672Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
    • F25J3/04678Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser cooled by oxygen enriched liquid from high pressure column bottoms
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04654Producing crude argon in a crude argon column
    • F25J3/04709Producing crude argon in a crude argon column as an auxiliary column system in at least a dual pressure main column system
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00Processes or apparatus using separation by rectification
    • F25J2200/20Processes or apparatus using separation by rectification in an elevated pressure multiple column system wherein the lowest pressure column is at a pressure well above the minimum pressure needed to overcome pressure drop to reject the products to atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2230/00Processes or apparatus involving steps for increasing the pressure of gaseous process streams
    • F25J2230/42Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2230/00Processes or apparatus involving steps for increasing the pressure of gaseous process streams
    • F25J2230/52Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being oxygen enriched compared to air, e.g. "crude oxygen"
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/58Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being argon or crude argon
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/02Recycle of a stream in general, e.g. a by-pass stream
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/42Processes or apparatus involving steps for recycling of process streams the recycled stream being nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/30External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
    • F25J2250/40One fluid being air
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/30External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
    • F25J2250/50One fluid being oxygen
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00Refrigeration
    • Y10S62/923Inert gas
    • Y10S62/924Argon

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Separation By Low-Temperature Treatments (AREA)
EP90103572A 1989-02-23 1990-02-23 Air rectification process and apparatus Expired - Lifetime EP0384483B1 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE3905521 1989-02-23
DE19893905521 DE3905521A1 (en) 1989-02-23 1989-02-23 METHOD AND DEVICE FOR AIR DISASSEMBLY BY RECTIFICATION
EP89113815 1989-07-26
EP19890113815 EP0383994A3 (en) 1989-02-23 1989-07-26 Air rectification process and apparatus

Publications (3)

Publication Number Publication Date
EP0384483A2 EP0384483A2 (en) 1990-08-29
EP0384483A3 true EP0384483A3 (en) 1990-11-07
EP0384483B1 EP0384483B1 (en) 1992-07-22

Family

ID=25878076

Family Applications (2)

Application Number Title Priority Date Filing Date
EP19890113815 Withdrawn EP0383994A3 (en) 1989-02-23 1989-07-26 Air rectification process and apparatus
EP90103572A Expired - Lifetime EP0384483B1 (en) 1989-02-23 1990-02-23 Air rectification process and apparatus

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP19890113815 Withdrawn EP0383994A3 (en) 1989-02-23 1989-07-26 Air rectification process and apparatus

Country Status (6)

Country Link
US (1) US5036672A (en)
EP (2) EP0383994A3 (en)
JP (1) JPH02245201A (en)
CN (1) CN1025068C (en)
AU (1) AU618659B2 (en)
DE (1) DE59000211D1 (en)

Families Citing this family (58)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3913880A1 (en) * 1989-04-27 1990-10-31 Linde Ag METHOD AND DEVICE FOR DEEP TEMPERATURE DISPOSAL OF AIR
FR2670278B1 (en) * 1990-12-06 1993-01-22 Air Liquide METHOD AND INSTALLATION FOR AIR DISTILLATION IN A VARIABLE REGIME FOR THE PRODUCTION OF GASEOUS OXYGEN.
DE4126945A1 (en) * 1991-08-14 1993-02-18 Linde Ag METHOD FOR AIR DISASSEMBLY BY RECTIFICATION
FR2681416B1 (en) * 1991-09-13 1993-11-19 Air Liquide METHOD FOR COOLING A GAS IN AN AIR GAS OPERATING INSTALLATION, AND INSTALLATION.
FR2685459B1 (en) * 1991-12-18 1994-02-11 Air Liquide PROCESS AND PLANT FOR PRODUCING IMPURATED OXYGEN.
US5197296A (en) * 1992-01-21 1993-03-30 Praxair Technology, Inc. Cryogenic rectification system for producing elevated pressure product
FR2689224B1 (en) 1992-03-24 1994-05-06 Lair Liquide PROCESS AND PLANT FOR THE PRODUCTION OF NITROGEN AT HIGH PRESSURE AND OXYGEN.
US5245832A (en) * 1992-04-20 1993-09-21 Praxair Technology, Inc. Triple column cryogenic rectification system
US5228297A (en) * 1992-04-22 1993-07-20 Praxair Technology, Inc. Cryogenic rectification system with dual heat pump
GB9208645D0 (en) * 1992-04-22 1992-06-10 Boc Group Plc Air separation
US5275004A (en) * 1992-07-21 1994-01-04 Air Products And Chemicals, Inc. Consolidated heat exchanger air separation process
FR2699992B1 (en) * 1992-12-30 1995-02-10 Air Liquide Process and installation for producing gaseous oxygen under pressure.
US5321953A (en) * 1993-05-10 1994-06-21 Praxair Technology, Inc. Cryogenic rectification system with prepurifier feed chiller
US5406786A (en) * 1993-07-16 1995-04-18 Air Products And Chemicals, Inc. Integrated air separation - gas turbine electrical generation process
US5410885A (en) * 1993-08-09 1995-05-02 Smolarek; James Cryogenic rectification system for lower pressure operation
US5463871A (en) * 1994-10-04 1995-11-07 Praxair Technology, Inc. Side column cryogenic rectification system for producing lower purity oxygen
US5461872A (en) * 1994-11-21 1995-10-31 The Boc Group, Inc. Air separation method and apparatus
DE19529681C2 (en) * 1995-08-11 1997-05-28 Linde Ag Method and device for air separation by low-temperature rectification
US5546767A (en) * 1995-09-29 1996-08-20 Praxair Technology, Inc. Cryogenic rectification system for producing dual purity oxygen
FR2739439B1 (en) * 1995-09-29 1997-11-14 Air Liquide METHOD AND PLANT FOR PRODUCTION OF A GAS UNDER PRESSURE BY CRYOGENIC DISTILLATION
US5799508A (en) * 1996-03-21 1998-09-01 Praxair Technology, Inc. Cryogenic air separation system with split kettle liquid
US5682762A (en) * 1996-10-01 1997-11-04 Air Products And Chemicals, Inc. Process to produce high pressure nitrogen using a high pressure column and one or more lower pressure columns
JP3527609B2 (en) * 1997-03-13 2004-05-17 株式会社神戸製鋼所 Air separation method and apparatus
AU7330298A (en) * 1997-05-21 1998-12-11 Kemin Huang An oxygen-rich air conditioner
US6009723A (en) * 1998-01-22 2000-01-04 Air Products And Chemicals, Inc. Elevated pressure air separation process with use of waste expansion for compression of a process stream
US5878597A (en) * 1998-04-14 1999-03-09 Praxair Technology, Inc. Cryogenic rectification system with serial liquid air feed
US5901578A (en) * 1998-05-18 1999-05-11 Praxair Technology, Inc. Cryogenic rectification system with integral product boiler
US6666048B1 (en) * 1999-04-05 2003-12-23 L'air Liquide - Societe Anonyme A Directoire Et Conseil De Surveillance Pour L'etude Et L'exploitation Des Procedes Georges Claude Variable capacity fluid mixture separation apparatus and process
WO2003006890A1 (en) * 2001-07-13 2003-01-23 Ebara Corporation Dehumidifying air-conditioning apparatus
CN100436989C (en) * 2004-01-29 2008-11-26 宝山钢铁股份有限公司 Method for preparing high purity oxygen using full low pressure air separation plant
JP4460975B2 (en) * 2004-08-20 2010-05-12 三菱重工業株式会社 Seawater treatment method and seawater treatment apparatus
US7421856B2 (en) * 2005-06-17 2008-09-09 Praxair Technology, Inc. Cryogenic air separation with once-through main condenser
CN101548145B (en) * 2006-11-07 2013-07-10 蒂艾克思股份有限公司 Dehumidification
DE102007031759A1 (en) 2007-07-07 2009-01-08 Linde Ag Method and apparatus for producing gaseous pressure product by cryogenic separation of air
DE102007031765A1 (en) 2007-07-07 2009-01-08 Linde Ag Process for the cryogenic separation of air
DE102009034979A1 (en) 2009-04-28 2010-11-04 Linde Aktiengesellschaft Method for producing pressurized oxygen by evaporating liquid oxygen using a copper and nickel heat exchanger block
EP2312248A1 (en) 2009-10-07 2011-04-20 Linde Aktiengesellschaft Method and device for obtaining pressurised oxygen and krypton/xenon
CN101886871B (en) * 2010-08-04 2012-08-08 四川空分设备(集团)有限责任公司 Method and device for producing pressure oxygen by air separation
DE102010052545A1 (en) 2010-11-25 2012-05-31 Linde Aktiengesellschaft Method and apparatus for recovering a gaseous product by cryogenic separation of air
DE102010052544A1 (en) 2010-11-25 2012-05-31 Linde Ag Process for obtaining a gaseous product by cryogenic separation of air
EP2520886A1 (en) 2011-05-05 2012-11-07 Linde AG Method and device for creating gaseous oxygen pressurised product by the cryogenic decomposition of air
EP2551619A1 (en) * 2011-07-26 2013-01-30 Linde Aktiengesellschaft Method and device for extracting pressurised oxygen and pressurised nitrogen by cryogenic decomposition of air
DE102011112909A1 (en) 2011-09-08 2013-03-14 Linde Aktiengesellschaft Process and apparatus for recovering steel
EP2600090B1 (en) 2011-12-01 2014-07-16 Linde Aktiengesellschaft Method and device for generating pressurised oxygen by cryogenic decomposition of air
US20130139547A1 (en) * 2011-12-05 2013-06-06 Henry Edward Howard Air separation method and apparatus
DE102011121314A1 (en) 2011-12-16 2013-06-20 Linde Aktiengesellschaft Method for producing gaseous oxygen product in main heat exchanger system in distillation column system, involves providing turbines, where one of turbines drives compressor, and other turbine drives generator
DE102012017488A1 (en) 2012-09-04 2014-03-06 Linde Aktiengesellschaft Method for building air separation plant, involves selecting air separation modules on basis of product specification of module set with different air pressure requirements
WO2014154339A2 (en) 2013-03-26 2014-10-02 Linde Aktiengesellschaft Method for air separation and air separation plant
EP2784420A1 (en) 2013-03-26 2014-10-01 Linde Aktiengesellschaft Method for air separation and air separation plant
EP2801777A1 (en) 2013-05-08 2014-11-12 Linde Aktiengesellschaft Air separation plant with main compressor drive
DE102013017590A1 (en) 2013-10-22 2014-01-02 Linde Aktiengesellschaft Method for recovering methane-poor fluids in liquid air separation system to manufacture air product, involves vaporizing oxygen, krypton and xenon containing sump liquid in low pressure column by using multi-storey bath vaporizer
EP2963367A1 (en) 2014-07-05 2016-01-06 Linde Aktiengesellschaft Method and device for cryogenic air separation with variable power consumption
EP2963369B1 (en) 2014-07-05 2018-05-02 Linde Aktiengesellschaft Method and device for the cryogenic decomposition of air
EP2963370B1 (en) 2014-07-05 2018-06-13 Linde Aktiengesellschaft Method and device for the cryogenic decomposition of air
TR201808162T4 (en) 2014-07-05 2018-07-23 Linde Ag Method and apparatus for recovering a pressurized gas product by decomposing air at low temperature.
CN104833174B (en) * 2015-05-26 2017-08-11 杭州杭氧股份有限公司 A kind of auxiliary oxygen column low energy consumption with pressure produces the device and method of low purity oxygen with pressure and high pure oxygen product
CN105066587A (en) * 2015-09-16 2015-11-18 开封空分集团有限公司 Cryogenic separation and low-purity oxygen and high-purity oxygen and nitrogen production device and method
EP3179186A1 (en) * 2015-12-07 2017-06-14 Linde Aktiengesellschaft Method for obtaining a liquid and a gaseous oxygen-rich air product in an air breakdown apparatus and air breakdown apparatus

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2666303A (en) * 1950-06-08 1954-01-19 British Oxygen Co Ltd Apparatus for the separation of gas mixtures by liquefaction and rectification
DE2548222B1 (en) * 1975-10-28 1977-01-27 Linde Ag Method and device for air separation
EP0316768A2 (en) * 1987-11-13 1989-05-24 Linde Aktiengesellschaft Air separation process by low temperature rectification

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3375673A (en) * 1966-06-22 1968-04-02 Hydrocarbon Research Inc Air separation process employing work expansion of high and low pressure nitrogen
FR2060184B1 (en) * 1969-09-10 1973-11-16 Air Liquide
DE2544340A1 (en) * 1975-10-03 1977-04-14 Linde Ag PROCEDURE FOR AIR SEPARATION
DE2557453C2 (en) * 1975-12-19 1982-08-12 Linde Ag, 6200 Wiesbaden Process for the production of gaseous oxygen
US4382366A (en) * 1981-12-07 1983-05-10 Air Products And Chemicals, Inc. Air separation process with single distillation column for combined gas turbine system
DE3531307A1 (en) * 1985-09-02 1987-03-05 Linde Ag METHOD FOR SEPARATING C (ARROW DOWN) 2 (ARROW DOWN) (ARROW DOWN) + (ARROW DOWN) HYDROCARBONS FROM NATURAL GAS
GB2192407B (en) * 1986-07-07 1990-12-19 Metal Box Plc Electro-coating apparatus and method
US4842625A (en) * 1988-04-29 1989-06-27 Air Products And Chemicals, Inc. Control method to maximize argon recovery from cryogenic air separation units

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2666303A (en) * 1950-06-08 1954-01-19 British Oxygen Co Ltd Apparatus for the separation of gas mixtures by liquefaction and rectification
DE2548222B1 (en) * 1975-10-28 1977-01-27 Linde Ag Method and device for air separation
EP0316768A2 (en) * 1987-11-13 1989-05-24 Linde Aktiengesellschaft Air separation process by low temperature rectification

Also Published As

Publication number Publication date
US5036672A (en) 1991-08-06
EP0384483A2 (en) 1990-08-29
CN1045173A (en) 1990-09-05
AU618659B2 (en) 1992-01-02
JPH02245201A (en) 1990-10-01
EP0384483B1 (en) 1992-07-22
AU4996090A (en) 1990-08-30
EP0383994A2 (en) 1990-08-29
DE59000211D1 (en) 1992-08-27
CN1025068C (en) 1994-06-15
EP0383994A3 (en) 1990-11-07

Similar Documents

Publication Publication Date Title
EP0384483A3 (en) Air rectification process and apparatus
EP0384213A3 (en) Air rectification process and apparatus
GB2219385B (en) Air separation process and apparatus
EP0338117A3 (en) Improved riveting process and apparatus
EP0244217A3 (en) Process and apparatus
HK59296A (en) Air conditioning apparatus
EP0421459A3 (en) Air conditioning apparatus
EP0454873A4 (en) Drying method and apparatus therefor
ZA894417B (en) Air conditioning process and apparatus therefor
ZA9019B (en) Apparatus and method for separating air
DE3662855D1 (en) Air distribution apparatus and method
EP0427486A3 (en) Air conditioner apparatus
ZA894419B (en) Air conditioning process and apparatus
ZA907188B (en) Cryogenic air separation process and apparatus
GB2255164B (en) Cooling process and apparatus
GB8912240D0 (en) Apparatus and method
GB9003803D0 (en) Sorting apparatus and apparatus
GB9025071D0 (en) Method and apparatus
GB2195758B (en) Air distribution apparatus
HUT45929A (en) Pneumatic classing method and apparatus
GB8925011D0 (en) Air cleaning and humidifying apparatus
GB2230099B (en) Sorting apparatus and method
GB2230698B (en) Explosive-screening apparatus and method
GB2227692B (en) Sorting method and apparatus
GB8912274D0 (en) Method and apparatus

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

AK Designated contracting states

Kind code of ref document: A2

Designated state(s): BE DE FR GB IT NL SE

PUAL Search report despatched

Free format text: ORIGINAL CODE: 0009013

AK Designated contracting states

Kind code of ref document: A3

Designated state(s): BE DE FR GB IT NL SE

17P Request for examination filed

Effective date: 19901010

17Q First examination report despatched

Effective date: 19910411

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): BE DE FR GB IT NL SE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT;WARNING: LAPSES OF ITALIAN PATENTS WITH EFFECTIVE DATE BEFORE 2007 MAY HAVE OCCURRED AT ANY TIME BEFORE 2007. THE CORRECT EFFECTIVE DATE MAY BE DIFFERENT FROM THE ONE RECORDED.

Effective date: 19920722

REF Corresponds to:

Ref document number: 59000211

Country of ref document: DE

Date of ref document: 19920827

ET Fr: translation filed
GBT Gb: translation of ep patent filed (gb section 77(6)(a)/1977)
PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed
PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 19940210

Year of fee payment: 5

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: GB

Payment date: 19940215

Year of fee payment: 5

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: BE

Payment date: 19940408

Year of fee payment: 5

EAL Se: european patent in force in sweden

Ref document number: 90103572.5

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Effective date: 19950223

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BE

Effective date: 19950228

BERE Be: lapsed

Owner name: LINDE A.G.

Effective date: 19950228

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 19950223

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Effective date: 19951031

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 19970226

Year of fee payment: 8

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: SE

Payment date: 19980218

Year of fee payment: 9

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: NL

Payment date: 19980226

Year of fee payment: 9

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 19981103

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 19990224

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NL

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 19990901

EUG Se: european patent has lapsed

Ref document number: 90103572.5