EP0053913A1 - Procédé pour la fabrication de tôles d'acier à phase double, à résistancee élevée et apte à l'emboutissage - Google Patents

Procédé pour la fabrication de tôles d'acier à phase double, à résistancee élevée et apte à l'emboutissage Download PDF

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Publication number
EP0053913A1
EP0053913A1 EP81305697A EP81305697A EP0053913A1 EP 0053913 A1 EP0053913 A1 EP 0053913A1 EP 81305697 A EP81305697 A EP 81305697A EP 81305697 A EP81305697 A EP 81305697A EP 0053913 A1 EP0053913 A1 EP 0053913A1
Authority
EP
European Patent Office
Prior art keywords
sheet
austenite
sufficient
steel
produce
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP81305697A
Other languages
German (de)
English (en)
Inventor
Hsun Hu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
USS Engineers and Consultants Inc
Original Assignee
USS Engineers and Consultants Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by USS Engineers and Consultants Inc filed Critical USS Engineers and Consultants Inc
Publication of EP0053913A1 publication Critical patent/EP0053913A1/fr
Withdrawn legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/04Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing
    • C21D8/0447Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing characterised by the heat treatment
    • C21D8/0473Final recrystallisation annealing
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/46Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals
    • C21D9/48Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals deep-drawing sheets
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • C21D1/185Hardening; Quenching with or without subsequent tempering from an intercritical temperature
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/002Bainite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/005Ferrite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/008Martensite

Definitions

  • This invention is directed to a method for the production of dual-phase steel sheet or strip products with improved deep drawability.
  • undesirable grain growth e.g. U. S. Patents 3,914,135 or 4,033,789
  • the formability of dual-phase steels, coupled with their relatively high-strength to weight ratios, have led to the adoption of such steels for the production of automotive parts such as bumpers, wheel racks, brackets--primarily as hot-rolled products.
  • cold-rolled, dual-phase steels have not been employed for the production of automobile body panels, one reason being that steel sheets for body panel applications must have good deep-drawing capabilities.
  • r m value is the ratio of true width strain to true thickness strain when the sheet is strained in tension.
  • r m value is the ratio of true width strain to true thickness strain when the sheet is strained in tension.
  • r m value is the ratio of true width strain to true thickness strain when the sheet is strained in tension.
  • the r values of dual-phase steel sheets are invariably poor, i.e. around unity (see, for example, Hayami et al., Formable HSLA and Dual-Phase Steels, Conference Proceedings, TMS-AIME, 1979, pages 167 to 180).
  • deep-drawing steels having r values of the order of 1.6 to 2.0 and yield strengths of the order of 40 ksi the presently available, dual-phase steels are much inferior.
  • crystallographic texture must be strongly (111) with very little (100) and other undesirable orientations.
  • strong (111) textures can be produced successfully in various low-carbon sheet steels, development of an equally strong (111) texture in the ferrite + martensite aggregate would be much more difficult to accomplish. This is because it is difficult to achieve a sharp texture in martensite due to the nature of the transformation variance. It has now been found that if proper orientations [e.g.
  • the predominant (111) texture] are first developed or provided to the steel, and if the steel is thereafter briefly intercritically annealed so that local regions with a high carbon content could become austenite pools at the intercritical temperature, these austenized regions will, upon rapid cooling, transform to martensite or bainite without unduly affecting the ferrite matrix - if the amount of martensite formed is small.
  • Patent 3,827,924 the disclosures of which patents are hereby incorporated by reference. Examples of three such steels were treated in the laboratory to provide an illustration of the properties which could be achieved. The chemical composition of these illustrative steels is provided in Table I below.
  • samples were given a simulated box-annealing treatment at 780°C for a period of four hours. Although the use of such a shortened soak period will result in some sacrifice of deep-drawing texture, it was deemed to be preferential, in order to reduce grain size and thereby attain a more uniform distribution of martensite during the subsequent transformation. After this four-hour hold at temperature, the specimens were cooled by removing them from the hot zone to the colder zone of the furnace. This simulated an accelerated cooling rate attainable in box-annealing and was intended further to reduce the size of the carbides or pearlite colonies at the grain boundaries.
  • the change in initial strain hardening rate, resulting from the intercritical heat treatment can be noted by the increase in flow stress after 4% elongation (column labeled "o0.04"). With the presence of yield point elongation of about 1 to 2%, the increase in flow strength at 4% elongation ranged from 10 to 14 ksi. When the yield point elongation was completely eliminated, the corresponding increase in flow stress ranged from 17 to 20 ksi.
  • both ductility and initial strain-hardening rate could be improved by changing the steel composition to increase the hardenability, for example, by utilizing elements such as nickel, which would have little or no effect on the annealing texture or the rm value.
  • Such increased hardenability would enable the employment of less severe cooling rates from the intercritical anneal, thereby minimizing supersaturation and quenched aging of the ferrite matrix.
  • box annealing has most widely been employed for the development of good deep-drawing properties in low carbon sheet steels; annealing with relatively rapid heating rates, such as in continuous annealing, can produce equally satisfactory results if (i) the prior hot processing conditions (such as the finishing and coiling temperature which influence the carbide size and the distribution in the hot rolled band), and (ii) the amount of subsequent cold rolling i reduction are appropriately adjusted.
  • the prior hot processing conditions such as the finishing and coiling temperature which influence the carbide size and the distribution in the hot rolled band
  • the amount of subsequent cold rolling i reduction are appropriately adjusted.
  • annealing to produce a high r m value and the subsequent intercritical heat treatment for the production of from about 2 to 10% austenite can be accomplished in one continuous anneal -- eliminating the separate intercritical heat treatment utilized in the aforementioned examples.
  • the steel sheet will be annealed to provide a crystallographic texture capable of yielding an r m value greater than 1.5 and preferably greater than 1.7.
  • the next heating phase whether performed as part of the initial anneal for texture formation o: as a discrete step, will be conducted for a time and temperature (preferably within the range A 1 to A 3 ) sufficient to produce from about 2 to 10% austenite, preferably less than 7% austenite.
  • the sheet will be cooled at a rate sufficient to transform all or a major portion of the austenite to martensite or bainite--the most preferred range of such decomposition products being about 3 to 5%.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatment Of Sheet Steel (AREA)
EP81305697A 1980-12-04 1981-12-03 Procédé pour la fabrication de tôles d'acier à phase double, à résistancee élevée et apte à l'emboutissage Withdrawn EP0053913A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US21278680A 1980-12-04 1980-12-04
US212786 1988-06-29

Publications (1)

Publication Number Publication Date
EP0053913A1 true EP0053913A1 (fr) 1982-06-16

Family

ID=22792420

Family Applications (1)

Application Number Title Priority Date Filing Date
EP81305697A Withdrawn EP0053913A1 (fr) 1980-12-04 1981-12-03 Procédé pour la fabrication de tôles d'acier à phase double, à résistancee élevée et apte à l'emboutissage

Country Status (5)

Country Link
EP (1) EP0053913A1 (fr)
JP (1) JPS57140828A (fr)
BR (1) BR8107848A (fr)
CA (1) CA1182387A (fr)
ES (1) ES507684A0 (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0196470A1 (fr) * 1985-03-08 1986-10-08 Hoogovens Groep B.V. Procédé de fabrication de bandes d'acier à structure double phase et bandes d'acier obtenues
GB2226571A (en) * 1988-12-22 1990-07-04 Sumitomo Metal Ind Magnetic stool plate for use as a magnetic shielding member and a method for the manufacture thereof
EP1378577A1 (fr) * 2002-07-02 2004-01-07 Centre de Recherches Metallurgiques A.S.B.L. Procédé pour le traitement thermique d'une bande d'acier laminée à froid, apte au formage, et bande d'acier ainsi obtenue
DE102004044021B3 (de) * 2004-09-09 2006-03-16 Salzgitter Flachstahl Gmbh Voll beruhigter, unlegierter oder niedriglegierter Stranggussstahl und Verfahren zu seiner Herstellung
CZ305697B6 (cs) * 2014-06-30 2016-02-10 Západočeská Univerzita V Plzni Způsob výroby ocelových dílů z plechu tažených zatepla

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1904162A1 (de) * 1968-01-30 1969-08-28 United States Steel Corp Verfahren zur Behandlung von Stahl
FR2176130A1 (fr) * 1972-03-15 1973-10-26 Nippon Kokan Kk
US3827924A (en) * 1971-05-21 1974-08-06 Nippon Steel Corp High-strength rolled steel sheets
FR2236945A1 (fr) * 1973-07-12 1975-02-07 Nippon Kokan Kk
FR2286205A1 (fr) * 1974-09-30 1976-04-23 Uss Eng & Consult Procede pour ameliorer l'aptitude a l'emboutissage de feuillards d'acier a basse teneur en manganese
US4033789A (en) * 1976-03-19 1977-07-05 Jones & Laughlin Steel Corporation Method of producing a high strength steel having uniform elongation
WO1979000644A1 (fr) * 1978-02-21 1979-09-06 Inland Steel Co Acier a haute resistance et son procede de fabrication
GB2028690A (en) * 1978-08-22 1980-03-12 Kawasaki Steel Co Steel sheets

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1904162A1 (de) * 1968-01-30 1969-08-28 United States Steel Corp Verfahren zur Behandlung von Stahl
US3502514A (en) * 1968-01-30 1970-03-24 United States Steel Corp Method of processing steel
US3827924A (en) * 1971-05-21 1974-08-06 Nippon Steel Corp High-strength rolled steel sheets
FR2176130A1 (fr) * 1972-03-15 1973-10-26 Nippon Kokan Kk
US3914135A (en) * 1972-03-15 1975-10-21 Nippon Kokan Kk Method of improving steel properties by using controlled cooling rates
FR2236945A1 (fr) * 1973-07-12 1975-02-07 Nippon Kokan Kk
US3904446A (en) * 1973-07-12 1975-09-09 Nippon Kokan Kk Process of making high strength cold rolled steel having excellent bake-hardening properties
FR2286205A1 (fr) * 1974-09-30 1976-04-23 Uss Eng & Consult Procede pour ameliorer l'aptitude a l'emboutissage de feuillards d'acier a basse teneur en manganese
US3954516A (en) * 1974-09-30 1976-05-04 United States Steel Corporation Method for enhancing the drawability of low manganese steel strip
US4033789A (en) * 1976-03-19 1977-07-05 Jones & Laughlin Steel Corporation Method of producing a high strength steel having uniform elongation
WO1979000644A1 (fr) * 1978-02-21 1979-09-06 Inland Steel Co Acier a haute resistance et son procede de fabrication
GB2028690A (en) * 1978-08-22 1980-03-12 Kawasaki Steel Co Steel sheets

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0196470A1 (fr) * 1985-03-08 1986-10-08 Hoogovens Groep B.V. Procédé de fabrication de bandes d'acier à structure double phase et bandes d'acier obtenues
US4698103A (en) * 1985-03-08 1987-10-06 Hoogovens Groep B.V. Method of manufacturing dual phase strip steel and steel strip manufactured by the method
GB2226571A (en) * 1988-12-22 1990-07-04 Sumitomo Metal Ind Magnetic stool plate for use as a magnetic shielding member and a method for the manufacture thereof
US5019191A (en) * 1988-12-22 1991-05-28 Sumitomo Metal Industries, Ltd. Magnetic steel plate for use as a magnetic shielding member and a method for the manufacture thereof
GB2226571B (en) * 1988-12-22 1993-06-23 Sumitomo Metal Ind Magnetic steel plate for use as a magnetic shielding member and a method for the manufacture thereof
EP1378577A1 (fr) * 2002-07-02 2004-01-07 Centre de Recherches Metallurgiques A.S.B.L. Procédé pour le traitement thermique d'une bande d'acier laminée à froid, apte au formage, et bande d'acier ainsi obtenue
BE1015018A3 (fr) * 2002-07-02 2004-08-03 Ct Rech Metallurgiques Asbl Procede pour le traitement thermique d'une bande d'acier laminee a froid, procede de fabrication d'une bande d'acier adaptee au fromage et bande d'acier ainsi obtenue.
DE102004044021B3 (de) * 2004-09-09 2006-03-16 Salzgitter Flachstahl Gmbh Voll beruhigter, unlegierter oder niedriglegierter Stranggussstahl und Verfahren zu seiner Herstellung
CZ305697B6 (cs) * 2014-06-30 2016-02-10 Západočeská Univerzita V Plzni Způsob výroby ocelových dílů z plechu tažených zatepla

Also Published As

Publication number Publication date
JPS57140828A (en) 1982-08-31
ES8207226A1 (es) 1982-09-01
CA1182387A (fr) 1985-02-12
BR8107848A (pt) 1982-09-08
ES507684A0 (es) 1982-09-01

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PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

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Inventor name: HU, HSUN