DK3380453T3 - Syntese af beta-mercaptoethanol - Google Patents

Syntese af beta-mercaptoethanol Download PDF

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Publication number
DK3380453T3
DK3380453T3 DK16813183.7T DK16813183T DK3380453T3 DK 3380453 T3 DK3380453 T3 DK 3380453T3 DK 16813183 T DK16813183 T DK 16813183T DK 3380453 T3 DK3380453 T3 DK 3380453T3
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DK
Denmark
Prior art keywords
mercaptoethanol
beta
synthesis
Prior art date
Application number
DK16813183.7T
Other languages
English (en)
Inventor
Daniel Hasenberg
Alex Pauwels
Original Assignee
Chevron Phillips Chemical Co Lp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chevron Phillips Chemical Co Lp filed Critical Chevron Phillips Chemical Co Lp
Application granted granted Critical
Publication of DK3380453T3 publication Critical patent/DK3380453T3/da

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/04Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by addition of hydrogen sulfide or its salts to unsaturated compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/001Controlling catalytic processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0292Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds with stationary packing material in the bed, e.g. bricks, wire rings, baffles
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/08Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by replacement of hydroxy groups or etherified or esterified hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/10Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C323/11Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/12Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00513Controlling the temperature using inert heat absorbing solids in the bed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00548Flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023Details
    • B01J2208/024Particulate material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023Details
    • B01J2208/024Particulate material
    • B01J2208/025Two or more types of catalyst
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D303/00Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02Compounds containing oxirane rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DK16813183.7T 2015-12-04 2016-11-30 Syntese af beta-mercaptoethanol DK3380453T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/959,328 US9718767B2 (en) 2015-12-04 2015-12-04 Beta-mercaptoethanol synthesis
PCT/US2016/064133 WO2017095873A1 (en) 2015-12-04 2016-11-30 Beta-mercaptoethanol synthesis

Publications (1)

Publication Number Publication Date
DK3380453T3 true DK3380453T3 (da) 2021-03-29

Family

ID=57570447

Family Applications (1)

Application Number Title Priority Date Filing Date
DK16813183.7T DK3380453T3 (da) 2015-12-04 2016-11-30 Syntese af beta-mercaptoethanol

Country Status (7)

Country Link
US (2) US9718767B2 (da)
EP (2) EP3597635A1 (da)
KR (2) KR102414346B1 (da)
DK (1) DK3380453T3 (da)
MY (1) MY170005A (da)
SG (2) SG11201804617WA (da)
WO (1) WO2017095873A1 (da)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9718767B2 (en) 2015-12-04 2017-08-01 Chevron Phillips Chemical Company Lp Beta-mercaptoethanol synthesis
CN109323240A (zh) * 2018-10-11 2019-02-12 长治市霍家工业有限公司 一种合成转化器内热水蒸汽回收利用装置
US10689333B1 (en) 2019-02-22 2020-06-23 Chevron Phillips Chemical Company Lp 2-mercaptoethanol synthesis

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB585655A (en) 1945-08-10 1947-02-14 Foster Neville Woodward Improvements in or relating to the production of monothioethylene glycol
US2776997A (en) * 1953-01-30 1957-01-08 Union Oil Co Preparation of hydroxy thio-ethers
US3086997A (en) 1961-11-07 1963-04-23 Phillips Petroleum Co Synthesis of 2-mercaptoethanol
FR1359678A (fr) 1963-01-14 1964-04-30 Aquitaine Petrole Préparation des hydroxythiols
US3366693A (en) 1964-09-16 1968-01-30 Gen Aniline & Film Corp Preparation of mercaptans and sulfides
US3394192A (en) 1966-03-16 1968-07-23 Du Pont Preparation of beta-mercaptoalkanols
US3462496A (en) 1967-01-10 1969-08-19 Dow Chemical Co Method of making mercapto alcohols
US3662004A (en) 1968-04-23 1972-05-09 Henkel & Cie Gmbh Process for producing hydroxyalkyl mercaptans
US3574768A (en) 1968-10-28 1971-04-13 Phillips Petroleum Co Synthesis of beta-mercaptoethanol
DE1914379A1 (da) 1969-03-21 1970-10-01
US3710439A (en) 1970-03-20 1973-01-16 Basf Ag Production of 2-mercaptoethanol
ZA713521B (en) 1970-06-11 1972-01-26 Uniroyal Ltd Preparation of mercaptoethanol
DE2529646A1 (de) 1975-07-03 1977-01-27 Erdoelchemie Gmbh Verfahren zur herstellung von thioglykolen
DE3014165C2 (de) 1980-04-12 1984-07-05 Degussa Ag, 6000 Frankfurt Verfahren zur Herstellung von 3-Mercapto-propandiol-(1,2)
JPS56147764A (en) * 1980-04-15 1981-11-16 Toyo Kasei Kogyo Kk Preparation of thioalkylene glycol
US4281202A (en) 1980-04-29 1981-07-28 Pennwalt Corporation Preparation of mercapto-alcohols
FR2483917A1 (fr) 1980-06-06 1981-12-11 Elf Aquitaine Production de mercapto-2 ethanol-1
JPS6058932A (ja) 1983-09-12 1985-04-05 Mitsubishi Gas Chem Co Inc メチル−ヒ−ブチルエ−テルの製造方法
US4564710A (en) 1984-11-08 1986-01-14 Phillips Petroleum Company Process for making mercapto alcohols
FR2609027B1 (fr) 1986-12-30 1989-08-11 Elf Aquitaine Procede de preparation de mercaptoalcools
JP2006184251A (ja) 2004-12-28 2006-07-13 Tdk Corp ガスセンサ
US7399893B2 (en) * 2005-12-13 2008-07-15 Chevron Phillips Chemical Company Lp Process and catalyst for synthesis of mercaptans and sulfides from alcohols
JP2008013453A (ja) 2006-07-04 2008-01-24 Sumitomo Chemical Co Ltd 2−メルカプトエタノールの製造方法
EP1923384B1 (de) 2006-11-09 2013-06-26 Basf Se Verfahren zur Herstellung von 2-Mercaptoethanol
US7645906B2 (en) * 2007-03-27 2010-01-12 Chevron Phillips Chemical Company Lp Graded catalyst bed for methyl mercaptan synthesis
CN101941928B (zh) 2010-08-12 2012-11-21 黑龙江省科学院大庆分院 一种巯基烷基醇合成方法
RU2556859C1 (ru) 2014-08-05 2015-07-20 Публичное Акционерное общество "Нижнекамскнефтехим"(ПАО "Нижнекамскнефтехим") Способ получения изопрена каталитическим дегидрированием изоамиленов в адиабатическом реакторе
US9718767B2 (en) 2015-12-04 2017-08-01 Chevron Phillips Chemical Company Lp Beta-mercaptoethanol synthesis

Also Published As

Publication number Publication date
US10544094B2 (en) 2020-01-28
KR20180088823A (ko) 2018-08-07
SG10202007468VA (en) 2020-09-29
KR102378698B1 (ko) 2022-03-24
KR102414346B1 (ko) 2022-06-28
US9718767B2 (en) 2017-08-01
EP3380453A1 (en) 2018-10-03
SG11201804617WA (en) 2018-06-28
KR20220038547A (ko) 2022-03-28
EP3597635A1 (en) 2020-01-22
EP3380453B1 (en) 2020-12-30
WO2017095873A1 (en) 2017-06-08
US20170291873A1 (en) 2017-10-12
US20170158630A1 (en) 2017-06-08
MY170005A (en) 2019-06-20

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