SG10202007468VA - Beta-mercaptoethanol synthesis - Google Patents

Beta-mercaptoethanol synthesis

Info

Publication number
SG10202007468VA
SG10202007468VA SG10202007468VA SG10202007468VA SG10202007468VA SG 10202007468V A SG10202007468V A SG 10202007468VA SG 10202007468V A SG10202007468V A SG 10202007468VA SG 10202007468V A SG10202007468V A SG 10202007468VA SG 10202007468V A SG10202007468V A SG 10202007468VA
Authority
SG
Singapore
Prior art keywords
mercaptoethanol
beta
synthesis
mercaptoethanol synthesis
Prior art date
Application number
SG10202007468VA
Inventor
Daniel Hasenberg
Alex Pauwels
Original Assignee
Chevron Phillips Chemical Co Lp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chevron Phillips Chemical Co Lp filed Critical Chevron Phillips Chemical Co Lp
Publication of SG10202007468VA publication Critical patent/SG10202007468VA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/04Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by addition of hydrogen sulfide or its salts to unsaturated compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/001Controlling catalytic processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0292Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds with stationary packing material in the bed, e.g. bricks, wire rings, baffles
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/02Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
    • C07C319/08Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by replacement of hydroxy groups or etherified or esterified hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/10Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C323/11Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/12Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00513Controlling the temperature using inert heat absorbing solids in the bed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00548Flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023Details
    • B01J2208/024Particulate material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023Details
    • B01J2208/024Particulate material
    • B01J2208/025Two or more types of catalyst
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D303/00Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02Compounds containing oxirane rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
SG10202007468VA 2015-12-04 2016-11-30 Beta-mercaptoethanol synthesis SG10202007468VA (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US14/959,328 US9718767B2 (en) 2015-12-04 2015-12-04 Beta-mercaptoethanol synthesis

Publications (1)

Publication Number Publication Date
SG10202007468VA true SG10202007468VA (en) 2020-09-29

Family

ID=57570447

Family Applications (2)

Application Number Title Priority Date Filing Date
SG10202007468VA SG10202007468VA (en) 2015-12-04 2016-11-30 Beta-mercaptoethanol synthesis
SG11201804617WA SG11201804617WA (en) 2015-12-04 2016-11-30 Beta-mercaptoethanol synthesis

Family Applications After (1)

Application Number Title Priority Date Filing Date
SG11201804617WA SG11201804617WA (en) 2015-12-04 2016-11-30 Beta-mercaptoethanol synthesis

Country Status (7)

Country Link
US (2) US9718767B2 (en)
EP (2) EP3380453B1 (en)
KR (2) KR102414346B1 (en)
DK (1) DK3380453T3 (en)
MY (1) MY170005A (en)
SG (2) SG10202007468VA (en)
WO (1) WO2017095873A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9718767B2 (en) 2015-12-04 2017-08-01 Chevron Phillips Chemical Company Lp Beta-mercaptoethanol synthesis
CN109323240A (en) * 2018-10-11 2019-02-12 长治市霍家工业有限公司 Hot water and steam recycle device in a kind of synthesis converter
US10689333B1 (en) 2019-02-22 2020-06-23 Chevron Phillips Chemical Company Lp 2-mercaptoethanol synthesis

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB585655A (en) 1945-08-10 1947-02-14 Foster Neville Woodward Improvements in or relating to the production of monothioethylene glycol
US2776997A (en) * 1953-01-30 1957-01-08 Union Oil Co Preparation of hydroxy thio-ethers
US3086997A (en) 1961-11-07 1963-04-23 Phillips Petroleum Co Synthesis of 2-mercaptoethanol
FR1359678A (en) 1963-01-14 1964-04-30 Aquitaine Petrole Preparation of hydroxythiols
US3366693A (en) 1964-09-16 1968-01-30 Gen Aniline & Film Corp Preparation of mercaptans and sulfides
US3394192A (en) 1966-03-16 1968-07-23 Du Pont Preparation of beta-mercaptoalkanols
US3462496A (en) 1967-01-10 1969-08-19 Dow Chemical Co Method of making mercapto alcohols
US3662004A (en) 1968-04-23 1972-05-09 Henkel & Cie Gmbh Process for producing hydroxyalkyl mercaptans
US3574768A (en) 1968-10-28 1971-04-13 Phillips Petroleum Co Synthesis of beta-mercaptoethanol
DE1914379A1 (en) 1969-03-21 1970-10-01
US3710439A (en) 1970-03-20 1973-01-16 Basf Ag Production of 2-mercaptoethanol
ZA713521B (en) 1970-06-11 1972-01-26 Uniroyal Ltd Preparation of mercaptoethanol
DE2529646A1 (en) 1975-07-03 1977-01-27 Erdoelchemie Gmbh METHOD FOR PRODUCING THIOGLYCOLS
DE3014165C2 (en) 1980-04-12 1984-07-05 Degussa Ag, 6000 Frankfurt Process for the preparation of 3-mercapto-propanediol- (1,2)
JPS56147764A (en) * 1980-04-15 1981-11-16 Toyo Kasei Kogyo Kk Preparation of thioalkylene glycol
US4281202A (en) 1980-04-29 1981-07-28 Pennwalt Corporation Preparation of mercapto-alcohols
FR2483917A1 (en) 1980-06-06 1981-12-11 Elf Aquitaine PRODUCTION OF MERCAPTO-2 ETHANOL-1
JPS6058932A (en) 1983-09-12 1985-04-05 Mitsubishi Gas Chem Co Inc Production of methyl-t-butyl ether
US4564710A (en) 1984-11-08 1986-01-14 Phillips Petroleum Company Process for making mercapto alcohols
FR2609027B1 (en) 1986-12-30 1989-08-11 Elf Aquitaine PROCESS FOR THE PREPARATION OF MERCAPTOALCOOLS
JP2006184251A (en) 2004-12-28 2006-07-13 Tdk Corp Gas sensor
US7399893B2 (en) * 2005-12-13 2008-07-15 Chevron Phillips Chemical Company Lp Process and catalyst for synthesis of mercaptans and sulfides from alcohols
JP2008013453A (en) 2006-07-04 2008-01-24 Sumitomo Chemical Co Ltd Method for producing 2-mercaptoethanol
EP1923384B1 (en) 2006-11-09 2013-06-26 Basf Se Method for manufacturing 2-mercapto ethanol
US7645906B2 (en) * 2007-03-27 2010-01-12 Chevron Phillips Chemical Company Lp Graded catalyst bed for methyl mercaptan synthesis
CN101941928B (en) 2010-08-12 2012-11-21 黑龙江省科学院大庆分院 Synthesis method of sulfhydryl alkyl alcohol
RU2556859C1 (en) 2014-08-05 2015-07-20 Публичное Акционерное общество "Нижнекамскнефтехим"(ПАО "Нижнекамскнефтехим") Method of producing isoprene by catalytic dehydrogenation of isoamylenes in adiabatic reactor
US9718767B2 (en) 2015-12-04 2017-08-01 Chevron Phillips Chemical Company Lp Beta-mercaptoethanol synthesis

Also Published As

Publication number Publication date
US10544094B2 (en) 2020-01-28
US9718767B2 (en) 2017-08-01
US20170291873A1 (en) 2017-10-12
MY170005A (en) 2019-06-20
US20170158630A1 (en) 2017-06-08
KR20180088823A (en) 2018-08-07
EP3597635A1 (en) 2020-01-22
KR102414346B1 (en) 2022-06-28
KR20220038547A (en) 2022-03-28
EP3380453A1 (en) 2018-10-03
EP3380453B1 (en) 2020-12-30
SG11201804617WA (en) 2018-06-28
KR102378698B1 (en) 2022-03-24
WO2017095873A1 (en) 2017-06-08
DK3380453T3 (en) 2021-03-29

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