DK1409162T4 - Fremgangsmåde og indretning til imprægnering af porøse genstande - Google Patents
Fremgangsmåde og indretning til imprægnering af porøse genstande Download PDFInfo
- Publication number
- DK1409162T4 DK1409162T4 DK01994786.0T DK01994786T DK1409162T4 DK 1409162 T4 DK1409162 T4 DK 1409162T4 DK 01994786 T DK01994786 T DK 01994786T DK 1409162 T4 DK1409162 T4 DK 1409162T4
- Authority
- DK
- Denmark
- Prior art keywords
- water
- bath
- washing
- impregnating
- container
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 29
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 66
- 238000005406 washing Methods 0.000 claims abstract description 56
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000004094 surface-active agent Substances 0.000 claims abstract description 36
- 239000011148 porous material Substances 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 238000005470 impregnation Methods 0.000 claims description 9
- 150000001252 acrylic acid derivatives Chemical class 0.000 claims description 6
- 229920001187 thermosetting polymer Polymers 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 5
- 239000000470 constituent Substances 0.000 claims description 3
- 238000005119 centrifugation Methods 0.000 claims 1
- 150000002734 metacrylic acid derivatives Chemical class 0.000 claims 1
- 239000000178 monomer Substances 0.000 description 9
- 239000000203 mixture Substances 0.000 description 7
- 239000011347 resin Substances 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 238000005238 degreasing Methods 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 2
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 2
- INQDDHNZXOAFFD-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOC(=O)C=C INQDDHNZXOAFFD-UHFFFAOYSA-N 0.000 description 2
- HCLJOFJIQIJXHS-UHFFFAOYSA-N 2-[2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOCCOC(=O)C=C HCLJOFJIQIJXHS-UHFFFAOYSA-N 0.000 description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical class CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
- 150000003926 acrylamides Chemical class 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- GMSCBRSQMRDRCD-UHFFFAOYSA-N dodecyl 2-methylprop-2-enoate Chemical compound CCCCCCCCCCCCOC(=O)C(C)=C GMSCBRSQMRDRCD-UHFFFAOYSA-N 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000005058 metal casting Methods 0.000 description 2
- 125000005395 methacrylic acid group Chemical group 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- KEROTHRUZYBWCY-UHFFFAOYSA-N tridecyl 2-methylprop-2-enoate Chemical compound CCCCCCCCCCCCCOC(=O)C(C)=C KEROTHRUZYBWCY-UHFFFAOYSA-N 0.000 description 2
- 239000003643 water by type Substances 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- WFUGQJXVXHBTEM-UHFFFAOYSA-N 2-hydroperoxy-2-(2-hydroperoxybutan-2-ylperoxy)butane Chemical compound CCC(C)(OO)OOC(C)(CC)OO WFUGQJXVXHBTEM-UHFFFAOYSA-N 0.000 description 1
- GNSFRPWPOGYVLO-UHFFFAOYSA-N 3-hydroxypropyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCCCO GNSFRPWPOGYVLO-UHFFFAOYSA-N 0.000 description 1
- JTHZUSWLNCPZLX-UHFFFAOYSA-N 6-fluoro-3-methyl-2h-indazole Chemical compound FC1=CC=C2C(C)=NNC2=C1 JTHZUSWLNCPZLX-UHFFFAOYSA-N 0.000 description 1
- DXPPIEDUBFUSEZ-UHFFFAOYSA-N 6-methylheptyl prop-2-enoate Chemical compound CC(C)CCCCCOC(=O)C=C DXPPIEDUBFUSEZ-UHFFFAOYSA-N 0.000 description 1
- 239000004342 Benzoyl peroxide Substances 0.000 description 1
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- BGNXCDMCOKJUMV-UHFFFAOYSA-N Tert-Butylhydroquinone Chemical compound CC(C)(C)C1=CC(O)=CC=C1O BGNXCDMCOKJUMV-UHFFFAOYSA-N 0.000 description 1
- OKKRPWIIYQTPQF-UHFFFAOYSA-N Trimethylolpropane trimethacrylate Chemical compound CC(=C)C(=O)OCC(CC)(COC(=O)C(C)=C)COC(=O)C(C)=C OKKRPWIIYQTPQF-UHFFFAOYSA-N 0.000 description 1
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 125000005119 alkyl cycloalkyl group Chemical group 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 235000019400 benzoyl peroxide Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- -1 caprolactonacrylate Chemical compound 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 230000009918 complex formation Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- YQHLDYVWEZKEOX-UHFFFAOYSA-N cumene hydroperoxide Chemical compound OOC(C)(C)C1=CC=CC=C1 YQHLDYVWEZKEOX-UHFFFAOYSA-N 0.000 description 1
- OIWOHHBRDFKZNC-UHFFFAOYSA-N cyclohexyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC1CCCCC1 OIWOHHBRDFKZNC-UHFFFAOYSA-N 0.000 description 1
- KBLWLMPSVYBVDK-UHFFFAOYSA-N cyclohexyl prop-2-enoate Chemical compound C=CC(=O)OC1CCCCC1 KBLWLMPSVYBVDK-UHFFFAOYSA-N 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 125000004386 diacrylate group Chemical group 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- LNCPIMCVTKXXOY-UHFFFAOYSA-N hexyl 2-methylprop-2-enoate Chemical compound CCCCCCOC(=O)C(C)=C LNCPIMCVTKXXOY-UHFFFAOYSA-N 0.000 description 1
- LNMQRPPRQDGUDR-UHFFFAOYSA-N hexyl prop-2-enoate Chemical compound CCCCCCOC(=O)C=C LNMQRPPRQDGUDR-UHFFFAOYSA-N 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- PBOSTUDLECTMNL-UHFFFAOYSA-N lauryl acrylate Chemical compound CCCCCCCCCCCCOC(=O)C=C PBOSTUDLECTMNL-UHFFFAOYSA-N 0.000 description 1
- FSAJWMJJORKPKS-UHFFFAOYSA-N octadecyl prop-2-enoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)C=C FSAJWMJJORKPKS-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000008237 rinsing water Substances 0.000 description 1
- 235000019795 sodium metasilicate Nutrition 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000004250 tert-Butylhydroquinone Substances 0.000 description 1
- 235000019281 tert-butylhydroquinone Nutrition 0.000 description 1
- XOALFFJGWSCQEO-UHFFFAOYSA-N tridecyl prop-2-enoate Chemical compound CCCCCCCCCCCCCOC(=O)C=C XOALFFJGWSCQEO-UHFFFAOYSA-N 0.000 description 1
- 229920006305 unsaturated polyester Polymers 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D31/00—Cutting-off surplus material, e.g. gates; Cleaning and working on castings
- B22D31/002—Cleaning, working on castings
- B22D31/005—Sealing or impregnating porous castings
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/40—Specific cleaning or washing processes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Mechanical Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Aftertreatments Of Artificial And Natural Stones (AREA)
- Paper (AREA)
- Polymerisation Methods In General (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
- Cleaning By Liquid Or Steam (AREA)
Claims (9)
1. Fremgangsmåde til imprægnering afen genstand med porer ved indførelse i porerne af et flydende, termohærdende imprægneringsmiddel, som i det væsentlige er fri for vandopløselige bestanddele, afvaskning af overskydende imprægneringsmiddel fra overfladen med vand og hærdning af imprægneringsmidlet ved opvarmning af den imprægnerede genstand, kendetegnet ved, at afvaskningen udføres i et første vaskebad og i et efterfølgende skyllebad, hvorved der tilsættes et eller flere overfladeaktive stoffer til vandet i skyllebadet, og hvor afvaskningen foretages i vaskebadet ved anvendelse af vand, som i det væsentlige er fri for overfladeaktive stoffer, eller som indeholder en mindre mængde af overfladeaktive stoffer end vandet i skyllebadet.
2. Fremgangsmåde ifølge krav 1, kendetegnet ved, at det overskydende imprægneringsmiddel, der afvaskes fra overfladen, genvindes fra vaskebadet og genanvendes til imprægneringen.
3. Fremgangsmåde ifølge krav 2, kendetegnet ved, at overskydende imprægneringsmiddel genvindes fra vaskebadet ved dekantering og/eller centrifugering.
4. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at der anvendes et imprægneringsmiddel, som i det væsentlige er fri for overfladeaktive stoffer.
5. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at der anvendes et imprægneringsmiddel, som indeholderen ellerflere i det væsentlige vanduopløselige acrylater og/eller methacrylater.
6. Fremgangsmåde ifølge et af de foregående krav, kendetegnet ved, at overskydende imprægneringsmiddel fjernes fra skyllebadet ved dekantering og/eller centrifugering.
7. Fremgangsmåde ifølge et af kravene 1 til 6, hvor hærdningen finder sted i vand, kendetegnet ved, at der tilsættes et eller flere overfladeaktive stoffer til vandet.
8. Apparatur til udførelse af fremgangsmåden ifølge ethvert af kravene 1 til 7, omfattende en beholder til imprægnering, en beholder til at kunne rumme et vaskebad og en beholder til at rumme et skyllebad samt indretninger til hærdning, kendetegnet ved, at beholderen til at indeholde vaskebadet har almindeligt anvendte indretninger til dekantering og/eller centrifugering, og beholderen til at indeholde skyllebladet har almindeligt anvendte filtrerings-, dekanterings- og/eller centrifugeringsindretninger, og hvor beholderen til imprægnering indeholder et flydende, varmehærdbart imprægneringsmiddel, som er i det væsentlige fri for vandopløselige komponenter.
9. Apparatur ifølge krav 8, kendetegnet ved, at beholderen til at rumme vaskebadet har indretninger til at returnere fraskilt imprægneringsmiddel til imprægneringsbeholderen.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10062316A DE10062316A1 (de) | 2000-12-14 | 2000-12-14 | Verfahren und Vorrichtung zum Imprägnieren poröser Gegenstände |
PCT/EP2001/014722 WO2002047833A1 (de) | 2000-12-14 | 2001-12-13 | Verfahren und vorrichtung zum imprägnieren poröser gegenstände |
Publications (2)
Publication Number | Publication Date |
---|---|
DK1409162T3 DK1409162T3 (da) | 2009-06-29 |
DK1409162T4 true DK1409162T4 (da) | 2017-04-03 |
Family
ID=7667121
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DK01994786.0T DK1409162T4 (da) | 2000-12-14 | 2001-12-13 | Fremgangsmåde og indretning til imprægnering af porøse genstande |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP1409162B2 (da) |
AT (1) | ATE425821T1 (da) |
DE (2) | DE10062316A1 (da) |
DK (1) | DK1409162T4 (da) |
ES (1) | ES2322554T5 (da) |
WO (1) | WO2002047833A1 (da) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6800328B2 (en) | 2001-07-31 | 2004-10-05 | Ballard Power Systems Inc. | Process for impregnating porous parts |
DE102010050202B4 (de) | 2010-11-04 | 2016-06-23 | Vdt Vakuumdichttechnik Gmbh | Reinigungsvorrichtung und Imprägnierverfahren |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2147387A5 (en) * | 1971-07-26 | 1973-03-09 | Albert Ag Chem Werke | Sealing metal castings - with thermosetting resin by treating in vacuum chamber and low pressure impregnating chamber separated by |
GB1547801A (en) * | 1976-08-17 | 1979-06-27 | Young P D | Stabilized impregnant compositions for porous articles |
DE3215395A1 (de) * | 1982-04-24 | 1983-10-27 | Hübers-Meier oHG, 4290 Bocholt | Wascheinrichtung fuer mit harz o.dgl. impraegnierte teile |
JPS62130202A (ja) * | 1985-12-02 | 1987-06-12 | Honda Motor Co Ltd | 含浸における洗浄方法及び装置 |
DE4001850A1 (de) * | 1990-01-23 | 1991-07-25 | Berghof Elektronik Produktions | Verfahren und vorrichtung zum reinigen von mit monomeren oder oligomeren belasteten spuelwassern |
US5126416A (en) * | 1990-03-26 | 1992-06-30 | Loctite Corporation | Peroxy cured (meth)acrylic ester compositions employing nitrite, borate, silicate or carbonate salt accelerators |
JPH04154822A (ja) * | 1990-10-19 | 1992-05-27 | Chuo Hatsumei Kenkyusho:Kk | 孔質物品の含浸液および処理方法 |
JPH04210212A (ja) * | 1990-12-12 | 1992-07-31 | Nikku Ind Co Ltd | 鋳物含浸液の洗浄排水からのモノマーの回収方法 |
JPH04243506A (ja) * | 1991-01-25 | 1992-08-31 | Chuo Hatsumei Kenkyusho:Kk | 孔質物品の含浸処理方法 |
JPH0724458A (ja) * | 1991-03-27 | 1995-01-27 | Loctite Corp | 含浸処理用洗浄廃水処理方法 |
JP3209426B2 (ja) * | 1991-10-04 | 2001-09-17 | シーエフエムティ インコーポレイテッド | 複雑な形状を有するマイクロパーツの洗浄 |
DE4410193A1 (de) * | 1994-03-24 | 1995-09-28 | Degussa | Verfahren zur Abdichtung von porösen Gegenständen |
-
2000
- 2000-12-14 DE DE10062316A patent/DE10062316A1/de not_active Ceased
-
2001
- 2001-12-13 ES ES01994786.0T patent/ES2322554T5/es not_active Expired - Lifetime
- 2001-12-13 WO PCT/EP2001/014722 patent/WO2002047833A1/de not_active Application Discontinuation
- 2001-12-13 DE DE50114779T patent/DE50114779D1/de not_active Expired - Lifetime
- 2001-12-13 EP EP01994786.0A patent/EP1409162B2/de not_active Expired - Lifetime
- 2001-12-13 DK DK01994786.0T patent/DK1409162T4/da active
- 2001-12-13 AT AT01994786T patent/ATE425821T1/de active
Also Published As
Publication number | Publication date |
---|---|
EP1409162A1 (de) | 2004-04-21 |
DE50114779D1 (de) | 2009-04-30 |
ES2322554T3 (es) | 2009-06-23 |
EP1409162B1 (de) | 2009-03-18 |
EP1409162B2 (de) | 2017-01-04 |
DE10062316A1 (de) | 2002-07-11 |
ES2322554T5 (es) | 2017-07-03 |
DK1409162T3 (da) | 2009-06-29 |
ATE425821T1 (de) | 2009-04-15 |
WO2002047833A1 (de) | 2002-06-20 |
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