DK0494177T3 - Kontinuerlig fremgangsmåde til fremstilling af lavere alkylestere - Google Patents

Kontinuerlig fremgangsmåde til fremstilling af lavere alkylestere

Info

Publication number
DK0494177T3
DK0494177T3 DK90913700.2T DK90913700T DK0494177T3 DK 0494177 T3 DK0494177 T3 DK 0494177T3 DK 90913700 T DK90913700 T DK 90913700T DK 0494177 T3 DK0494177 T3 DK 0494177T3
Authority
DK
Denmark
Prior art keywords
stage
continuous process
lower alkyl
alkyl esters
reactors
Prior art date
Application number
DK90913700.2T
Other languages
Danish (da)
English (en)
Inventor
Lutz Jeromin
Georg Assmann
Gerhard Blasey
Bernhard Gutsche
Jean Rigal
Rene Armengaud
Bernard Cormary
Original Assignee
Henkel Kgaa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel Kgaa filed Critical Henkel Kgaa
Application granted granted Critical
Publication of DK0494177T3 publication Critical patent/DK0494177T3/da

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • B01J19/242Tubular reactors in series
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/03Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00168Controlling or regulating processes controlling the viscosity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00171Controlling or regulating processes controlling the density

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Liquid Carbonaceous Fuels (AREA)
DK90913700.2T 1989-09-29 1990-09-21 Kontinuerlig fremgangsmåde til fremstilling af lavere alkylestere DK0494177T3 (da)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3932514A DE3932514A1 (de) 1989-09-29 1989-09-29 Kontinuierliches verfahren zum herstellen niederer alkylester

Publications (1)

Publication Number Publication Date
DK0494177T3 true DK0494177T3 (da) 1996-07-15

Family

ID=6390460

Family Applications (1)

Application Number Title Priority Date Filing Date
DK90913700.2T DK0494177T3 (da) 1989-09-29 1990-09-21 Kontinuerlig fremgangsmåde til fremstilling af lavere alkylestere

Country Status (10)

Country Link
EP (1) EP0494177B1 (es)
JP (1) JPH05500505A (es)
KR (1) KR920703771A (es)
AT (1) ATE135036T1 (es)
BR (1) BR9007689A (es)
DE (2) DE3932514A1 (es)
DK (1) DK0494177T3 (es)
ES (1) ES2083462T3 (es)
MY (1) MY107286A (es)
WO (1) WO1991005034A1 (es)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT394374B (de) * 1990-06-29 1992-03-25 Wimmer Theodor Verfahren zur herstellung von fettsaeureestern niederer alkohole
DE4123928A1 (de) * 1991-07-19 1993-01-21 Metallgesellschaft Ag Verfahren zum erzeugen von fettsaeure-methylester oder fettsaeure-aethylester und glycerin durch umesterung von oelen oder fetten
DE4209779C1 (es) * 1992-03-26 1993-07-15 Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De
DE4422858C1 (de) 1994-06-30 1995-07-27 Henkel Kgaa Ungesättigte Fettalkohole mit verbessertem Kälteverhalten
DE4436517C1 (de) * 1994-10-13 1995-10-26 Metallgesellschaft Ag Verfahren zum Erzeugen von Fettsäure-Methylester oder Fettsäure-Äthylester und Glycerin durch Umesterung von Öl oder Fett
DE19510098A1 (de) * 1995-03-20 1996-09-26 Henkel Kgaa Verfahren zum Gewinnen von Carotin aus Palmöl
CN1117063C (zh) * 1997-11-24 2003-08-06 能源环境技术股份有限公司 生产脂肪酸甲酯的方法及其生产设备
DE19810440C1 (de) * 1998-03-11 1999-09-23 Dhw Deutsche Hydrierwerke Gmbh Verfahren zur Herstellung von ungesättigten Fettalkoholen aus Lauricölen
DE19956599C2 (de) 1999-11-25 2003-11-13 Cognis Deutschland Gmbh Verfahren zur Herstellung von entsäuerten Triglyceriden
DE10038442A1 (de) 2000-08-07 2002-02-21 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Sterinen aus fettsäurehaltigen Rückständen
DE10043644A1 (de) * 2000-09-05 2002-03-28 Goes Ges Fuer Forschung Und Te Verfahren zur kontinuierlichen Herstellung von Biomethanol- und Bioethanoldiesel in Kleinstanlagen
DE10043575A1 (de) * 2000-09-05 2002-03-28 Biodiesel Plants Res & Enginee Verfahren zur kontinuierlichen Herstellung eines als Kraft- und/oder Brennstoff geeigneten Fettsäurealkylestergemisches sowie Verwendung des Fettsäurealkylesters als Kraft- bzw. Brennstoff
DE20113126U1 (de) * 2001-08-14 2001-11-22 Berger, Bruno, Braunau Umesterungsvorrichtung mit Schrägrohrreaktor
DE10164274B4 (de) * 2001-12-27 2005-12-29 Energietechnik Leipzig Gmbh Verfahren und Vorrichtung zur kontinuierlichen Extraktion von freien Fettsäuren, Tocopherolen und/oder Sterolen aus nativen Ölen und zur Umesterung nativer Öle
DE10210432A1 (de) * 2002-03-09 2003-09-18 Dracowo Forschungs Und Entwick Verfahren zur kontinuierlichen Herstellung von Biomethanoldiesel
ES2278533B1 (es) * 2006-01-20 2008-07-01 Biodiesel De Andalucia 2004, S.A. Procedimiento para la obtencion de un biodiesel a partir de aceites vegetales de grado de acidez variable en sistema continuo y combustible biodiesel obtenido.
WO2008049260A2 (de) * 2006-10-27 2008-05-02 Mecan Ecosystems Ag Verfahren zur herstellung von fettsäureestern
US8070836B2 (en) 2007-10-16 2011-12-06 Wayne State University Combined homogeneous and heterogeneous catalytic transesterification process for biodiesel production
US8975426B2 (en) 2008-05-19 2015-03-10 Wayne State University ZnO nanoparticle catalysts for use in transesterification and esterification reactions and method of making
US8895764B2 (en) 2008-05-19 2014-11-25 Wayne State University ZnO nanoparticle catalysts for use in biodiesel production and method of making
BRPI0913099A2 (pt) 2008-05-19 2019-09-24 Univ Wayne State métodos e catalizadores para preparar biodiesel a partir da transesterificação de óleo não refinados
DE102009006777A1 (de) 2009-01-30 2010-08-05 Wolfgang F. Prof. Dr. Hölderich Verfahren zur Herstellung von Fettsäureestern und Glycerin durch Umesterung von pflanzlichen und tierischen Fetten und Ölen
EP4071226A1 (en) 2021-04-08 2022-10-12 AT Agrar-Technik Int. GmbH Process for producing fatty acid alkyl esters
WO2024017722A1 (en) 2022-07-21 2024-01-25 Basf Se Mixed alkoxide catalyst for biodiesel production

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2360844A (en) * 1941-11-26 1944-10-24 Du Pont Preparation of detergents
GB634411A (en) * 1946-07-16 1950-03-22 Unilever Ltd Method of treating low-grade fatty stock to form alkyl esters therefrom
JPS5665097A (en) * 1979-05-30 1981-06-02 Lion Corp Manufacture of fatty acid lower alcohol ester
EP0131991B1 (de) * 1983-07-12 1986-12-03 Metallgesellschaft Ag Kontinuierliches Alkoholyseverfahren

Also Published As

Publication number Publication date
EP0494177B1 (de) 1996-03-06
EP0494177A1 (de) 1992-07-15
DE59010183D1 (de) 1996-04-11
BR9007689A (pt) 1992-07-21
MY107286A (en) 1995-10-31
ES2083462T3 (es) 1996-04-16
KR920703771A (ko) 1992-12-18
WO1991005034A1 (de) 1991-04-18
JPH05500505A (ja) 1993-02-04
DE3932514A1 (de) 1991-04-18
ATE135036T1 (de) 1996-03-15

Similar Documents

Publication Publication Date Title
DK0494177T3 (da) Kontinuerlig fremgangsmåde til fremstilling af lavere alkylestere
DK0562504T3 (da) Fremgangsmåde til kontinuerlig fremstilling af C1-til C4-alkylestere af højere fedtsyrer
US5514820A (en) Continuous process for the production of lower alkyl esters
MY107920A (en) Process for producing alcohol
TW354784B (en) Sulfonation of fatty acid esters
MX9703727A (es) Preparacion de caprolactama.
CN101450897A (zh) 一种乙酸甘油酯的生产方法
MY113918A (en) Process for the production of phenol
CN105801408A (zh) 一种生产高纯丙烯酸正丁酯的反应精馏装置及方法
DE3817816A1 (de) Verfahren zur herstellung von dimethylether
CN112371185B (zh) 一种多酸催化剂及其制备方法和用途
CN117924135A (zh) 一种叔丁基过氧化碳酸-2-乙基己酯的合成反应和精制方法
CN100526427C (zh) 用高酸值油脂生产生物柴油的催化剂及生物柴油生产方法
CN216005722U (zh) 一种连续反应制备对氨基苯甲酸乙酯的生产系统
CN109824498B (zh) 一种二丙酮醇连续化生产装置及生产工艺
DE102009035387A1 (de) Verfahren und Anordnung zur Umwandlung von Kohlenmonoxid und Wasser in Kohlendioxid und Wasserstoff mit der Abtrennung von zumindest einem Produktgas
CN111978361A (zh) 一种高纯度天麻素的合成方法
CN112174825B (zh) 一种降低以废酸为原料合成硝酸异辛酯酸度的方法
CN103131540A (zh) 一种基于离子液体催化高酸值米糠油制备生物柴油的方法
CN102649732B (zh) Co气相偶联催化反应生产草酸酯的方法
CN101113351A (zh) 生物柴油的固体催化生产方法
GB870356A (en) Preparation of polyvinyl alcohol
CN202315851U (zh) 一种增塑剂的连续酯化生产装置
JPS5585577A (en) Production of cis-epoxysuccinic ester
CN102649733B (zh) Co气体气相催化偶联制草酸酯的方法