DE69916465D1 - Verfahren zur kontinuierlichen herstellung von einem wässerigen gemisch von epsilon-caprolactam und epsilon-caprolactamvorläufern - Google Patents

Verfahren zur kontinuierlichen herstellung von einem wässerigen gemisch von epsilon-caprolactam und epsilon-caprolactamvorläufern

Info

Publication number
DE69916465D1
DE69916465D1 DE69916465T DE69916465T DE69916465D1 DE 69916465 D1 DE69916465 D1 DE 69916465D1 DE 69916465 T DE69916465 T DE 69916465T DE 69916465 T DE69916465 T DE 69916465T DE 69916465 D1 DE69916465 D1 DE 69916465D1
Authority
DE
Germany
Prior art keywords
epsilon
caprolactam
aqueous mixture
continuous production
precursors
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69916465T
Other languages
English (en)
Other versions
DE69916465T2 (de
Inventor
Robert Pestman
Lieshout Hubertus Van
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Invista Technologies SARL Switzerland
Original Assignee
DSM IP Assets BV
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DSM IP Assets BV, EI Du Pont de Nemours and Co filed Critical DSM IP Assets BV
Application granted granted Critical
Publication of DE69916465D1 publication Critical patent/DE69916465D1/de
Publication of DE69916465T2 publication Critical patent/DE69916465T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/04Formation of amino groups in compounds containing carboxyl groups
    • C07C227/06Formation of amino groups in compounds containing carboxyl groups by addition or substitution reactions, without increasing the number of carbon atoms in the carbon skeleton of the acid
    • C07C227/08Formation of amino groups in compounds containing carboxyl groups by addition or substitution reactions, without increasing the number of carbon atoms in the carbon skeleton of the acid by reaction of ammonia or amines with acids containing functional groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/14Preparation of carboxylic acid amides by formation of carboxamide groups together with reactions not involving the carboxamide groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02Preparation of lactams
    • C07D201/08Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Measurement Of Unknown Time Intervals (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
DE69916465T 1998-09-03 1999-09-01 Verfahren zur kontinuierlichen herstellung von einem wässerigen gemisch von epsilon-caprolactam und epsilon-caprolactamvorläufern Expired - Lifetime DE69916465T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP98202943A EP0984002A1 (de) 1998-09-03 1998-09-03 Verfahren zur kontinuierlichen Herstellung von einem wässrigen Gemisch von Epsilon-Caprolactam und Epsilon-Caprolactamvorläufern
EP98202943 1998-09-03
PCT/NL1999/000544 WO2000014062A1 (en) 1998-09-03 1999-09-01 PROCESS TO CONTINUOUSLY PREPARE AN AQUEOUS MIXTURE OF ε-CAPROLACTAM AND εCAPROLACTAM PRECURSORS

Publications (2)

Publication Number Publication Date
DE69916465D1 true DE69916465D1 (de) 2004-05-19
DE69916465T2 DE69916465T2 (de) 2005-03-24

Family

ID=8234084

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69916465T Expired - Lifetime DE69916465T2 (de) 1998-09-03 1999-09-01 Verfahren zur kontinuierlichen herstellung von einem wässerigen gemisch von epsilon-caprolactam und epsilon-caprolactamvorläufern

Country Status (13)

Country Link
US (1) US6452002B2 (de)
EP (2) EP0984002A1 (de)
JP (1) JP2002524441A (de)
KR (1) KR20010073078A (de)
CN (1) CN1142907C (de)
AT (1) ATE264300T1 (de)
AU (1) AU5535699A (de)
CA (1) CA2342364A1 (de)
DE (1) DE69916465T2 (de)
ID (1) ID29478A (de)
MY (1) MY121373A (de)
TW (1) TW461884B (de)
WO (1) WO2000014062A1 (de)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1251122A1 (de) * 2001-04-17 2002-10-23 Dsm N.V. Verfahren zur Herstellung von Epsilon-Caprolactam
KR100667006B1 (ko) * 2006-09-22 2007-01-12 주식회사 도화종합기술공사 공동구내 지중배전 케이블 지지앵글 수평유지 장치
CN101747248B (zh) * 2008-12-03 2012-08-22 中国科学院大连化学物理研究所 一种由5-甲酰基戊酸甲酯制备己内酰胺的方法
JP5512202B2 (ja) * 2009-09-14 2014-06-04 株式会社クラレ β,β−ジメチル−ε−カプロラクタムの製造方法
EP2817293A1 (de) 2012-02-23 2014-12-31 Rennovia, Inc. Gewinnung von caprolactam aus adipinsäure
CN112300047B (zh) * 2019-08-01 2023-02-07 凯特立斯(深圳)科技有限公司 一种串联还原胺化合成手性内酰胺的方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0150295A3 (de) * 1983-12-19 1988-03-30 Allied Corporation Selektive Herstellung von N-substituierten Amiden unter Verwendung von Cu(O)/Metalloxid-Katalysator-Zusammensetzungen
JPS62169769A (ja) * 1986-01-23 1987-07-25 Mitsubishi Heavy Ind Ltd ε−カプロラクタムの合成方法
DE3602377A1 (de) * 1986-01-28 1987-07-30 Basf Ag Verfahren zur herstellung von caprolactam
DE3602378A1 (de) * 1986-01-28 1987-07-30 Basf Ag Verfahren zur herstellung von 6-aminocapronsaeureestern
US5717089A (en) * 1995-03-01 1998-02-10 Dsm N.V. Process for the preparation of E-caprolactam
US5700934A (en) 1995-03-01 1997-12-23 Dsm N.V. Process for the preparation of epsilon-caprolactam and epsilon-caprolactam precursors
MY113899A (en) * 1995-03-01 2002-06-29 Dsm Ip Assets Bv Process for the preparation of (permittivy)-caprolactam and (permittivy)-caprolactam precursors
US5652362A (en) * 1996-05-06 1997-07-29 Industrial Technology Research Institute Preparation of caprolactam
EP0826666A1 (de) * 1996-09-02 1998-03-04 Dsm N.V. Verfahren zur Herstellung von epsilon-Caprolactam
US5877314A (en) 1997-02-14 1999-03-02 Dsm N.V. Process to continuously prepare an aqueous mixture of episilon caprolactum and episilon caprolactum precursors
US5977356A (en) * 1997-07-02 1999-11-02 Industrial Technology Research Institute Process for preparing caprolactam

Also Published As

Publication number Publication date
EP1109781A1 (de) 2001-06-27
US20020007058A1 (en) 2002-01-17
EP0984002A1 (de) 2000-03-08
EP1109781B1 (de) 2004-04-14
WO2000014062A8 (en) 2000-06-08
TW461884B (en) 2001-11-01
CN1142907C (zh) 2004-03-24
ID29478A (id) 2001-08-30
CN1315941A (zh) 2001-10-03
ATE264300T1 (de) 2004-04-15
MY121373A (en) 2006-01-28
DE69916465T2 (de) 2005-03-24
KR20010073078A (ko) 2001-07-31
AU5535699A (en) 2000-03-27
WO2000014062A1 (en) 2000-03-16
JP2002524441A (ja) 2002-08-06
CA2342364A1 (en) 2000-03-16
US6452002B2 (en) 2002-09-17

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: E.I. DUPONT DE NEMOURS AND CO., WILMINGTON, DEL.,

Owner name: INVISTA TECHNOLOGIES S.A.R.L., ZWEIGNIEDERLASSUNG

8327 Change in the person/name/address of the patent owner

Owner name: INVISTA TECHNOLOGIES S.A.R.L., ZWEIGNIEDERLASSUNG