DE69905713D1 - Behälter mit kontrolliertem volumen für mikrowellen assistierte chemische prozesse - Google Patents

Behälter mit kontrolliertem volumen für mikrowellen assistierte chemische prozesse

Info

Publication number
DE69905713D1
DE69905713D1 DE69905713T DE69905713T DE69905713D1 DE 69905713 D1 DE69905713 D1 DE 69905713D1 DE 69905713 T DE69905713 T DE 69905713T DE 69905713 T DE69905713 T DE 69905713T DE 69905713 D1 DE69905713 D1 DE 69905713D1
Authority
DE
Germany
Prior art keywords
cavity
attenuator
assisted chemical
source
microwave assisted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69905713T
Other languages
English (en)
Other versions
DE69905713T2 (de
Inventor
Nelson Mutterer
Price Hargett
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CEM Corp
Original Assignee
CEM Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CEM Corp filed Critical CEM Corp
Application granted granted Critical
Publication of DE69905713D1 publication Critical patent/DE69905713D1/de
Publication of DE69905713T2 publication Critical patent/DE69905713T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122—Incoherent waves
    • B01J19/126—Microwaves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00065—Pressure measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1209—Features relating to the reactor or vessel
    • B01J2219/1212—Arrangements of the reactor or the reactors
    • B01J2219/1218—Multiple reactors

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
DE69905713T 1998-04-20 1999-04-20 Behälter mit kontrolliertem volumen für mikrowellen assistierte chemische prozesse Expired - Lifetime DE69905713T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US09/062,979 US6258329B1 (en) 1998-04-20 1998-04-20 Microwave transparent vessel for microwave assisted chemical processes
US62979 1998-04-20
PCT/US1999/008727 WO1999054033A1 (en) 1998-04-20 1999-04-20 Controlled volume vessel from microwave assisted chemical processes

Publications (2)

Publication Number Publication Date
DE69905713D1 true DE69905713D1 (de) 2003-04-10
DE69905713T2 DE69905713T2 (de) 2004-01-08

Family

ID=22046107

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69905713T Expired - Lifetime DE69905713T2 (de) 1998-04-20 1999-04-20 Behälter mit kontrolliertem volumen für mikrowellen assistierte chemische prozesse

Country Status (8)

Country Link
US (1) US6258329B1 (de)
EP (1) EP1079922B1 (de)
JP (1) JP2002512111A (de)
AT (1) ATE233593T1 (de)
AU (1) AU3658599A (de)
CA (1) CA2328944C (de)
DE (1) DE69905713T2 (de)
WO (1) WO1999054033A1 (de)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6793890B2 (en) * 1997-08-20 2004-09-21 The University Of Miami Rapid tissue processor
US6864092B1 (en) * 1998-08-13 2005-03-08 Symyx Technologies, Inc. Parallel reactor with internal sensing and method of using same
FR2798552B1 (fr) * 1999-09-13 2001-11-30 Centre Nat Rech Scient Dispositif assurant une division de puissance micro-onde predeterminee sur une pluralite de charges, notamment pour la production de plasma
US6753517B2 (en) * 2001-01-31 2004-06-22 Cem Corporation Microwave-assisted chemical synthesis instrument with fixed tuning
US7282184B2 (en) * 2002-04-19 2007-10-16 Cem Corporation Microwave assisted chemical synthesis instrument with controlled pressure release
US6833536B2 (en) 2002-05-22 2004-12-21 Applera Corporation Non-contact radiant heating and temperature sensing device for a chemical reaction chamber
US7144739B2 (en) * 2002-11-26 2006-12-05 Cem Corporation Pressure measurement and relief for microwave-assisted chemical reactions
JP2006524339A (ja) * 2003-04-15 2006-10-26 ブラックライト パワー インコーポレーティド 低エネルギー水素種を生成するためのプラズマ反応炉およびプロセス
KR100554649B1 (ko) * 2003-06-09 2006-02-24 주식회사 아이센스 전기화학적 바이오센서
US7348526B2 (en) * 2004-08-20 2008-03-25 Cem Corporation Microwave-assisted chromatography preparation
EP1827678B1 (de) * 2004-08-31 2012-07-18 Total Synthesis Ltd. Verfahren und vorrichtung zur durchführung von chemischen reaktionen im mikromassstab
CN101180339A (zh) * 2005-05-24 2008-05-14 日立化成工业株式会社 共轭聚合物的制造方法
US20070202607A1 (en) * 2006-02-24 2007-08-30 Revesz Robert N Filtration apparatus and associated method for microwave-assisted chemistry
US7955479B2 (en) * 2006-03-07 2011-06-07 Cem Corporation Method and apparatus for conducting microwave assisted organic reactions with gas-phase reactants
US8349140B2 (en) * 2006-03-16 2013-01-08 Francisco Cereceda Balic Device for extraction of organic chemical compounds with toxic properties, which are present in atmospheric samples, by using solvents heated by the application of focalized microwaves in open systems (not pressurized)
US7744728B2 (en) * 2007-07-13 2010-06-29 Wei-Hsin Chen Apparatus for and method of producing hydrogen using microwaves
JP2009202389A (ja) * 2008-02-27 2009-09-10 Seiko Epson Corp 廃液処理装置
US20090298172A1 (en) 2008-05-28 2009-12-03 Steven Paul Wheeler Histological specimen treatment apparatus and method
US7829040B2 (en) * 2009-03-05 2010-11-09 Cem Corporation High temperature high pressure vessel for microwave assisted chemistry
US9161395B2 (en) 2011-06-30 2015-10-13 Cem Corporation Instrument for performing microwave-assisted reactions
US9522380B2 (en) 2013-06-20 2016-12-20 Cem Corporation Control apparatus for dispensing small precise amounts of liquid reagents
DE102015105925A1 (de) * 2015-04-17 2016-10-20 Krones Ag Vorrichtung zum Erwärmen von Kunststoffvorformlingen mittels Mikrowellen
US10365189B2 (en) 2015-05-07 2019-07-30 Steven Wheeler Histological specimen treatment
US20190048471A1 (en) * 2016-02-24 2019-02-14 Inje University Industry-Academic Cooperation Foudation Nanostructure formation device using microwaves
US10065168B2 (en) 2016-05-02 2018-09-04 Cem Corporation High temperature pressure digestion vessel system with dual action seal
US11351515B2 (en) 2019-03-14 2022-06-07 Cem Corporation Pressure-release vessel with rigid proportional liner and associated microwave-assisted chemistry methods

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3098718A (en) * 1959-09-08 1963-07-23 Technicon Instr Concentration apparatus for quantitative analysis of a substance in a liquid
US3926556A (en) 1973-05-30 1975-12-16 Raymond Marcel Gut Boucher Biocidal electromagnetic synergistic process
US4933529A (en) 1989-04-03 1990-06-12 Savillex Corporation Microwave heating digestion vessel
AU649770B2 (en) 1991-01-25 1994-06-02 Societe Prolabo Apparatus for simultaneous treatment, in a moist medium, on a plurality of samples, and utilisation of the said apparatus
DE4223116A1 (de) 1992-04-30 1993-11-04 Mikrowellen Labor Systeme Vorrichtung zur verdampfungsbehandlung von vorzugsweise fluessigen stoffen, insbesondere reagenzstoffen, oder zum aufbereiten oder analysieren von probenmaterial
DE59407365D1 (de) 1993-06-11 1999-01-14 Werner Lautenschlaeger Rotationsverdampfer
ES2162870T3 (es) * 1993-10-28 2002-01-16 Commw Scient Ind Res Org Reactor de microondas en discontinuo.
DE4401601A1 (de) 1994-01-20 1995-07-27 Lautenschlaeger Werner Topfförmiger Behälter für eine Vorrichtung zur Verdampfungsbehandlung oder Aufbereitung oder Analyse von Stoffen
US5451302A (en) 1994-05-03 1995-09-19 Cha; Chang Y. Process for microwave catalysis of chemical reactions using waveguide liquid films
US5796080A (en) 1995-10-03 1998-08-18 Cem Corporation Microwave apparatus for controlling power levels in individual multiple cells

Also Published As

Publication number Publication date
ATE233593T1 (de) 2003-03-15
EP1079922B1 (de) 2003-03-05
CA2328944A1 (en) 1999-10-28
AU3658599A (en) 1999-11-08
CA2328944C (en) 2003-09-09
US6258329B1 (en) 2001-07-10
EP1079922A1 (de) 2001-03-07
DE69905713T2 (de) 2004-01-08
JP2002512111A (ja) 2002-04-23
WO1999054033A1 (en) 1999-10-28

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