DE69517093T2 - Trennverfahren mittels simulierter Wanderbettchromatographie mit Korrektur des Totvolumens durch erhöhte Förderleistung - Google Patents
Trennverfahren mittels simulierter Wanderbettchromatographie mit Korrektur des Totvolumens durch erhöhte FörderleistungInfo
- Publication number
- DE69517093T2 DE69517093T2 DE69517093T DE69517093T DE69517093T2 DE 69517093 T2 DE69517093 T2 DE 69517093T2 DE 69517093 T DE69517093 T DE 69517093T DE 69517093 T DE69517093 T DE 69517093T DE 69517093 T2 DE69517093 T2 DE 69517093T2
- Authority
- DE
- Germany
- Prior art keywords
- extract
- raffinate
- column
- dead volume
- stream
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000926 separation method Methods 0.000 title description 11
- 238000004587 chromatography analysis Methods 0.000 title description 9
- 239000000203 mixture Substances 0.000 claims description 30
- 238000002347 injection Methods 0.000 claims description 19
- 239000007924 injection Substances 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 19
- 239000012530 fluid Substances 0.000 claims description 18
- 239000003480 eluent Substances 0.000 claims description 13
- 239000007788 liquid Substances 0.000 claims description 11
- 238000011144 upstream manufacturing Methods 0.000 claims description 9
- 238000005070 sampling Methods 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 3
- 239000008246 gaseous mixture Substances 0.000 claims description 3
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 239000011800 void material Substances 0.000 claims 1
- 238000004064 recycling Methods 0.000 description 42
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 8
- 239000007787 solid Substances 0.000 description 8
- 239000007789 gas Substances 0.000 description 5
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000005526 G1 to G0 transition Effects 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- IVSZLXZYQVIEFR-UHFFFAOYSA-N m-xylene Chemical group CC1=CC=CC(C)=C1 IVSZLXZYQVIEFR-UHFFFAOYSA-N 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 230000001360 synchronised effect Effects 0.000 description 2
- WECIKJKLCDCIMY-UHFFFAOYSA-N 2-chloro-n-(2-cyanoethyl)acetamide Chemical compound ClCC(=O)NCCC#N WECIKJKLCDCIMY-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical group [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 210000004534 cecum Anatomy 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 238000001033 granulometry Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052700 potassium Chemical group 0.000 description 1
- 239000011591 potassium Chemical group 0.000 description 1
- 238000004237 preparative chromatography Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1814—Recycling of the fraction to be distributed
- B01D15/1821—Simulated moving beds
- B01D15/1828—Simulated moving beds characterised by process features
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9407762A FR2721527B1 (fr) | 1994-06-22 | 1994-06-22 | Procédé de séparation par chromatographie en lit mobile simulé avec correction de volume mort par augmentation de débit. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69517093D1 DE69517093D1 (de) | 2000-06-29 |
| DE69517093T2 true DE69517093T2 (de) | 2000-09-14 |
Family
ID=9464605
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69517093T Expired - Lifetime DE69517093T2 (de) | 1994-06-22 | 1995-06-15 | Trennverfahren mittels simulierter Wanderbettchromatographie mit Korrektur des Totvolumens durch erhöhte Förderleistung |
Country Status (8)
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2764822B1 (fr) * | 1997-06-19 | 1999-08-13 | Novasep | Methode pour optimiser le fonctionnement d'un systeme de separation des constituants d'un melange |
| FR2772634B1 (fr) * | 1997-12-22 | 2000-02-18 | Inst Francais Du Petrole | Procede et dispositif d'amelioration de la purete d'un produit en lit mobile simule |
| US7048766B2 (en) * | 2003-06-06 | 2006-05-23 | Ferree Bret A | Methods and apparatus for total disc replacements with oblique keels |
| FR2856313B1 (fr) * | 2003-06-17 | 2005-07-29 | Inst Francais Du Petrole | Methode de gestion des vannes d'un systeme de separation a lit mobile simule |
| US6896812B1 (en) | 2003-07-17 | 2005-05-24 | Uop Llc | Process to compensate for a discrete non-separating section in simulated moving bed adsorptive separation processes |
| DE102004025000A1 (de) | 2004-05-21 | 2005-12-08 | Bayer Technology Services Gmbh | Verfahren zur Herstellung von chemischen und pharmazeutischen Produkten mit integrierter Mehrsäulen-Chromatographie |
| EP1840657A1 (en) * | 2006-03-28 | 2007-10-03 | Carl Zeiss SMT AG | Support structure for temporarily supporting a substrate |
| KR100914393B1 (ko) * | 2007-10-19 | 2009-08-28 | 인하대학교 산학협력단 | 4구역 ｓｍｂ 크로마토그래피의 불연속적인 유량조절을이용한 물질의 분리방법 |
| EP3742161B1 (en) * | 2019-05-24 | 2023-07-19 | Sartorius Stedim Biotech GmbH | Chromatography method, method of determining the concentration of at least one compound in a chromatography method and method of obtaining at least one chromatography method parameter |
| EP3742159A1 (en) | 2019-05-24 | 2020-11-25 | Sartorius Stedim Biotech GmbH | Chromatography method, method of determining the influence of the interdependency of at least two parameters in a chromatography method and method of obtaining at least one chromatography method parameter |
| EP3742160B1 (en) | 2019-05-24 | 2023-08-09 | Sartorius Stedim Biotech GmbH | Chromatography method, method of determining the concentration of at least one compound in a chromatography method and method of obtaining at least one chromatography method parameter |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2985589A (en) | 1957-05-22 | 1961-05-23 | Universal Oil Prod Co | Continuous sorption process employing fixed bed of sorbent and moving inlets and outlets |
| US4402832A (en) | 1982-08-12 | 1983-09-06 | Uop Inc. | High efficiency continuous separation process |
| US4498991A (en) | 1984-06-18 | 1985-02-12 | Uop Inc. | Serial flow continuous separation process |
| US4724081A (en) * | 1986-04-28 | 1988-02-09 | Soken Kagaku Kabushiki Kaisha | Process and apparatus for separation by liquid chromatography |
| JPH0669521B2 (ja) * | 1986-12-23 | 1994-09-07 | 三菱化成エンジニアリング株式会社 | クロマト分離法 |
| JPH0746097B2 (ja) * | 1988-05-17 | 1995-05-17 | 三菱化成エンジニアリング株式会社 | クロマト分離法 |
| US4990259A (en) * | 1988-12-16 | 1991-02-05 | The Amalgamated Sugar Company | Chromatographic separator sorbent bed preparation |
| FR2651148B1 (fr) * | 1989-08-28 | 1992-05-07 | Inst Francais Du Petrole | Procede continu et dispositif de separation chromatographique d'un melange d'au moins trois constituants en trois effluents purifies au moyen de deux solvants. |
| FR2651149B1 (fr) * | 1989-08-28 | 1992-06-05 | Inst Francais Du Petrole | Procede continu et dispositif de separation chromatographique d'un melange d'au moins trois constituants en trois effluents purifies au moyen d'un seul solvant a deux temperatures et/ou a deux pressions differentes. |
| WO1991008815A1 (en) * | 1989-12-08 | 1991-06-27 | The Amalgamated Sugar Company | Time variable simulated moving bed process |
| EP0592646B1 (fr) | 1992-04-29 | 1999-02-03 | Institut Francais Du Petrole | Procede et dispositif de fractionnement d'un melange en lit mobile simule en presence d'un gaz comprime, d'un fluide supercritique ou d'un liquide subcritique |
| FR2690630B1 (fr) * | 1992-04-29 | 1994-07-22 | Separex Sa | Procede et dispositif de fractionnement de melanges de composants par voie chromatographique a l'aide d'un eluant a pression supercritique. |
| US5470464A (en) * | 1994-04-06 | 1995-11-28 | Uop | Small scale simulated moving bed separation apparatus and process |
-
1994
- 1994-06-22 FR FR9407762A patent/FR2721527B1/fr not_active Expired - Lifetime
-
1995
- 1995-06-15 EP EP95401407A patent/EP0688588B1/fr not_active Expired - Lifetime
- 1995-06-15 ES ES95401407T patent/ES2148453T3/es not_active Expired - Lifetime
- 1995-06-15 DE DE69517093T patent/DE69517093T2/de not_active Expired - Lifetime
- 1995-06-20 TW TW084106336A patent/TW289737B/zh not_active IP Right Cessation
- 1995-06-22 US US08/494,562 patent/US5582736A/en not_active Expired - Lifetime
- 1995-06-22 JP JP15655295A patent/JP3496104B2/ja not_active Expired - Lifetime
- 1995-06-22 KR KR1019950016819A patent/KR100375980B1/ko not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0688588A1 (fr) | 1995-12-27 |
| US5582736A (en) | 1996-12-10 |
| KR960000277A (ko) | 1996-01-25 |
| DE69517093D1 (de) | 2000-06-29 |
| JPH0843371A (ja) | 1996-02-16 |
| TW289737B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1996-11-01 |
| JP3496104B2 (ja) | 2004-02-09 |
| ES2148453T3 (es) | 2000-10-16 |
| KR100375980B1 (ko) | 2003-05-17 |
| FR2721527A1 (fr) | 1995-12-29 |
| FR2721527B1 (fr) | 1996-09-06 |
| EP0688588B1 (fr) | 2000-05-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8328 | Change in the person/name/address of the agent |
Representative=s name: VONNEMANN, KLOIBER & KOLLEGEN, 80796 MUENCHEN |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: IFP ENERGIES NOUVELLES, RUEIL-MALMAISON, FR |
|
| 8328 | Change in the person/name/address of the agent |
Representative=s name: VONNEMANN, KLOIBER & KOLLEGEN, 81667 MUENCHEN |