DE69431528T2 - Verfahren zur herstellung von trioxan aus formaldehyd - Google Patents

Verfahren zur herstellung von trioxan aus formaldehyd

Info

Publication number
DE69431528T2
DE69431528T2 DE69431528T DE69431528T DE69431528T2 DE 69431528 T2 DE69431528 T2 DE 69431528T2 DE 69431528 T DE69431528 T DE 69431528T DE 69431528 T DE69431528 T DE 69431528T DE 69431528 T2 DE69431528 T2 DE 69431528T2
Authority
DE
Germany
Prior art keywords
formaldehyde
producing trioxane
trioxane
producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69431528T
Other languages
English (en)
Other versions
DE69431528D1 (de
Inventor
W Steele
N Jawaid
Stewart Allen
E Thames
A Reck
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CNA Holdings LLC
Original Assignee
Hoechst Celanese Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Celanese Corp filed Critical Hoechst Celanese Corp
Application granted granted Critical
Publication of DE69431528D1 publication Critical patent/DE69431528D1/de
Publication of DE69431528T2 publication Critical patent/DE69431528T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D323/00—Heterocyclic compounds containing more than two oxygen atoms as the only ring hetero atoms
    • C07D323/04—Six-membered rings
    • C07D323/06—Trioxane
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0476—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds
    • B01J8/048—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds the beds being superimposed one above the other
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69431528T 1993-12-06 1994-12-06 Verfahren zur herstellung von trioxan aus formaldehyd Expired - Fee Related DE69431528T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/162,689 US5767294A (en) 1993-02-17 1993-12-06 Process for the production of trioxane from formaldehyde
PCT/US1994/014008 WO1995015960A1 (en) 1993-12-06 1994-12-06 Process for the production of trioxane from formaldehyde

Publications (2)

Publication Number Publication Date
DE69431528D1 DE69431528D1 (de) 2002-11-14
DE69431528T2 true DE69431528T2 (de) 2003-02-13

Family

ID=22586716

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69431528T Expired - Fee Related DE69431528T2 (de) 1993-12-06 1994-12-06 Verfahren zur herstellung von trioxan aus formaldehyd

Country Status (11)

Country Link
US (1) US5767294A (de)
EP (1) EP0733050B1 (de)
JP (1) JP3859701B2 (de)
KR (1) KR100373955B1 (de)
CN (1) CN1070858C (de)
BR (1) BR9408251A (de)
CA (1) CA2176581A1 (de)
DE (1) DE69431528T2 (de)
SG (1) SG48165A1 (de)
TW (1) TW268004B (de)
WO (1) WO1995015960A1 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19732291A1 (de) * 1997-07-26 1999-01-28 Basf Ag Verfahren zur Abtrennung von Trioxan
DE102008007314A1 (de) * 2008-02-02 2009-08-06 Merck Patent Gmbh Verfahren zur Herstellung von 3,6-Dihydro-1,3,5-triazinderivaten
CN101975838B (zh) * 2010-09-16 2012-10-03 上海蓝星聚甲醛有限公司 三聚甲醛聚合反应器内总酸、硫酸及甲酸含量的测定方法
EP2782906B1 (de) 2011-11-24 2019-05-22 Celanese Sales Germany GmbH Verfahren zur herstellung eines cyclischen acetals
FR3024729B1 (fr) * 2014-08-07 2018-09-07 Arkema France Procede de preparation du trioxane
CN107417662A (zh) * 2017-07-03 2017-12-01 湖北三里枫香科技有限公司 一种液体酸型三聚甲醛生产工艺方法及萃取反应塔
CN107474036A (zh) * 2017-07-03 2017-12-15 湖北三里枫香科技有限公司 一种三聚甲醛生产工艺方法及萃取反应塔
CN111971276A (zh) 2018-03-29 2020-11-20 塞拉尼斯销售德国有限公司 在非均相反应体系中生产环状缩醛的方法
CN108395422A (zh) * 2018-05-16 2018-08-14 凯瑞环保科技股份有限公司 一种三聚甲醛的合成萃取方法及装置
CN111859595B (zh) * 2019-04-16 2024-04-26 左益玮 一种基于多组分多参数动态模型的室内装修甲醛浓度及其衰减的预测方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US432644A (en) * 1890-07-22 Current and switch controlling mechanism
DE1493997C3 (de) * 1964-11-28 1973-11-08 Fa. Josef Meissner, 5000 Koeln Verfahren zur Herstellung von Trioxan
DE1919495A1 (de) * 1969-04-17 1970-10-29 Basf Ag Verfahren zur Herstellung von Trioxan
US3697546A (en) * 1970-01-14 1972-10-10 Japan Gas Chemical Co Method of producing trioxan
CA952132A (en) * 1970-11-12 1974-07-30 Jacob Gorla Minore Ackermann Method of purifying polymerizable organic substances
US4026873A (en) * 1973-04-21 1977-05-31 Agency Of Industrial Science & Technology Needle-like crystals of polyoxymethylene and method for manufacture thereof
US4043873A (en) * 1973-06-15 1977-08-23 Societa' Italiana Resine S.I.R. S.P.A. Plural stage recovery of trioxane in a process having a molecular distillation step
US4110298A (en) * 1976-08-30 1978-08-29 Celanese Corporation Trioxane production
DE2843468A1 (de) * 1978-10-05 1980-04-24 Hoechst Ag Verfahren zur gleichzeitigen herstellung von trioxan und cyclischen formalen
DE2912767A1 (de) * 1979-03-30 1980-10-09 Hoechst Ag Verfahren zur kontinuierlichen herstellung von trioxan
JPS56118079A (en) * 1980-02-22 1981-09-16 Asahi Chem Ind Co Ltd Synthesis of trioxane
JPS57179182A (en) * 1981-04-27 1982-11-04 Asahi Chem Ind Co Ltd Recovering method of trioxane
US4332644A (en) * 1981-06-08 1982-06-01 Asahi Kasei Kogyo Kabushiki Kaisha Process for separating trioxane
DE3421300A1 (de) * 1984-06-08 1985-12-12 Hoechst Ag, 6230 Frankfurt Verfahren zur gewinnung von trioxan aus waessrigen loesungen durch hochdruck-extraktion
DE3445921A1 (de) * 1984-12-17 1986-06-19 Hoechst Ag, 6230 Frankfurt Verfahren zur kontinuierlichen herstellung von trioxan
US5061349A (en) * 1988-12-20 1991-10-29 Kueppenbender Herbert Method of isolating trioxane from aqueous trioxane solutions by distillative separation
JP2872344B2 (ja) * 1990-04-27 1999-03-17 セントラル硝子株式会社 アモルファス材料の形成法およびその装置

Also Published As

Publication number Publication date
CN1070858C (zh) 2001-09-12
SG48165A1 (en) 1998-04-17
EP0733050A1 (de) 1996-09-25
JPH09506105A (ja) 1997-06-17
CN1136812A (zh) 1996-11-27
EP0733050A4 (de) 1997-05-02
WO1995015960A1 (en) 1995-06-15
KR960706487A (ko) 1996-12-09
US5767294A (en) 1998-06-16
KR100373955B1 (ko) 2003-10-04
TW268004B (de) 1996-01-11
BR9408251A (pt) 1997-05-27
EP0733050B1 (de) 2002-10-09
JP3859701B2 (ja) 2006-12-20
DE69431528D1 (de) 2002-11-14
CA2176581A1 (en) 1995-06-15

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8328 Change in the person/name/address of the agent

Representative=s name: VONNEMANN, KLOIBER & KOLLEGEN, 80796 MUENCHEN

8339 Ceased/non-payment of the annual fee