DE69200178D1 - Kryogenverfahren zur Zerlegung von Sauerstoff enthaltenden Mischungen, strukturierte Packung zur Verwendung im selben und Luftdestillationskolonne mit derartiger Packung. - Google Patents

Kryogenverfahren zur Zerlegung von Sauerstoff enthaltenden Mischungen, strukturierte Packung zur Verwendung im selben und Luftdestillationskolonne mit derartiger Packung.

Info

Publication number
DE69200178D1
DE69200178D1 DE69200178T DE69200178T DE69200178D1 DE 69200178 D1 DE69200178 D1 DE 69200178D1 DE 69200178 T DE69200178 T DE 69200178T DE 69200178 T DE69200178 T DE 69200178T DE 69200178 D1 DE69200178 D1 DE 69200178D1
Authority
DE
Germany
Prior art keywords
packing
decomposition
oxygen
distillation column
same
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69200178T
Other languages
English (en)
Other versions
DE69200178T2 (de
Inventor
Jean-Yves Lehman
Jean-Claude Colin
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of DE69200178D1 publication Critical patent/DE69200178D1/de
Application granted granted Critical
Publication of DE69200178T2 publication Critical patent/DE69200178T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04769—Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04854—Safety aspects of operation
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763—Start-up or control of the process; Details of the apparatus used
    • F25J3/04866—Construction and layout of air fractionation equipments, e.g. valves, machines
    • F25J3/04896—Details of columns, e.g. internals, inlet/outlet devices
    • F25J3/04909—Structured packings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/3221—Corrugated sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/32213—Plurality of essentially parallel sheets
    • B01J2219/3222—Plurality of essentially parallel sheets with sheets having corrugations which intersect at an angle different from 90 degrees
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/32224—Sheets characterised by the orientation of the sheet
    • B01J2219/32227—Vertical orientation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
    • B01J2219/32255—Other details of the sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
    • B01J2219/32279—Tubes or cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324—Composition or microstructure of the elements
    • B01J2219/32408—Metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/324—Composition or microstructure of the elements
    • B01J2219/32483—Plastics
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/326—Mathematical modelling
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/50—Oxygen or special cases, e.g. isotope-mixtures or low purity O2
    • F25J2215/56—Ultra high purity oxygen, i.e. generally more than 99,9% O2
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/12—Particular process parameters like pressure, temperature, ratios
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/20—Particular dimensions; Small scale or microdevices
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/44—Particular materials used, e.g. copper, steel or alloys thereof or surface treatments used, e.g. enhanced surface
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/902—Apparatus
    • Y10S62/905—Column

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
DE69200178T 1991-04-19 1992-04-17 Kryogenverfahren zur Zerlegung von Sauerstoff enthaltenden Mischungen, strukturierte Packung zur Verwendung im selben und Luftdestillationskolonne mit derartiger Packung. Expired - Fee Related DE69200178T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9104844A FR2675568B1 (fr) 1991-04-19 1991-04-19 Procede de separation cryogenique de melanges contenant de l'oxygene et garnissages organises pour la mise en óoeuvre de ce procede.

Publications (2)

Publication Number Publication Date
DE69200178D1 true DE69200178D1 (de) 1994-07-14
DE69200178T2 DE69200178T2 (de) 1994-10-06

Family

ID=9412045

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69200178T Expired - Fee Related DE69200178T2 (de) 1991-04-19 1992-04-17 Kryogenverfahren zur Zerlegung von Sauerstoff enthaltenden Mischungen, strukturierte Packung zur Verwendung im selben und Luftdestillationskolonne mit derartiger Packung.

Country Status (6)

Country Link
US (1) US5267444A (de)
EP (1) EP0509929B1 (de)
JP (1) JPH05264167A (de)
CA (1) CA2066366A1 (de)
DE (1) DE69200178T2 (de)
FR (1) FR2675568B1 (de)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4209132A1 (de) * 1992-03-20 1993-09-23 Linde Ag Luftzerlegungsanlage und verfahren zur tieftemperaturzerlegung von luft
FI97277C (fi) * 1993-01-25 1996-11-25 Suomen Sokeri Oy Kromatografinen erotuskolonni, sen sisärakenteet ja kromatografinen erotusmenetelmä
US5419136A (en) * 1993-09-17 1995-05-30 The Boc Group, Inc. Distillation column utilizing structured packing having varying crimp angle
JP3319174B2 (ja) * 1994-09-19 2002-08-26 株式会社日立製作所 充填物及び空気分離装置
CN1091646C (zh) * 1994-10-04 2002-10-02 普莱克斯技术有限公司 用于精炼系统的高容量结构填料
US5730000A (en) * 1996-05-14 1998-03-24 Air Products And Chemicals, Inc. Structured packing element and a mass and heat transfer process using such packing element
US5876638A (en) * 1996-05-14 1999-03-02 Air Products And Chemicals, Inc. Structured packing element with bi-directional surface texture and a mass and heat transfer process using such packing element
US5802858A (en) * 1997-03-27 1998-09-08 Praxair Technology, Inc. Cryogenic cooling tower
US6286818B1 (en) * 1997-07-04 2001-09-11 Kuhni Ag Internal members for mass transfer columns
US6244333B1 (en) 1998-08-27 2001-06-12 Zeks Air Drier Corporation Corrugated folded plate heat exchanger
US6186223B1 (en) 1998-08-27 2001-02-13 Zeks Air Drier Corporation Corrugated folded plate heat exchanger
US6565629B1 (en) * 1998-12-28 2003-05-20 Nippon Sanso Corporation Vapor-liquid contactor, cryogenic air separation unit and method of gas separation
US6378332B1 (en) * 2000-09-07 2002-04-30 Praxair Technology, Inc. Packing with low contacting crimp pattern
TWI351306B (en) 2003-05-16 2011-11-01 Sulzer Chemtech Ag Method of mass transfer of a material or heat
FR2867697B1 (fr) * 2004-03-16 2007-06-01 Air Liquide Structure de garnissage ondule-croise
FR2895069B1 (fr) * 2005-12-20 2014-01-31 Air Liquide Appareil de separation d'air par distillation cryogenique
ITUB20152873A1 (it) * 2015-08-05 2017-02-05 Baretti Mefe S R L Impaccamento strutturato ad alta efficienza e capacita? per colonne di distillazione.
FR3095129B1 (fr) * 2019-04-16 2021-03-12 Air Liquide Garnissage ondulé-croisé en mousse métallique

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE328597B (de) * 1968-04-04 1970-09-21 C Munters
US3612494A (en) * 1968-09-11 1971-10-12 Kobe Steel Ltd Gas-liquid contact apparatus
US4385012A (en) * 1980-01-28 1983-05-24 Ronald Priestley Phase-contacting apparatus
DE3272205D1 (en) * 1981-12-21 1986-08-28 Ici Plc Process for steam reforming a hydrocarbon feedstock and catalyst therefor
SE459826B (sv) * 1984-10-03 1989-08-07 Munters Ab Carl Insatskropp av veckade skikt med speciellt utformade kantpartier
CH664091A5 (de) * 1985-01-30 1988-02-15 Sulzer Ag Packungskoerper aus duennem, folienartigen material fuer stoff- und waermeaustauschkolonnen zwischen fluessigen und gasfoermigen phasen.
US4670196A (en) * 1985-09-05 1987-06-02 Norton Company Tower packing element
US4740334A (en) * 1987-05-29 1988-04-26 Norton Company Tower packing element with embossed surfaces
US4871382A (en) * 1987-12-14 1989-10-03 Air Products And Chemicals, Inc. Air separation process using packed columns for oxygen and argon recovery
BR8901120A (pt) * 1988-03-17 1989-10-31 Union Carbide Corp Elemento de enchimento de coluna;processo para a pratica de transferencia de massa entre vapor e liquido
US4929399A (en) * 1988-03-17 1990-05-29 Union Carbide Industrial Gases Technology Inc. Structured column packing with liquid holdup
US5076823A (en) * 1990-03-20 1991-12-31 Air Products And Chemicals, Inc. Process for cryogenic air separation
US5100448A (en) * 1990-07-20 1992-03-31 Union Carbide Industrial Gases Technology Corporation Variable density structured packing cryogenic distillation system
US5132056A (en) * 1991-05-28 1992-07-21 Union Carbide Industrial Gases Technology Corporation Structured column packing with improved turndown and method

Also Published As

Publication number Publication date
JPH05264167A (ja) 1993-10-12
CA2066366A1 (fr) 1992-10-20
EP0509929B1 (de) 1994-06-08
FR2675568B1 (fr) 1993-07-16
EP0509929A1 (de) 1992-10-21
US5267444A (en) 1993-12-07
DE69200178T2 (de) 1994-10-06
FR2675568A1 (fr) 1992-10-23

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